CN106283336B - A kind of comfortable nylon fabric of antibacterial and preparation method thereof - Google Patents
A kind of comfortable nylon fabric of antibacterial and preparation method thereof Download PDFInfo
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- CN106283336B CN106283336B CN201610641262.5A CN201610641262A CN106283336B CN 106283336 B CN106283336 B CN 106283336B CN 201610641262 A CN201610641262 A CN 201610641262A CN 106283336 B CN106283336 B CN 106283336B
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
- D03D15/54—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads coloured
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
- D01F6/60—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyamides
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/10—Patterned fabrics or articles
- D04B1/12—Patterned fabrics or articles characterised by thread material
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B21/00—Warp knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B21/06—Patterned fabrics or articles
- D04B21/08—Patterned fabrics or articles characterised by thread material
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/16—Physical properties antistatic; conductive
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses comfortable nylon fabric of a kind of antibacterial and preparation method thereof, count in parts by weight, the raw material of described nylon fabric includes：0.5 ~ 1 part of 100 ~ 110 parts of slices of caprone, 5 ~ 8 parts of antibacterial nylon agglomerate, 3 ~ 5 parts of moisture-absorption modifier, 0.5 ~ 1 part of antioxidant SEED and antistatic agent.Added in nylon fabric produced by the present invention and carry silver-colored medical stone antiseptic, then impregnated in antimicrobial fluid, had the antibacterial action of the antimicrobial component in inorganic antiseptic and natural Chinese medicinal herb, bidirectional modulation concurrently, very strong bactericidal effect is served, more than 99% is up to the clearance of various bacteriums.In addition, nylon fabric produced by the present invention has good hygroscopicity, water imbibition and antistatic property, there is very high practical value, and preparation technology is simple, is suitable for promoting the use of.
Description
Technical field
The invention belongs to textile technology field, and in particular to comfortable nylon fabric of a kind of antibacterial and preparation method thereof.
Background technology
Nylon fibre is to realize industrialized synthetic fibers earliest in the world, has intensity is high, elasticity is good, wearability is good etc.
Feature, turn into one of most popular fiber of twentieth century.But with the economic development and improvement of people's living standards, people couple
Comfortably, health, the pursuit of dress ornament of health and the demand of other special dimensions, conventional polyamide fibre product can not meet.
And conventional nylon fibre is also easy to produce electrostatic, and make fabric face dust suction more because of Electrostatic Absorption, plus the sweat of human body discharge
Liquid, easily bacterial growth, therefore it is of great practical value to develop the comfortable nylon fabric with anti-bacterial anti-foul function.
The content of the invention
It is an object of the invention in view of the shortcomings of the prior art, providing comfortable nylon fabric and its preparation side of a kind of antibacterial
Method.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of comfortable nylon fabric of antibacterial, is counted in parts by weight, and its raw material includes：
Slices of caprone：100 ~ 110 parts；
Antibacterial nylon agglomerate：5 ~ 8 parts；
Moisture-absorption modifier：3 ~ 5 parts；
Antioxidant SEED：0.5 ~ 1 part；
Antistatic agent：0.5 ~ 1 part；
Described moisture-absorption modifier is polyvinylpyrrolidone；Described antistatic agent is AEO.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps：
（1）Carry the preparation of silver-colored medical stone antiseptic：After taking medical stone to cross 200 mesh sieves after crushed, two are cleaned with distilled water
Dry medical stone powder, standby after secondary；Prepare 0.008mol/L AgNO3Solution, medical stone powder is added to what is prepared
AgNO3In solution, after stirring 2h, regulation pH value of solution to 7.0, then mixed liquor is filtered, filter gained filter cake distillation
Water is rinsed until being free of Ag in washing lotion+；It will be pulverized after the filtration cakes torrefaction of gained, be made and carry silver-colored medical stone antiseptic；It is described
Carry in silver-colored medical stone antiseptic, by mass percentage, medical stone accounts for 96 ~ 98%, AgNO3Account for 2 ~ 4%；
（2）The preparation of antibacterial nylon agglomerate：In mixer, 10 ~ 15 parts by weight steps are taken（1）It is obtained to carry silver-colored medical stone
After antiseptic carries out surface Anti- tarnishing processing, the silane coupler for adding 0.5 ~ 2 parts by weight is well mixed, and obtains antiseptic mixing
Thing；The melting extrusion in double screw extruder after gained antimicrobial mix is mixed with the slices of caprone of 60 ~ 80 parts by weight, system
Obtain antibacterial matrices.
The preparation method of the comfortable nylon fabric of antibacterial as described above, specifically includes following steps：
（1）Used after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent are mixed
Melt spinning method carries out spinning；
（2）By step（1）Nylon fibre yarn, gained nylon fibre is made by textile technology in obtained nylon fibre
Nylon fabric is made through dyeing and finishing technology again in yarn；
（3）By step（2）Obtained nylon fabric impregnates 30 minutes in antimicrobial fluid, bath raio 1:25；
（4）By step（3）The comfortable nylon fabric of the antibacterial is made after nylon fabric drying after dipping.
Step（3）Described antimicrobial fluid, is counted in parts by weight, and its raw material includes：Golden 25 ~ 30 parts of clock rattan, purslane 10 ~ 12
8 ~ 10 parts of part, 15 ~ 20 parts of the fruit of medicinal cornel, 10 ~ 15 parts of leaf of Japanese banana and cactus；The preparation method of the antimicrobial fluid is：
（A）Cactus is cleaned and goes after the removal of impurity to carry out squeezing to obtain cactus juice and cactus slag, toward gained celestial being
Slap slag in plus 4 times of weight water, extract 2 hours at 60 DEG C, filters to obtain cactus slag extract solution, by gained cactus juice with
Cactus slag extract solution mixes to obtain cactus extraction；
（B）Jin Zhongteng, purslane, the fruit of medicinal cornel and leaf of Japanese banana is taken to be decocted twice with the boiling water of 8 times of weight, 1.5 hours every time, mistake
Filter and merge filtrate twice, gained filtrate is concentrated to the concentrate for being 1.1 for relative density again；Into obtained concentrate again
The 95wt% of 5 times of weight ethanol is added, carries out refluxing extraction 2 times, 1.5 hours every time, ethanol is reclaimed, obtains mixed liquor；
（C）By step（A）Obtained cactus extraction and step（B）Carried out after obtained mixed liquor mixing at decolouring
Reason, antimicrobial fluid is made.
The beneficial effects of the present invention are：
（1）Nylon fabric antibacterial effect produced by the present invention is notable, is added in its antibacterial matrices and carries silver-colored medical stone antibacterial
Agent, using the characteristic of medical stone high-specific surface area, as the carrier of antiseptic, silver ion on the one hand can be adsorbed well；
On the other hand, due to the pole Porous state and abundant-Si-O atomic groups of medical stone, itself bacterium can just be played good
Good suction-operated；In addition, the present invention adds in the feed before this carries silver-colored medical stone antiseptic, then soaked in antimicrobial fluid
Stain, the antibacterial action of the antimicrobial component in inorganic antiseptic and natural Chinese medicinal herb is had concurrently, bidirectional modulation, has served very strong kill
Bacterium effect, more than 99% is up to the clearance of various bacteriums；
（2）Nylon fabric produced by the present invention has good hygroscopicity, water imbibition and antistatic property, has very high
Practical value, and preparation technology is simple, is suitable for promoting the use of.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described, but the present invention is not limited only to these embodiments.
Embodiment 1
A kind of comfortable nylon fabric of antibacterial, is counted in parts by weight, and its raw material includes：
Slices of caprone：100 parts；
Antibacterial nylon agglomerate：5 parts；
Polyvinylpyrrolidone：3 parts；
Antioxidant SEED：0.5 part；
AEO：0.5 part.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps：
（1）Carry the preparation of silver-colored medical stone antiseptic：After taking medical stone to cross 200 mesh sieves after crushed, two are cleaned with distilled water
Dry medical stone powder, standby after secondary；Prepare 0.008mol/L AgNO3Solution, medical stone powder is added to what is prepared
AgNO3In solution, after stirring 2h, regulation pH value of solution to 7.0, then mixed liquor is filtered, filter gained filter cake distillation
Water is rinsed until being free of Ag in washing lotion+；It will be pulverized after the filtration cakes torrefaction of gained, be made and carry silver-colored medical stone antiseptic；It is described
Carry in silver-colored medical stone antiseptic, by mass percentage, medical stone accounts for 96%, AgNO3Account for 4%；
（2）The preparation of antibacterial nylon agglomerate：In mixer, 10 parts by weight steps are taken（1）The obtained silver-colored medical stone of load resists
After microbial inoculum carries out surface Anti- tarnishing processing, the silane coupler for adding 0.5 parts by weight is well mixed, and obtains antimicrobial mix；
The melting extrusion in double screw extruder after gained antimicrobial mix is mixed with the slices of caprone of 60 parts by weight, antibacterial is made
Master batch.
The preparation method of the comfortable nylon fabric of antibacterial as described above, specifically includes following steps：
（1）Used after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent are mixed
Melt spinning method carries out spinning；
（2）By step（1）Nylon fibre yarn, gained nylon fibre is made by textile technology in obtained nylon fibre
Nylon fabric is made through dyeing and finishing technology again in yarn；
（3）By step（2）Obtained nylon fabric impregnates 30 minutes in antimicrobial fluid, bath raio 1:25；
（4）By step（3）The comfortable nylon fabric of the antibacterial is made after nylon fabric drying after dipping.
Step（3）Described antimicrobial fluid, is counted in parts by weight, and its raw material includes：Golden 25 parts of clock rattan, 10 parts of purslane, Zhu
8 parts of 15 parts of cornel, 10 parts of leaf of Japanese banana and cactus.
Embodiment 2
A kind of comfortable nylon fabric of antibacterial, is counted in parts by weight, and its raw material includes：
Slices of caprone：110 parts；
Antibacterial nylon agglomerate：8 parts；
Polyvinylpyrrolidone：5 parts；
Antioxidant SEED：1 part；
AEO：1 part.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps：
（1）Carry the preparation of silver-colored medical stone antiseptic：After taking medical stone to cross 200 mesh sieves after crushed, two are cleaned with distilled water
Dry medical stone powder, standby after secondary；Prepare 0.008mol/L AgNO3Solution, medical stone powder is added to what is prepared
AgNO3In solution, after stirring 2h, regulation pH value of solution to 7.0, then mixed liquor is filtered, filter gained filter cake distillation
Water is rinsed until being free of Ag in washing lotion+；It will be pulverized after the filtration cakes torrefaction of gained, be made and carry silver-colored medical stone antiseptic；It is described
Carry in silver-colored medical stone antiseptic, by mass percentage, medical stone accounts for 98%, AgNO3Account for 2%；
（2）The preparation of antibacterial nylon agglomerate：In mixer, 15 parts by weight steps are taken（1）The obtained silver-colored medical stone of load resists
After microbial inoculum carries out surface Anti- tarnishing processing, the silane coupler for adding 2 parts by weight is well mixed, and obtains antimicrobial mix；Will
The melting extrusion in double screw extruder after gained antimicrobial mix mixes with the slices of caprone of 80 parts by weight, it is female that antibacterial is made
Grain.
The preparation method of the comfortable nylon fabric of antibacterial as described above, specifically includes following steps：
（1）Used after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent are mixed
Melt spinning method carries out spinning；
（2）By step（1）Nylon fibre yarn, gained nylon fibre is made by textile technology in obtained nylon fibre
Nylon fabric is made through dyeing and finishing technology again in yarn；
（3）By step（2）Obtained nylon fabric impregnates 30 minutes in antimicrobial fluid, bath raio 1:25；
（4）By step（3）The comfortable nylon fabric of the antibacterial is made after nylon fabric drying after dipping.
Step（3）Described antimicrobial fluid, is counted in parts by weight, and its raw material includes：Golden 30 parts of clock rattan, 12 parts of purslane, Zhu
10 parts of 20 parts of cornel, 15 parts of leaf of Japanese banana and cactus.
Embodiment 3
A kind of comfortable nylon fabric of antibacterial, is counted in parts by weight, and its raw material includes：
Slices of caprone：105 parts；
Antibacterial nylon agglomerate：6.5 part；
Polyvinylpyrrolidone：4 parts；
Antioxidant SEED：0.8 part；
AEO：0.8 part.
The preparation method of described antibacterial nylon agglomerate, specifically includes following steps：
（1）Carry the preparation of silver-colored medical stone antiseptic：After taking medical stone to cross 200 mesh sieves after crushed, two are cleaned with distilled water
Dry medical stone powder, standby after secondary；Prepare 0.008mol/L AgNO3Solution, medical stone powder is added to what is prepared
AgNO3In solution, after stirring 2h, regulation pH value of solution to 7.0, then mixed liquor is filtered, filter gained filter cake distillation
Water is rinsed until being free of Ag in washing lotion+；It will be pulverized after the filtration cakes torrefaction of gained, be made and carry silver-colored medical stone antiseptic；It is described
Carry in silver-colored medical stone antiseptic, by mass percentage, medical stone accounts for 97%, AgNO3Account for 3%；
（2）The preparation of antibacterial nylon agglomerate：In mixer, 12 parts by weight steps are taken（1）The obtained silver-colored medical stone of load resists
After microbial inoculum carries out surface Anti- tarnishing processing, the silane coupler for adding 1.5 parts by weight is well mixed, and obtains antimicrobial mix；
The melting extrusion in double screw extruder after gained antimicrobial mix is mixed with the slices of caprone of 70 parts by weight, antibacterial is made
Master batch.
The preparation method of the comfortable nylon fabric of antibacterial as described above, specifically includes following steps：
（1）Used after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent are mixed
Melt spinning method carries out spinning；
（2）By step（1）Nylon fibre yarn, gained nylon fibre is made by textile technology in obtained nylon fibre
Nylon fabric is made through dyeing and finishing technology again in yarn；
（3）By step（2）Obtained nylon fabric impregnates 30 minutes in antimicrobial fluid, bath raio 1:25；
（4）By step（3）The comfortable nylon fabric of the antibacterial is made after nylon fabric drying after dipping.
Step（3）Described antimicrobial fluid, is counted in parts by weight, and its raw material includes：Golden 28 parts of clock rattan, 11 parts of purslane, Zhu
9 parts of 18 parts of cornel, 12 parts of leaf of Japanese banana and cactus.
The preparation method of antimicrobial fluid described in embodiment 1-3, specifically includes following steps：
（A）Cactus is cleaned and goes after the removal of impurity to carry out squeezing to obtain cactus juice and cactus slag, toward gained celestial being
Slap slag in plus 4 times of weight water, extract 2 hours at 60 DEG C, filters to obtain cactus slag extract solution, by gained cactus juice with
Cactus slag extract solution mixes to obtain cactus extraction；
（B）Jin Zhongteng, purslane, the fruit of medicinal cornel and leaf of Japanese banana is taken to be decocted twice with the boiling water of 8 times of weight, 1.5 hours every time, mistake
Filter and merge filtrate twice, gained filtrate is concentrated to the concentrate for being 1.1 for relative density again；Into obtained concentrate again
The 95wt% of 5 times of weight ethanol is added, carries out refluxing extraction 2 times, 1.5 hours every time, ethanol is reclaimed, obtains mixed liquor；
（C）By step（A）Obtained cactus extraction and step（B）Carried out after obtained mixed liquor mixing at decolouring
Reason, antimicrobial fluid is made.
Anti-microbial property test
According to AATCC100-2004《The performance evaluation of textile material antibiotic finish》Standard testing, using the inventive method
After the comfortable nylon fabric of the antibacterial of production, antibiotic rate >=99.9%, its result is listed in table 1.
The anti-bacteria test result of table 1
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, it should all belong to the covering scope of the present invention.
Claims (1)
- A kind of 1. comfortable nylon fabric of antibacterial, it is characterised in that：Count in parts by weight, the raw material bag of described nylon fabric Include：Slices of caprone：100 ~ 110 parts；Antibacterial nylon agglomerate：5 ~ 8 parts；Moisture-absorption modifier：3 ~ 5 parts；Antioxidant SEED：0.5 ~ 1 part；Antistatic agent：0.5 ~ 1 part；Described moisture-absorption modifier is polyvinylpyrrolidone；Described antistatic agent is AEO；Described The preparation method of antibacterial nylon agglomerate, specifically includes following steps：（1）Carry the preparation of silver-colored medical stone antiseptic：After taking medical stone to cross 200 mesh sieves after crushed, after being cleaned twice with distilled water Dry medical stone powder, it is standby；Prepare 0.008mol/L AgNO3Solution, medical stone powder is added to prepared AgNO3It is molten In liquid, after stirring 2h, regulation pH value of solution to 7.0, then mixed liquor is filtered, it is straight to filter gained filter cake distilled water flushing Ag is free of into washing lotion+；It will be pulverized after the filtration cakes torrefaction of gained, be made and carry silver-colored medical stone antiseptic；It is described to carry silver-colored wheat meal In stone antiseptic, by mass percentage, medical stone accounts for 96 ~ 98%, AgNO3Account for 2 ~ 4%；（2）The preparation of antibacterial nylon agglomerate：In mixer, 10 ~ 15 parts by weight steps are taken（1）It is obtained to carry silver-colored medical stone antibacterial After agent carries out surface Anti- tarnishing processing, the silane coupler for adding 0.5 ~ 2 parts by weight is well mixed, and obtains antimicrobial mix； The melting extrusion in double screw extruder after gained antimicrobial mix is mixed with the slices of caprone of 60 ~ 80 parts by weight, it is made Antibacterial matrices；The preparation method of the comfortable nylon fabric of described antibacterial, specifically includes following steps：（I）Using melting after slices of caprone, antibacterial nylon agglomerate, moisture-absorption modifier, antioxidant SEED and antistatic agent are mixed Spin processes carry out spinning；（II）By step（I）Nylon fibre yarn is made by textile technology in obtained nylon fibre, and gained nylon fibre is spun Nylon fabric is made through dyeing and finishing technology again in yarn；（III）By step（II）Obtained nylon fabric impregnates 30 minutes in antimicrobial fluid, bath raio 1:25；（IV）By step（III）The comfortable nylon fabric of the antibacterial is made after nylon fabric drying after dipping；Step（III）Described antimicrobial fluid, is counted in parts by weight, and its raw material includes：Golden 25 ~ 30 parts of clock rattan, purslane 10 ~ 12 8 ~ 10 parts of part, 15 ~ 20 parts of the fruit of medicinal cornel, 10 ~ 15 parts of leaf of Japanese banana and cactus；The preparation method of the antimicrobial fluid is：（A）By celestial being The palm is cleaned and carries out squeezing to obtain cactus juice and cactus slag after going the removal of impurity, and 4 times of weight is added into gained cactus slag Water, extracted 2 hours at 60 DEG C, filter to obtain cactus slag extract solution, gained cactus juice and cactus slag extract solution are mixed Close to obtain cactus extraction；（B）Jin Zhongteng, purslane, the fruit of medicinal cornel and leaf of Japanese banana is taken to be decocted twice with the boiling water of 8 times of weight, 1.5 hours every time, filtering was simultaneously And merge filtrate twice, gained filtrate is concentrated to the concentrate for being 1.1 for relative density again；Added into obtained concentrate The 95wt% of 5 times of weight ethanol, carries out refluxing extraction 2 times, 1.5 hours every time, reclaims ethanol, obtains mixed liquor；（C）By step（A）Obtained cactus extraction and step（B）Decolorization is carried out after obtained mixed liquor mixing, is made Obtain antimicrobial fluid.
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