CN106283336A - A kind of antibacterial comfortable nylon fabric and preparation method thereof - Google Patents
A kind of antibacterial comfortable nylon fabric and preparation method thereof Download PDFInfo
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- CN106283336A CN106283336A CN201610641262.5A CN201610641262A CN106283336A CN 106283336 A CN106283336 A CN 106283336A CN 201610641262 A CN201610641262 A CN 201610641262A CN 106283336 A CN106283336 A CN 106283336A
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/54—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads coloured
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
- D01F6/60—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyamides
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/10—Patterned fabrics or articles
- D04B1/12—Patterned fabrics or articles characterised by thread material
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B21/00—Warp knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B21/06—Patterned fabrics or articles
- D04B21/08—Patterned fabrics or articles characterised by thread material
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/16—Physical properties antistatic; conductive
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- Chemical Kinetics & Catalysis (AREA)
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- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses a kind of antibacterial comfortable nylon fabric and preparation method thereof, counting by weight, the raw material of described nylon fabric includes: slices of caprone 100 ~ 110 parts, antibacterial nylon agglomerate 5 ~ 8 parts, moisture-absorption modifier 3 ~ 5 parts, antioxidant SEED 0.5 ~ 1 part and antistatic agent 0.5 ~ 1 part.The nylon fabric that the present invention prepares adds load silver Maifanitum antibacterial, impregnate in antimicrobial fluid subsequently, had the antibacterial action of antimicrobial component in inorganic antiseptic and natural Chinese medicinal herb, two-ways regulation concurrently, serve the strongest bactericidal effect, the clearance of various antibacterials is up to more than 99%.Additionally, the nylon fabric that the present invention prepares has good hygroscopicity, water absorption and antistatic property, there is the highest practical value, and preparation technology is simple, is suitable for promoting the use of.
Description
Technical field
The invention belongs to textile technology field, be specifically related to a kind of antibacterial comfortable nylon fabric and preparation method thereof.
Background technology
Nylon fibre is to realize industrialized synthetic fibers the most the earliest, has intensity height, good springiness, wearability good etc.
Feature, becomes one of most popular fiber of twentieth century.But along with expanding economy and the raising of people's living standard, people couple
Comfortable, health, the pursuit of healthy dress ornament and the demand of other special dimensions, conventional chinlon product can not meet.
And the nylon fibre of routine is easily generated electrostatic, and make because of Electrostatic Absorption fabric face dust suction many, add the antiperspirant that human body is discharged
Liquid, easily bacterial growth, therefore exploitation has the comfortable nylon fabric of anti-bacterial anti-foul function is of great practical value.
Summary of the invention
Present invention aims to prior art not enough, it is provided that a kind of antibacterial comfortable nylon fabric and preparation side thereof
Method.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of antibacterial comfortable nylon fabric, counts by weight, and its raw material includes:
Slices of caprone: 100 ~ 110 parts；
Antibacterial nylon agglomerate: 5 ~ 8 parts；
Moisture-absorption modifier: 3 ~ 5 parts；
Antioxidant SEED:0.5 ~ 1 part；
Antistatic agent: 0.5 ~ 1 part；
Described moisture-absorption modifier is polyvinylpyrrolidone；Described antistatic agent is fatty alcohol-polyoxyethylene ether.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps:
(1) preparation of silver Maifanitum antibacterial is carried: after taking Maifanitum 200 mesh sieves excessively after crushed, after cleaning twice with distilled water
It is dried to obtain medical stone powder, standby；The AgNO of preparation 0.008mol/L3Solution, joins prepared AgNO by medical stone powder3Molten
In liquid, after stirring 2h, mixed liquor, to 7.0, is carried out sucking filtration by regulation pH value of solution subsequently, and sucking filtration gained filter cake distilled water flushing is straight
Without Ag to washing liquid+；Pulverize after the filtration cakes torrefaction of gained, prepare and carry silver Maifanitum antibacterial；Described load silver wheat meal
In stone antibacterial, by mass percentage, Maifanitum accounts for 96 ~ 98%, AgNO3Account for 2 ~ 4%；
(2) preparation of antibacterial nylon agglomerate: in mixer, the load silver Maifanitum taking 10 ~ 15 weight portion steps (1) prepared is antibacterial
After agent carries out surface Anti-tarnishing process, add the silane coupler mix homogeneously of 0.5 ~ 2 weight portion, obtain antimicrobial mix；
Melt extrude in double screw extruder after the slices of caprone of gained antimicrobial mix and 60 ~ 80 weight portions is mixed, prepare
Antibacterial matrices.
The preparation method of the most antibacterial comfortable nylon fabric, specifically includes following steps:
(1) use melted after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent being mixed
Spin processes carries out spinning；
(2) nylon fibre step (1) obtained prepares nylon fibre yarn through textile technology, and gained nylon fibre spins
Line prepares nylon fabric through dyeing and finishing technology again；
(3) being impregnated in antimicrobial fluid 30 minutes by the nylon fabric that step (2) obtains, bath raio is 1:25；
(4) nylon fabric after step (3) being impregnated prepares described antibacterial comfortable nylon fabric after drying.
Antimicrobial fluid described in step (3), counts by weight, and its raw material includes: gold 25 ~ 30 parts of clock rattan, Herba Portulacae 10 ~ 12
Part, the Fructus Evodiae 15 ~ 20 parts, Folium Musae 10 ~ 15 parts and Radix et Caulis Opuntiae Dillenii 8 ~ 10 parts；The preparation method of described antimicrobial fluid is:
(A) Radix et Caulis Opuntiae Dillenii cleaned and go the laggard row of the removal of impurity to squeeze to obtain Radix et Caulis Opuntiae Dillenii juice and Radix et Caulis Opuntiae Dillenii slag, toward gained Radix et Caulis Opuntiae Dillenii slag
In add the water of 4 times of weight, extract 2 hours at 60 DEG C, filter to obtain Radix et Caulis Opuntiae Dillenii slag extracting solution, by gained Radix et Caulis Opuntiae Dillenii juice and celestial being
Palm slag extracting solution mixes to obtain cactus extraction；
(B) depletion clock rattan, Herba Portulacae, the Fructus Evodiae and the Folium Musae boiling water of 8 times of weight decocts twice, each 1.5 hours, filters also
And merge twice filtrate, by gained filtrate reconcentration be relative density be the concentrated solution of 1.1；Add in the concentrated solution obtained
The ethanol of the 95wt% of 5 times of weight, carries out reflux, extract, 2 times, each 1.5 hours, reclaims ethanol, obtains mixed liquor；
(C) desolventing technology is carried out after being mixed by mixed liquor prepared with step (B) for cactus extraction prepared for step (A), system
Obtain antimicrobial fluid.
The beneficial effects of the present invention is:
(1) the nylon fabric antibacterial effect that the present invention prepares is notable, adds load silver Maifanitum antibacterial, profit in its antibacterial matrices
By the characteristic of Maifanitum high-specific surface area, as the carrier of antibacterial, on the one hand can good Adsorption For Ag ion；The opposing party
Face, due to pole Porous state and the abundant-Si-O atomic group of Maifanitum, antibacterial just can be played good suction by itself
Attached effect；Additionally, the present invention adds load silver Maifanitum antibacterial the most in the feed, impregnate in antimicrobial fluid subsequently, have concurrently
The antibacterial action of the antimicrobial component in inorganic antiseptic and natural Chinese medicinal herb, two-ways regulation, serve the strongest bactericidal effect,
The clearance of various antibacterials is up to more than 99%；
(2) nylon fabric that the present invention prepares has good hygroscopicity, water absorption and antistatic property, has the highest reality
By value, and preparation technology is simple, is suitable for promoting the use of.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described, but the present invention is not limited only to these embodiments.
Embodiment 1
A kind of antibacterial comfortable nylon fabric, counts by weight, and its raw material includes:
Slices of caprone: 100 parts；
Antibacterial nylon agglomerate: 5 parts；
Polyvinylpyrrolidone: 3 parts；
Antioxidant SEED:0.5 part；
Fatty alcohol-polyoxyethylene ether: 0.5 part.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps:
(1) preparation of silver Maifanitum antibacterial is carried: after taking Maifanitum 200 mesh sieves excessively after crushed, after cleaning twice with distilled water
It is dried to obtain medical stone powder, standby；The AgNO of preparation 0.008mol/L3Solution, joins prepared AgNO by medical stone powder3Molten
In liquid, after stirring 2h, mixed liquor, to 7.0, is carried out sucking filtration by regulation pH value of solution subsequently, and sucking filtration gained filter cake distilled water flushing is straight
Without Ag to washing liquid+；Pulverize after the filtration cakes torrefaction of gained, prepare and carry silver Maifanitum antibacterial；Described load silver wheat meal
In stone antibacterial, by mass percentage, Maifanitum accounts for 96%, AgNO3Account for 4%；
(2) preparation of antibacterial nylon agglomerate: in mixer, takes the load silver Maifanitum antibacterial that 10 weight portion steps (1) prepare
After carrying out surface Anti-tarnishing process, add the silane coupler mix homogeneously of 0.5 weight portion, obtain antimicrobial mix；By institute
Melt extrude in double screw extruder after obtaining the slices of caprone mixing of antimicrobial mix and 60 weight portions, prepare antibacterial mother
Grain.
The preparation method of the most antibacterial comfortable nylon fabric, specifically includes following steps:
(1) use melted after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent being mixed
Spin processes carries out spinning；
(2) nylon fibre step (1) obtained prepares nylon fibre yarn through textile technology, and gained nylon fibre spins
Line prepares nylon fabric through dyeing and finishing technology again；
(3) being impregnated in antimicrobial fluid 30 minutes by the nylon fabric that step (2) obtains, bath raio is 1:25；
(4) nylon fabric after step (3) being impregnated prepares described antibacterial comfortable nylon fabric after drying.
Antimicrobial fluid described in step (3), counts by weight, and its raw material includes: gold 25 parts of clock rattan, Herba Portulacae 10 parts, Zhu
Cornel 15 parts, Folium Musae 10 parts and Radix et Caulis Opuntiae Dillenii 8 parts.
Embodiment 2
A kind of antibacterial comfortable nylon fabric, counts by weight, and its raw material includes:
Slices of caprone: 110 parts；
Antibacterial nylon agglomerate: 8 parts；
Polyvinylpyrrolidone: 5 parts；
Antioxidant SEED:1 part；
Fatty alcohol-polyoxyethylene ether: 1 part.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps:
(1) preparation of silver Maifanitum antibacterial is carried: after taking Maifanitum 200 mesh sieves excessively after crushed, after cleaning twice with distilled water
It is dried to obtain medical stone powder, standby；The AgNO of preparation 0.008mol/L3Solution, joins prepared AgNO by medical stone powder3Molten
In liquid, after stirring 2h, mixed liquor, to 7.0, is carried out sucking filtration by regulation pH value of solution subsequently, and sucking filtration gained filter cake distilled water flushing is straight
Without Ag to washing liquid+；Pulverize after the filtration cakes torrefaction of gained, prepare and carry silver Maifanitum antibacterial；Described load silver wheat meal
In stone antibacterial, by mass percentage, Maifanitum accounts for 98%, AgNO3Account for 2%；
(2) preparation of antibacterial nylon agglomerate: in mixer, takes the load silver Maifanitum antibacterial that 15 weight portion steps (1) prepare
After carrying out surface Anti-tarnishing process, add the silane coupler mix homogeneously of 2 weight portions, obtain antimicrobial mix；By gained
Melt extrude in double screw extruder after the slices of caprone mixing of antimicrobial mix and 80 weight portions, prepare antibacterial matrices.
The preparation method of the most antibacterial comfortable nylon fabric, specifically includes following steps:
(1) use melted after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent being mixed
Spin processes carries out spinning；
(2) nylon fibre step (1) obtained prepares nylon fibre yarn through textile technology, and gained nylon fibre spins
Line prepares nylon fabric through dyeing and finishing technology again；
(3) being impregnated in antimicrobial fluid 30 minutes by the nylon fabric that step (2) obtains, bath raio is 1:25；
(4) nylon fabric after step (3) being impregnated prepares described antibacterial comfortable nylon fabric after drying.
Antimicrobial fluid described in step (3), counts by weight, and its raw material includes: gold 30 parts of clock rattan, Herba Portulacae 12 parts, Zhu
Cornel 20 parts, Folium Musae 15 parts and Radix et Caulis Opuntiae Dillenii 10 parts.
Embodiment 3
A kind of antibacterial comfortable nylon fabric, counts by weight, and its raw material includes:
Slices of caprone: 105 parts；
Antibacterial nylon agglomerate: 6.5 parts；
Polyvinylpyrrolidone: 4 parts；
Antioxidant SEED:0.8 part；
Fatty alcohol-polyoxyethylene ether: 0.8 part.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps:
(1) preparation of silver Maifanitum antibacterial is carried: after taking Maifanitum 200 mesh sieves excessively after crushed, after cleaning twice with distilled water
It is dried to obtain medical stone powder, standby；The AgNO of preparation 0.008mol/L3Solution, joins prepared AgNO by medical stone powder3Molten
In liquid, after stirring 2h, mixed liquor, to 7.0, is carried out sucking filtration by regulation pH value of solution subsequently, and sucking filtration gained filter cake distilled water flushing is straight
Without Ag to washing liquid+；Pulverize after the filtration cakes torrefaction of gained, prepare and carry silver Maifanitum antibacterial；Described load silver wheat meal
In stone antibacterial, by mass percentage, Maifanitum accounts for 97%, AgNO3Account for 3%；
(2) preparation of antibacterial nylon agglomerate: in mixer, takes the load silver Maifanitum antibacterial that 12 weight portion steps (1) prepare
After carrying out surface Anti-tarnishing process, add the silane coupler mix homogeneously of 1.5 weight portions, obtain antimicrobial mix；By institute
Melt extrude in double screw extruder after obtaining the slices of caprone mixing of antimicrobial mix and 70 weight portions, prepare antibacterial mother
Grain.
The preparation method of the most antibacterial comfortable nylon fabric, specifically includes following steps:
(1) use melted after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent being mixed
Spin processes carries out spinning；
(2) nylon fibre step (1) obtained prepares nylon fibre yarn through textile technology, and gained nylon fibre spins
Line prepares nylon fabric through dyeing and finishing technology again；
(3) being impregnated in antimicrobial fluid 30 minutes by the nylon fabric that step (2) obtains, bath raio is 1:25；
(4) nylon fabric after step (3) being impregnated prepares described antibacterial comfortable nylon fabric after drying.
Antimicrobial fluid described in step (3), counts by weight, and its raw material includes: gold 28 parts of clock rattan, Herba Portulacae 11 parts, Zhu
Cornel 18 parts, Folium Musae 12 parts and Radix et Caulis Opuntiae Dillenii 9 parts.
The preparation method of the antimicrobial fluid described in embodiment 1-3, specifically includes following steps:
(A) Radix et Caulis Opuntiae Dillenii cleaned and go the laggard row of the removal of impurity to squeeze to obtain Radix et Caulis Opuntiae Dillenii juice and Radix et Caulis Opuntiae Dillenii slag, toward gained Radix et Caulis Opuntiae Dillenii slag
In add the water of 4 times of weight, extract 2 hours at 60 DEG C, filter to obtain Radix et Caulis Opuntiae Dillenii slag extracting solution, by gained Radix et Caulis Opuntiae Dillenii juice and celestial being
Palm slag extracting solution mixes to obtain cactus extraction；
(B) depletion clock rattan, Herba Portulacae, the Fructus Evodiae and the Folium Musae boiling water of 8 times of weight decocts twice, each 1.5 hours, filters also
And merge twice filtrate, by gained filtrate reconcentration be relative density be the concentrated solution of 1.1；Add in the concentrated solution obtained
The ethanol of the 95wt% of 5 times of weight, carries out reflux, extract, 2 times, each 1.5 hours, reclaims ethanol, obtains mixed liquor；
(C) desolventing technology is carried out after being mixed by mixed liquor prepared with step (B) for cactus extraction prepared for step (A), system
Obtain antimicrobial fluid.
Anti-microbial property is tested
According to AATCC100-2004 " performance evaluation of textile material antibiotic finish " standard testing, the inventive method is used to produce
Antibacterial comfortable nylon fabric after, antibiotic rate >=99.9%, its result is listed in table 1.
Table 1 anti-bacteria test result
The foregoing is only presently preferred embodiments of the present invention, all equalizations done according to scope of the present invention patent change and repair
Decorations, all should belong to the covering scope of the present invention.
Claims (4)
1. an antibacterial comfortable nylon fabric, it is characterised in that: count by weight, the raw material bag of described nylon fabric
Include:
Slices of caprone: 100 ~ 110 parts；
Antibacterial nylon agglomerate: 5 ~ 8 parts；
Moisture-absorption modifier: 3 ~ 5 parts；
Antioxidant SEED:0.5 ~ 1 part；
Antistatic agent: 0.5 ~ 1 part；
Described moisture-absorption modifier is polyvinylpyrrolidone；Described antistatic agent is fatty alcohol-polyoxyethylene ether.
Antibacterial comfortable nylon fabric the most according to claim 1, it is characterised in that: the system of described antibacterial nylon agglomerate
Preparation Method, specifically includes following steps:
(1) preparation of silver Maifanitum antibacterial is carried: after taking Maifanitum 200 mesh sieves excessively after crushed, after cleaning twice with distilled water
It is dried to obtain medical stone powder, standby；The AgNO of preparation 0.008mol/L3Solution, joins prepared AgNO by medical stone powder3Molten
In liquid, after stirring 2h, mixed liquor, to 7.0, is carried out sucking filtration by regulation pH value of solution subsequently, and sucking filtration gained filter cake distilled water flushing is straight
Without Ag to washing liquid+；Pulverize after the filtration cakes torrefaction of gained, prepare and carry silver Maifanitum antibacterial；Described load silver wheat meal
In stone antibacterial, by mass percentage, Maifanitum accounts for 96 ~ 98%, AgNO3Account for 2 ~ 4%；
(2) preparation of antibacterial nylon agglomerate: in mixer, the load silver Maifanitum taking 10 ~ 15 weight portion steps (1) prepared is antibacterial
After agent carries out surface Anti-tarnishing process, add the silane coupler mix homogeneously of 0.5 ~ 2 weight portion, obtain antimicrobial mix；
Melt extrude in double screw extruder after the slices of caprone of gained antimicrobial mix and 60 ~ 80 weight portions is mixed, prepare
Antibacterial matrices.
3. the method preparing the most antibacterial comfortable nylon fabric, it is characterised in that: specifically include with
Lower step:
(1) use melted after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent being mixed
Spin processes carries out spinning；
(2) nylon fibre step (1) obtained prepares nylon fibre yarn through textile technology, and gained nylon fibre spins
Line prepares nylon fabric through dyeing and finishing technology again；
(3) being impregnated in antimicrobial fluid 30 minutes by the nylon fabric that step (2) obtains, bath raio is 1:25；
(4) nylon fabric after step (3) being impregnated prepares described antibacterial comfortable nylon fabric after drying.
The preparation method of antibacterial comfortable nylon fabric the most according to claim 3, it is characterised in that: step (3) is described
Antimicrobial fluid, count by weight, its raw material includes: gold 25 ~ 30 parts of clock rattan, Herba Portulacae 10 ~ 12 parts, the Fructus Evodiae 15 ~ 20 parts, Musa basjoo Sieb. Et Zucc.
10 ~ 15 parts of leaf and Radix et Caulis Opuntiae Dillenii 8 ~ 10 parts；The preparation method of described antimicrobial fluid is: Radix et Caulis Opuntiae Dillenii is cleaned and goes the removal of impurity laggard by (A)
Row squeezes to obtain Radix et Caulis Opuntiae Dillenii juice and Radix et Caulis Opuntiae Dillenii slag, adds the water of 4 times of weight in gained Radix et Caulis Opuntiae Dillenii slag, extracts 2 hours at 60 DEG C,
Filter to obtain Radix et Caulis Opuntiae Dillenii slag extracting solution, gained Radix et Caulis Opuntiae Dillenii juice and Radix et Caulis Opuntiae Dillenii slag extracting solution are mixed to obtain cactus extraction；
(B) depletion clock rattan, Herba Portulacae, the Fructus Evodiae and the Folium Musae boiling water of 8 times of weight decocts twice, each 1.5 hours, filters also
And merge twice filtrate, by gained filtrate reconcentration be relative density be the concentrated solution of 1.1；Add in the concentrated solution obtained
The ethanol of the 95wt% of 5 times of weight, carries out reflux, extract, 2 times, each 1.5 hours, reclaims ethanol, obtains mixed liquor；
(C) desolventing technology is carried out after being mixed by mixed liquor prepared with step (B) for cactus extraction prepared for step (A), system
Obtain antimicrobial fluid.
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| CN201610641262.5A CN106283336B (en) | 2016-08-08 | 2016-08-08 | A kind of comfortable nylon fabric of antibacterial and preparation method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106939465A (en) * | 2017-04-10 | 2017-07-11 | 太仓绒彩纺织品有限公司 | A kind of weaving face fabric for baby |
| CN106948063A (en) * | 2017-04-10 | 2017-07-14 | 太仓绒彩纺织品有限公司 | A kind of antibacterial weaving face fabric for baby |
| CN107190358A (en) * | 2017-06-30 | 2017-09-22 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial anti-radiation garment fabric |
| CN108385227A (en) * | 2018-01-30 | 2018-08-10 | 平湖市伊凡家箱包有限公司 | A kind of half spinning carpet yarn of antibacterial and preparation method thereof |
| CN108517578A (en) * | 2018-04-20 | 2018-09-11 | 刘凡领 | A kind of preparation method of modified medical stone base nylon fibre |
| CN108978198A (en) * | 2018-07-23 | 2018-12-11 | 含山县海达服饰有限公司 | A kind of polyester fiber fabric treatment fluid |
| CN108978199A (en) * | 2018-07-23 | 2018-12-11 | 含山县海达服饰有限公司 | A kind of polyester fiber fabric with anti-microbial property |
| CN109505024A (en) * | 2018-11-26 | 2019-03-22 | 福建凤竹纺织科技股份有限公司 | A kind of antibacterial ultraviolet-resistannanofiber line fabric and preparation method thereof |
| CN112853570A (en) * | 2020-12-31 | 2021-05-28 | 嘉兴市昊鸣纺织股份有限公司 | Metallic yarn composite fabric and preparation method thereof |
| CN113417027A (en) * | 2021-08-03 | 2021-09-21 | 海阳科技股份有限公司 | Preparation process of non-dyed nylon fiber |
| CN114318733A (en) * | 2021-12-01 | 2022-04-12 | 福州市晟浩纺织科技有限公司 | Preparation method of antibacterial polyamide fabric |
| CN117604703A (en) * | 2023-12-18 | 2024-02-27 | 汕头市英华织造实业有限公司 | Weaving method of blended fabric |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106939465A (en) * | 2017-04-10 | 2017-07-11 | 太仓绒彩纺织品有限公司 | A kind of weaving face fabric for baby |
| CN106948063A (en) * | 2017-04-10 | 2017-07-14 | 太仓绒彩纺织品有限公司 | A kind of antibacterial weaving face fabric for baby |
| CN107190358A (en) * | 2017-06-30 | 2017-09-22 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial anti-radiation garment fabric |
| CN108385227A (en) * | 2018-01-30 | 2018-08-10 | 平湖市伊凡家箱包有限公司 | A kind of half spinning carpet yarn of antibacterial and preparation method thereof |
| CN108517578A (en) * | 2018-04-20 | 2018-09-11 | 刘凡领 | A kind of preparation method of modified medical stone base nylon fibre |
| CN108978199A (en) * | 2018-07-23 | 2018-12-11 | 含山县海达服饰有限公司 | A kind of polyester fiber fabric with anti-microbial property |
| CN108978198A (en) * | 2018-07-23 | 2018-12-11 | 含山县海达服饰有限公司 | A kind of polyester fiber fabric treatment fluid |
| CN109505024A (en) * | 2018-11-26 | 2019-03-22 | 福建凤竹纺织科技股份有限公司 | A kind of antibacterial ultraviolet-resistannanofiber line fabric and preparation method thereof |
| CN109505024B (en) * | 2018-11-26 | 2021-02-23 | 福建凤竹纺织科技股份有限公司 | Antibacterial ultraviolet-proof fabric and preparation method thereof |
| CN112853570A (en) * | 2020-12-31 | 2021-05-28 | 嘉兴市昊鸣纺织股份有限公司 | Metallic yarn composite fabric and preparation method thereof |
| CN112853570B (en) * | 2020-12-31 | 2021-12-31 | 嘉兴市昊鸣纺织股份有限公司 | Metallic yarn composite fabric and preparation method thereof |
| CN113417027A (en) * | 2021-08-03 | 2021-09-21 | 海阳科技股份有限公司 | Preparation process of non-dyed nylon fiber |
| CN114318733A (en) * | 2021-12-01 | 2022-04-12 | 福州市晟浩纺织科技有限公司 | Preparation method of antibacterial polyamide fabric |
| CN114318733B (en) * | 2021-12-01 | 2023-08-22 | 福州市晟浩纺织科技有限公司 | Preparation method of antibacterial nylon fabric |
| CN117604703A (en) * | 2023-12-18 | 2024-02-27 | 汕头市英华织造实业有限公司 | Weaving method of blended fabric |
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