CN101077079A - Plant-type antibacterial agent - Google Patents
Plant-type antibacterial agent Download PDFInfo
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- CN101077079A CN101077079A CN 200610042869 CN200610042869A CN101077079A CN 101077079 A CN101077079 A CN 101077079A CN 200610042869 CN200610042869 CN 200610042869 CN 200610042869 A CN200610042869 A CN 200610042869A CN 101077079 A CN101077079 A CN 101077079A
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Abstract
The present invention relates to one kind of botanical antiseptic. The botanical antiseptic with plant extracts as main components is superior in antiseptic spectrum, safety, durability, heat resistance and other aspects. It is prepared with phellodendron bark, skullcap root, honeysuckle and other Chinese medicinal materials, and through soaking, decocting, concentrating decoction and alcohol depositing. It has high safety, ideal antiseptic effect, no contamination to product, no environmental pollution and other features, and may be used widely.
Description
Technical field:
The present invention relates to a kind of antibiotic articles for use, is a kind of botanical antiseptic specifically.
Background technology:
Along with social development, self health care consciousness of people is in continuous enhancing, and the personal hygiene nursing materials tends to functionalization gradually, and wherein, the bactericidal function of product receives much concern.So, safe, nuisanceless, the functional strong target that green resists, antibacterial product becomes producer and distributors chases jointly.
China's located in subtropical zone and area, temperate zone totally have a moderate climate, and are well suited for various microbial growths.Especially moist rainy south, various malignant bacterias, mould and saccharomycete are bred in a large number, seriously threaten health.Therefore, the development of antibacterial agent obtains extensive concern in recent years.
According to the difference of composition, antibacterial agent can be divided into natural, organic and inorganic 3 big classes.Inorganic antiseptic, be subjected to the restriction of resource, application has certain difficulty: though organic antibacterial agent has the applicating history in more than 30 year, except that safety (as toxic and side effect, some monomer in addition carcinogenesis is arranged), also have poor heat resistance, easily decompose and problem such as service life is short; Natural antibacterial agent is mainly the extract of natural plants, and all there is advantage in broad-spectrum antiseptic at aspects such as safety, persistence, warm tolerances, so its application and research more and more are subject to people's attention.
The present situation of domestic and international antibacterial agent:
Abroad particularly H originally in recent years antibacterial agent develop very soon.From 1991～nineteen ninety-five, Japanese antibacterial product has entered great development period, and nearly 30 tame enterprises of industries such as chemical industry, fiber, food, motor, cement all develop antibacterial product.At present stoneman nitre, East Asia is synthetic, bell spins and several giant manufacturers' such as Panasonic antibacterial agent occupation rate of market is more than 80% of whole Japanese market.
American-European countries mainly uses inorganic antiseptic at commodity in early days, uses the fashionable U.S. of anti-biotic material and other area in recent years on toy product.According to the U.S. " NAS's journal ", developed the new coating of ethyl PVP by name from the researcher of Massachusetts Polytechnics and TuftsUniversity, they are sprayed on this polymer coating on the sheet glass of using in the laboratory, to observe the performance of polymer coating.As a result, this coating can kill the microorganisms such as iron link chain coccus, pseudomonad and Escherichia coli of glass sheet surface 94% to 99%.Its sterilization mechanism is: by making the adventitia that a kind of reaction upsets microorganism, finally cause microorganism in the fatal position.This special fungicidal paint is expected to be used for the surface of utensils such as toy, computer keyboard and phone, articles for daily use is possessed kill the ability of pathogenic microorganisms.The researcher points out that this coating has purposes widely, can be applied to the surface of multiple material, as produces consumer products with sterilizing ability and medical product etc.As long as regularly clean, the microbial cell of dying in the sterilization material surface just can be flushed away, and material surface recovers disinfection vitality again.China delivers retrospective report " Science and Technology Daily " on January 4th, 2002, claims that the invention of antibiotic paint is the U.S.'s great new technology of calendar year 2001.China scientist notices the huge potential demand and the good development prospect of anti-biotic material for a long time, just followed the tracks of the research and the application of international antibiotic material before more than 10 year, but because the starting point of study condition and input is lower, fail to form the research system of oneself for a long time, fragmentary result of study and world level have big gap, so the research of anti-biotic material and application almost are blank outs.On the other hand, China's economy is backward a lot of with respect to western developed country for a long time, and living standards of the people are not high, so the market of anti-biotic material is up to just making first appearance in recent years.
The unit that China early drops into antibacterial agent research mainly contains Institute of Chemistry, Academia Sinica, Xibei Inst. of Non-Ferrous Metals, Kunming Institute of Precious Metals, Hunan Chemical Research Institute, is engaged in the units such as State Bureau of Building Materials Industry of inorganic chemistry and organic polymer chemical research.Donghua University (former China Textile University) etc. has then carried out antimicrobial treatment in the back arrangement of products such as cotton fiber.At present domestic bigger antibacterial agent manufacturer mainly contains lucky technology Co., Ltd of abundant former plastic-rubber antibacterial agent Co., Ltd of Beijing big octuple scientific ﹠ trading Co., Ltd., Anshan, Shenzhen three, company of section of Haier, Suzhou City rising sun new material Science and Technology Ltd., Xi'an Convrl Rntibiotic Science ﹠ Technique Co., Ltd., Qingdao De Deer Co., Ltd and Hangzhou and reflects day sky cottonrose hibiscus hygienic articles Co., Ltd etc.
Along with going deep into of domestic and international research, the performance of antibacterial agent also will progressively improve, and its range of application also can be more and more extensive.At present, it is cross-centennial environmental protection and health-oriented products that antibacterial product is known as by countries in the world, particularly current anti-chemical and biological weapons, when anti-bacteriological warfare is caught agenda day by day, the overall application of antimicrobial product can fundamentally be stopped the bacterium cross infection between person to person, people and animal, thing and the thing.For this reason, the demand of antibacterial agent has formed enormous and latent market.
Triclosan is as the antibacterial agent of a kind of efficient, wide spectrum, safety, extensive application in daily chemical products and medical disinfectant.The insider points out that from present domestic and international market, its Application and Development has demonstrated the fast-developing impetus, and the triclosan chemical name is 2,4,4 '-three chloro-2 '-dihydroxy diphenyl ethers, is the international at present efficient and environment-friendly type antibacterial agent that extensively adopts.Compare with traditional bactericide, have good stability, consumption is few and advantage such as lasting medicine, be widely used in industries such as daily chemical products, medical disinfectant, infectious disease control, weaving and leather arrangement, all need to use a large amount of these products every year such as P﹠G, Henkel, Uniliver, Ciba, Johnson ﹠ Johnson, worker employed in a plant nursery.Triclosan is mainly with 2 at present, and 5-dichloronitrobenzene and 2,4 dichloro benzene phenol are raw material, through condensation, nitroreduction, the preparation of diazotising hydrolysis.But because technical reason has only Ciba can produce qualified products in a large number.Though China has minority enterprise to produce, product yield and purity are all undesirable, can only export to external major company as primary raw materials.
From now on along with the raising of China's living standards of the people and people to health and healthy attention, pure plant type antibiotic and sterilizing product will become development trend.
Summary of the invention:
The object of the present invention is to provide a kind of antibacterial effect ideal, antibiotic time long, do not damage polluted product, free from environmental pollution and to the plant-type antibacterial agent of human body safety.
For achieving the above object, the technical solution used in the present invention is:
Plant-type antibacterial agent, its contained active ingredient is made by the following weight proportion raw material:
Golden cypress 28-38 part root of large-flowered skullcap 28-38 part honeysuckle 20-28 part.
Plant-type antibacterial agent, its contained active ingredient is made by the following weight proportion raw material:
26 parts of 37 portions of honeysuckles of 37 parts of roots of large-flowered skullcap of golden cypress.
The preparation technology of above-mentioned plant-type antibacterial agent is as follows:
(1), the raw material after Chinese medicine material cleaned decocts 2 times, each 2 hours, the simmer down to relative density was the concentrate of 1.1-1.12 again;
(2), again 95% the ethanol that adds 3 times of amounts, alcohol precipitation, carry alcohol, filter after, add pure water and form brown liquid, get final product.
The present invention to human body safety, good with the goods compatibility, antibacterial effect is desirable, the antibiotic time is long, do not damage polluted product, characteristics such as free from environmental pollution, easy to use.Now as popular antibacterial agent in the world because of its in sterilization, superior function on lasting antibacterial, particularly characteristic such as its non-stimulated, safety and environmental protection makes it be widely applied to fields such as amenities, detergents and cosmetic, health care.
Pure drug ingedient is composite forms with the root of large-flowered skullcap and other for this product, can make amenities realize sterilization in process of production, the colleague can guarantee to avoid secondary pollution in the packing preservation process, and the growth of the pathogenic bacteria that can suppress newly to be infected with in use, has the long acting antibiotic function, have no side effect, healthy and safe, can satisfy the needs of " effect product sterilization " and " sterile products " simultaneously.
Embodiment:
Specific embodiment 1:
Plant-type antibacterial agent, its contained active ingredient is made by the following weight proportion raw material:
Golden cypress 37g root of large-flowered skullcap 37g honeysuckle 26g;
The preparation technology of above-mentioned plant-type antibacterial agent is as follows:
(1), the raw material after Chinese medicine material cleaned decocts 2 times, each 2 hours, the simmer down to relative density was the concentrate of 1.1-1.12 again;
(2), again 95% the ethanol that adds 3 times of amounts, alcohol precipitation, carry alcohol, filter after, add pure water and form brown liquid, get final product.
Specific embodiment 2:
Plant-type antibacterial agent, its contained active ingredient is made by the following weight proportion raw material:
Golden cypress 28g root of large-flowered skullcap 28g honeysuckle 20g;
The preparation technology of above-mentioned plant-type antibacterial agent is identical with specific embodiment 1.
Specific embodiment 3:
Plant-type antibacterial agent, its contained active ingredient is made by the following weight proportion raw material:
Golden cypress 38g root of large-flowered skullcap 38g honeysuckle 28g;
The preparation technology of above-mentioned plant-type antibacterial agent is identical with specific embodiment 1.
For verifying bactericidal and bacteriostatic effect of the present invention:
Through the check of disease prevention and control center, Shaanxi Province, the sterilization experiment result is as follows:
| Liquor strength (is 100% with finished product) | Bacterial classification and quantity | Time (branch) | Killing rate (%) |
| 50％ | Staphylococcus aureus (ATCC6538) 2.9 * 10 6Individual/ | 5 | 99.9999 |
| Sheet | |||
| 50％ | Escherichia coli (ATCC8099) 5.7 * 10 5Individual/ml | 5 | 99.999 |
| 50％ | Candida albicans (ATCC10231) 2.9 * 10 6Individual/ml | 5 | 100.00 |
| 100％ | Withered grass gemma (ATCC9372) 2.9 * 10 7Individual/sheet | 5 | 99.9172 |
| 100％ | Hepatitis B surface antigen (Purification of HBsAg) 5ug/ml | 5 | P/N 1.07(-) |
| 25％ | Gonococcus 9 * 10 5Individual/ml | 5 | 99.9999 |
| 50％ | Trichomonas 7.5 * 10 9/L | 5 | 97.88 |
This product proterties is as follows:
[characteristic]:
1, the high-purity brown liquid of fragrant is not infected with product and skin.
2, be dissolved in multiple organic solvent and surfactant.
3, strong acid and strong base and heat had high stability.
4, infect or pathogenicity is removed from office blue formula positive bacteria, fungi, yeast and virus (as first, hepatitis B, rabies virus, AIDS virus HTV) etc. and all had and kill widely and inhibitory action causing.
5, to the skin nonirritant.
6, effective equally to antiviral antibiotic and non-antibiotic.
[characteristic and quality index]:
1, proterties: brown transparency liquid, tasteless or fragranced slightly.
2, dissolubility: water-soluble, make transparent concentrated liquid product.
3, quality index:
Content 99.0-100.0% (HPLC)
57 ± 10 ℃ of fusing points
Loss on drying＜0.1%
Ash＜0.1%
Heavy metal (in ph)＜10ppm
[security performance]:
Product and human body skin have good intermiscibility, animal toxicology experiment has widely for a long time proved that also this product is under the suggestion scope of application and consumption, can reach the international standard of the world today to chemical toxicity, be the safe and efficient broad spectrum antimicrobicide of praising highly in the world at present.
National product monitoring authoritative department is tested this product: chmice acute per os toxicity test, LD
50＞5000mg/kg body weight, according to the toxicology acute toxicity grading criteria, the nontoxic level in the true border of product; Irritant experiment: the stoste with 1%, 5%, 10% evenly is applied to cavy depilation district, covers with yarn and fixes, and continues 6 days, and the 7th day, the 13rd day repeats once equally, and product sensitization rate is zero.
[anti-microbial property]:
This product is the high-efficiency broad spectrum antibacterial agent, and gram-positive bacteria, negative bacterium, yeast and virus are all killed and inhibitory action.The disease-resistant performance of this product is tested, and its minimal inhibitory concentration is as follows: microorganism MIC (PPm).Staphylococcus glucose coccus: must not detect hemolytic streptococcus: must not detect Escherichia coli: must not detect Pseudomonas aeruginosa: must not detect, total number of bacterial colonies: 125, fungus colony sum: 20.
[using and scope]:
This product is widely used in efficient medicated soap/health perfumed soap, sanitary lotion, remove internal organs smelly/pin aerosol, disinfection hand cleanser, wound disinfection spray, medical device disinfectant, health mildy wash/cream, air freshener and deodorant for refrigerator etc., also be used for the arrangement of hygiene tissue and the anticorrosion and processing of plastics, more highly purified also being widely used in curative effect toothpaste such as treating tooth plough inflammation, periodontitis and canker sore and the mouthwash, the suggestion working concentration is 0.05%-0.3%.
[storage]: hermetically drying, shady place are stored, and storage temperature is no more than 40 ℃
The present invention is mainly used in antibiotic, the cleaning-nursing of skin.
Claims (3)
1, plant-type antibacterial agent is characterized in that its contained active ingredient made by the following weight proportion raw material:
Golden cypress 28-38 part root of large-flowered skullcap 28-38 part honeysuckle 20-28 part.
2, plant-type antibacterial agent according to claim 1 is characterized in that its contained active ingredient made by the following weight proportion raw material:
26 parts of 37 portions of honeysuckles of 37 parts of roots of large-flowered skullcap of golden cypress.
3, plant-type antibacterial agent according to claim 1 and 2 is characterized in that: the preparation technology of described plant-type antibacterial agent is as follows:
(1), the raw material after Chinese medicine material cleaned decocts 2 times, each 2 hours, the simmer down to relative density was the concentrate of 1.1-1.12 again;
(2), again 95% the ethanol that adds 3 times of amounts, alcohol precipitation, carry alcohol, filter after, add pure water and form brown liquid, get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100428698A CN100551244C (en) | 2006-05-25 | 2006-05-25 | Plant-type antibacterial agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100428698A CN100551244C (en) | 2006-05-25 | 2006-05-25 | Plant-type antibacterial agent |
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| CN101077079A true CN101077079A (en) | 2007-11-28 |
| CN100551244C CN100551244C (en) | 2009-10-21 |
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| CNB2006100428698A Active CN100551244C (en) | 2006-05-25 | 2006-05-25 | Plant-type antibacterial agent |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101766193B (en) * | 2010-01-12 | 2012-11-21 | 武汉工程大学 | Disinfecting and antiseptic Chinese patent medicine and preparation method thereof |
| CN103039538A (en) * | 2012-12-25 | 2013-04-17 | 浙江农林大学 | Refrigerator deodorization sterilization liquid containing Chinese herbal medicines and application thereof |
| CN103194341A (en) * | 2013-04-25 | 2013-07-10 | 上海巴方精细化工有限公司 | Low-irritation baical skullcap root skin care soap |
| CN103749564A (en) * | 2014-02-08 | 2014-04-30 | 王贵年 | Composite plant disinfectant and preparation method thereof |
| CN103835126A (en) * | 2013-12-12 | 2014-06-04 | 青岛无为保温材料有限公司 | Novel mildew preventive for textile, and preparation method thereof |
| CN104255823A (en) * | 2014-09-15 | 2015-01-07 | 天津郁美净集团有限公司 | Plant bacteriostatic composition and application thereof in liquid detergent |
| CN105434298A (en) * | 2015-06-30 | 2016-03-30 | 厦门医学高等专科学校 | Natural Chinese prescription mouthwash |
| CN106283336A (en) * | 2016-08-08 | 2017-01-04 | 福建万鸿纺织有限公司 | A kind of antibacterial comfortable nylon fabric and preparation method thereof |
| CN107197886A (en) * | 2017-06-27 | 2017-09-26 | 陈魏魏 | Towel soaks degerming medicament |
| CN107302917A (en) * | 2016-04-21 | 2017-10-31 | 上海新舒环环保科技有限公司 | It is a kind of to prevent and treat the preparation method that pythium spp realizes soil remediation |
| CN108042610A (en) * | 2018-02-05 | 2018-05-18 | 上海御齿台医疗科技有限公司 | Safety plantation dental restortion liquid and preparation method thereof |
| CN108721503A (en) * | 2018-08-22 | 2018-11-02 | 南阳市中心医院 | One kind is for anti-infectious drug of postoperative wound and preparation method thereof |
| CN109125180A (en) * | 2018-10-15 | 2019-01-04 | 山东麦德森医疗科技有限公司 | A kind of preparation and its detection test method of Traditional Chinese medicinal hand lotion |
| CN110179879A (en) * | 2019-06-28 | 2019-08-30 | 成都中医药大学 | A kind of pharmaceutical composition that treating oral inflammation disease and preparation method and purposes |
| CN111467402A (en) * | 2020-05-13 | 2020-07-31 | 黄敏 | Antibacterial traditional Chinese medicine extracting solution and preparation method and application thereof |
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2006
- 2006-05-25 CN CNB2006100428698A patent/CN100551244C/en active Active
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101766193B (en) * | 2010-01-12 | 2012-11-21 | 武汉工程大学 | Disinfecting and antiseptic Chinese patent medicine and preparation method thereof |
| CN103039538B (en) * | 2012-12-25 | 2016-06-29 | 浙江农林大学暨阳学院 | A kind of refrigerator deodorization sterilization liquid containing Chinese herbal medicine and application thereof |
| CN103039538A (en) * | 2012-12-25 | 2013-04-17 | 浙江农林大学 | Refrigerator deodorization sterilization liquid containing Chinese herbal medicines and application thereof |
| CN103194341A (en) * | 2013-04-25 | 2013-07-10 | 上海巴方精细化工有限公司 | Low-irritation baical skullcap root skin care soap |
| CN103835126A (en) * | 2013-12-12 | 2014-06-04 | 青岛无为保温材料有限公司 | Novel mildew preventive for textile, and preparation method thereof |
| CN103835126B (en) * | 2013-12-12 | 2016-08-17 | 青岛无为保温材料有限公司 | A kind of anti-mildew agent for textiles and preparation method thereof |
| CN103749564A (en) * | 2014-02-08 | 2014-04-30 | 王贵年 | Composite plant disinfectant and preparation method thereof |
| CN103749564B (en) * | 2014-02-08 | 2015-08-05 | 王贵年 | A kind of composite plant disinfectant and preparation method thereof |
| CN104255823A (en) * | 2014-09-15 | 2015-01-07 | 天津郁美净集团有限公司 | Plant bacteriostatic composition and application thereof in liquid detergent |
| CN104255823B (en) * | 2014-09-15 | 2017-04-05 | 天津郁美净集团有限公司 | A kind of plant bacteriostatic composition and its application in liquid detergent |
| CN105434298A (en) * | 2015-06-30 | 2016-03-30 | 厦门医学高等专科学校 | Natural Chinese prescription mouthwash |
| CN105434298B (en) * | 2015-06-30 | 2018-11-02 | 厦门医学院 | A kind of natural Chinese prescription mouthwash |
| CN107302917A (en) * | 2016-04-21 | 2017-10-31 | 上海新舒环环保科技有限公司 | It is a kind of to prevent and treat the preparation method that pythium spp realizes soil remediation |
| CN106283336A (en) * | 2016-08-08 | 2017-01-04 | 福建万鸿纺织有限公司 | A kind of antibacterial comfortable nylon fabric and preparation method thereof |
| CN106283336B (en) * | 2016-08-08 | 2018-04-10 | 福建万鸿纺织有限公司 | A kind of comfortable nylon fabric of antibacterial and preparation method thereof |
| CN107197886A (en) * | 2017-06-27 | 2017-09-26 | 陈魏魏 | Towel soaks degerming medicament |
| CN108042610A (en) * | 2018-02-05 | 2018-05-18 | 上海御齿台医疗科技有限公司 | Safety plantation dental restortion liquid and preparation method thereof |
| CN108042610B (en) * | 2018-02-05 | 2021-02-19 | 上海御齿台医疗科技有限公司 | Safe dental implant restoration liquid and preparation method thereof |
| CN108721503A (en) * | 2018-08-22 | 2018-11-02 | 南阳市中心医院 | One kind is for anti-infectious drug of postoperative wound and preparation method thereof |
| CN109125180A (en) * | 2018-10-15 | 2019-01-04 | 山东麦德森医疗科技有限公司 | A kind of preparation and its detection test method of Traditional Chinese medicinal hand lotion |
| CN110179879A (en) * | 2019-06-28 | 2019-08-30 | 成都中医药大学 | A kind of pharmaceutical composition that treating oral inflammation disease and preparation method and purposes |
| CN111467402A (en) * | 2020-05-13 | 2020-07-31 | 黄敏 | Antibacterial traditional Chinese medicine extracting solution and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100551244C (en) | 2009-10-21 |
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Address after: 710075, twenty-two floor, Shanxi Securities Building, 2 hi tech two road, Shaanxi, Xi'an Patentee after: Xi'an Greens Biologic Medicine Co., Ltd. Address before: 710075, seven floor, Shanxi Securities Building, 2 hi tech two road, Shaanxi, Xi'an Patentee before: Xi'an Greens Biologic Medicine Co., Ltd. |
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