CN105603765A - Method for preparing rose essential oil microcapsule finishing agent and application thereof - Google Patents
Method for preparing rose essential oil microcapsule finishing agent and application thereof Download PDFInfo
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- CN105603765A CN105603765A CN201610101764.9A CN201610101764A CN105603765A CN 105603765 A CN105603765 A CN 105603765A CN 201610101764 A CN201610101764 A CN 201610101764A CN 105603765 A CN105603765 A CN 105603765A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a method for preparing a rose essential oil microcapsule finishing agent and application thereof and belongs to the technical field of pure cotton fabric finishing. The preparation method comprises a first step of preparing a rose essential oil microcapsule and a second step of preparing the rose essential oil microcapsule finishing agent. The invention also discloses the application of the rose essential oil microcapsule finishing agent to a finishing process of a pure cotton fabric. The method is simple to operate, the surface of the microcapsule is continuous, the capsule wall has semipermeability, rose essential oil can be slowly released through the capsule wall, and main raw materials are extracted from plants and are natural and green. The finished pure cotton fabric can adjust female endocrine and nourish the uterus when applied to women's underwear. The microcapsule prepared through the method can adhere to the pure cotton fabric well, serve a lasting health care effect and have important marketing potential.
Description
Technical field:
The present invention relates to a kind of rear finishing technique field of pure cotton fabric, relate to the system of rose essential-oil microcapsule dressing liquidPreparation Method and the application on pure cotton fabric thereof.
Background technology:
Develop rapidly along with modern society is high-tech, the raising of people's living standard, people also more and more start to pay attention toQuality of the life, traditional bafta function singleness, can not meet the needs of people to healthy living pursuit. CauseThis multifunctional fabric is the direction of present field of textiles research.
And along with the development of microcapsules technology, using microcapsules as finishing agent, be applied in field of textiles, will make weavingThe functional of product gets more and more. Microcapsules are applied to has become in the rear arrangement of textile that to give product polyfunctionalOne of important channel.
Beijing Lusan Chemical Co., Ltd. adopts beta-cyclodextrin inclusion compound Rosa Damascana to prepare microcapsule essence, is applied toIn washing powder, can obviously improve the aroma retaining effect of fabric. But the microcapsule dressing agent bonding that adopts beta-schardinger dextrin-to prepareFabric, washable weak effect, can not give fabric functional for a long time. Pulullan polysaccharide is that one is sent out by Aureobasidium pullulansThe similar glucan that ferment produces, the outer water-soluble cement polysaccharide of the born of the same parents of xanthans, its film forming, plasticity, caking propertyAll stronger, and there is good characteristic nontoxic, colorless and odorless.
If utilize pulullan polysaccharide to substitute beta-schardinger dextrin-as wall material, can make and be applicable to pure cotton fabric arranges, energySlowly discharge the finishing agent of content, can make microcapsules further obtain in the technology application in fabric post-treatment field simultaneouslyPromote.
Summary of the invention:
The present invention aims to provide a kind of rose essential-oil microcapsule finishing agent, and its primary raw material adopts plant extract, natural greenLook; Pure cotton fabric after arrangement is applied on women underwear can regulate female incretion and nourishing uterus, adopts weThe microcapsules that method makes can well bond on pure cotton fabric, bring into play lasting health-care effect.
Preparation method's simple possible of rose essential-oil microcapsule finishing agent, rose essential-oil microcapsule prepared by this method arrangesAgent, adopts pulullan polysaccharide as wall material, can make microcapsules well be bonded on bafta, and can control lastinglyThe slow release of Rosa Damascana.
The invention provides following technical scheme:
A preparation method for rose essential-oil microcapsule finishing agent, comprises the following steps:
The first step: prepare rose essential-oil microcapsule:
By 10-20g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely preparationPulullan polysaccharide solution;
Take out 100ml-300ml pulullan polysaccharide solution, add 10-30g Rosa Damascana, at temperature 30-50 DEG C, stirMix 1-3h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
25-35g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 2-4g, microcapsules are disperseed uniformlyIn dressing liquid, mix and obtain composite essential oil microcapsule dressing agent.
Preferably, the first step is prepared in rose essential-oil microcapsule 10-15g pulullan polysaccharide, adds 1000ml distillationIn water, in 30 DEG C of water-baths, dissolve completely, prepare pulullan polysaccharide solution.
Preferably, the first step is prepared in rose essential-oil microcapsule and is taken out 100ml-200ml pulullan polysaccharide solution, adds20-30g Rosa Damascana stirs.
Preferably, the first step is prepared in rose essential-oil microcapsule and is added after Rosa Damascana, at 30-40 DEG C, stirs 2-3h.
Preferably, second step is prepared in rose essential-oil microcapsule finishing agent 30-35g microcapsules is dissolved in 1L purified water,Add pulullan polysaccharide 3-4g, microcapsules are dispersed in dressing liquid uniformly, mix and obtain the micro-glue of composite essential oilCapsule finishing agent.
The application of above-mentioned rose essential-oil microcapsule finishing agent is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 50-70 DEG C, make cotton textiles and knitThing.
Preferably, microcapsule dressing agent solution is sprayed on bafta with watering can, makes rose essential-oil microcapsule finishing agent pairPure cotton fabric evenly soaks, and dries at 60-70 DEG C, makes bafta.
Beneficial effect of the present invention:
1. the present invention has expanded the application of Rosa Damascana, is adjusting female incretion and the nourishing uterus of Rosa DamascanaEffect be well applied in the finishing agent of bafta.
2. preparation method's operation is simple, and materials kind is few, has higher market popularization value.
3. preparation method's Rosa Damascana of the present invention can not only be brought into play the effect that regulates female incretion and nourish uterus, can alsoBring into play to a certain extent antibacterial effect.
4. the present invention adopts pulullan polysaccharide as wall material, can make full use of the characteristic of the good overlay film of pulullan polysaccharide,Form the water white tough film of one deck on Rosa Damascana surface, rose essential-oil microcapsule can slowly be discharged, lastingPlay a role.
5. the present invention adds pulullan polysaccharide in making finishing agent, can form layer of transparent film, makes Rosa Damascana micro-Capsule is well bonded on bafta, and is difficult for being washed and comes off.
Detailed description of the invention:
Be described in detail of the present invention below in conjunction with embodiment, the present embodiment is under taking invention technical scheme as prerequisiteImplement, provided detailed embodiment and concrete operating process, but protection scope of the present invention is not limited toFollowing embodiment. The experimental program of unreceipted actual conditions in embodiment, conventionally according to normal condition or manufacturerThe condition of advising is implemented.
Embodiment mono-
The first step: prepare rose essential-oil microcapsule:
By 10g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 100mlml pulullan polysaccharide solution, add 10g Rosa Damascana, at 30 DEG C of temperature, stir 1h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
25g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 2g, make microcapsules be dispersed in uniformly arrangementIn liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 50 DEG C, make pure cotton fabric.
Embodiment bis-
The first step: prepare rose essential-oil microcapsule:
By 20g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 300ml pulullan polysaccharide solution, add 30g Rosa Damascana, under temperature 50 C, stir 3h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
35g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 4g, make microcapsules be dispersed in uniformly arrangementIn liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 70 DEG C, make pure cotton fabric.
Embodiment tri-
The first step: prepare rose essential-oil microcapsule:
By 18g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 250ml pulullan polysaccharide solution, add 25g Rosa Damascana, at 35 DEG C of temperature, stir 2.5h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
32g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 3.5g, microcapsules are dispersed in uniformly wholeIn reason liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 55 DEG C, make pure cotton fabric.
Embodiment tetra-
The first step: prepare rose essential-oil microcapsule:
By 12g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 150ml pulullan polysaccharide solution, add 15g Rosa Damascana, under temperature 45 C, stir 1.5h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
28g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 2.5g, microcapsules are dispersed in uniformly wholeIn reason liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 65 DEG C, make pure cotton fabric.
Embodiment five
The first step: prepare rose essential-oil microcapsule:
By 15g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 200ml pulullan polysaccharide solution, add 30g Rosa Damascana, at 40 DEG C of temperature, stir 3h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
35g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 4g, make microcapsules be dispersed in uniformly arrangementIn liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 70 DEG C, make pure cotton fabric.
Embodiment six
The first step: prepare rose essential-oil microcapsule:
By 10g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 100ml pulullan polysaccharide solution, add 20g Rosa Damascana, at 30 DEG C of temperature, stir 2h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
30g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 3g, make microcapsules be dispersed in uniformly arrangementIn liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 60 DEG C, make pure cotton fabric.
Embodiment seven
The first step: prepare rose essential-oil microcapsule:
By 10g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 200ml pulullan polysaccharide solution, add 20g Rosa Damascana, at 40 DEG C of temperature, stir 2h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
35g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 3g, make microcapsules be dispersed in uniformly arrangementIn liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 70 DEG C, make pure cotton fabric.
Embodiment eight
The first step: prepare rose essential-oil microcapsule:
By 15g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 100ml pulullan polysaccharide solution, add 30g Rosa Damascana, at 30 DEG C of temperature, stir 3h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
30g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 4g, make microcapsules be dispersed in uniformly arrangementIn liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 60 DEG C, make pure cotton fabric.
Embodiment nine
The first step: prepare rose essential-oil microcapsule:
By 12g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 150ml pulullan polysaccharide solution, add 25g Rosa Damascana, at 35 DEG C of temperature, stir 2.7h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
34g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 3.2g, microcapsules are dispersed in uniformly wholeIn reason liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 67 DEG C, make pure cotton fabric.
Embodiment ten
The first step: prepare rose essential-oil microcapsule:
By 14g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolve completely, prepare general ShandongBlue polysaccharide solution;
Take out 150ml pulullan polysaccharide solution, add 25g Rosa Damascana, at 35 DEG C of temperature, stir 2.5h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, and collect lower floor's container, be placed inDry 12h in the baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
32g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 3.5g, microcapsules are dispersed in uniformly wholeIn reason liquid, mix and obtain composite essential oil microcapsule dressing agent.
The application of rose essential-oil microcapsule finishing agent of the present invention is, with watering can, microcapsule dressing agent solution is sprayed on to baftaUpper, rose essential-oil microcapsule finishing agent is evenly soaked pure cotton fabric, dry at 65 DEG C, make pure cotton fabric.
The test of menstrual regulation situation:
Choose 220 irregular menstruation persons and test, wherein wear by above-mentioned 10 embodiment and process rear gained for 200The underwear that pure cotton fabric is made, is divided into 10 groups, 20 every group; Wear undressed pure cotton fabric underwear for other 20,Everyone 4, everyone evaluates oneself, from whether menstrual period are normal, whether skin improves and whether emotional state is improved.Taking every group of number of improving as pure cotton fabric prepared by index measurement the present invention, whether female incretion is had to effect.
Table one: dress implements to arrange the test result that rear underwear improved menstrual period
| 0 day | 30 days | 60 days | 90 days | |
| Embodiment mono- | 0 | 4 | 7 | 14 |
| Embodiment bis- | 0 | 5 | 7 | 13 |
| Embodiment tri- | 0 | 4 | 6 | 13 |
| Embodiment tetra- | 0 | 6 | 9 | 15 |
| Embodiment five | 0 | 8 | 11 | 17 |
| Embodiment six | 0 | 9 | 12 | 18 |
| Embodiment seven | 0 | 7 | 11 | 18 |
| Embodiment eight | 0 | 8 | 11 | 18 |
| Embodiment nine | 0 | 7 | 10 | 17 |
| Embodiment ten | 0 | 6 | 9 | 17 |
| Do not arrange | 0 | 2 | 4 | 3 |
Table two: dress implements to arrange rear underwear to improving the test result of skin
| 0 day | 30 days | 60 days | 90 days | |
| Embodiment mono- | 0 | 7 | 12 | 15 |
| Embodiment bis- | 0 | 5 | 10 | 14 |
| Embodiment tri- | 0 | 7 | 11 | 16 |
| Embodiment tetra- | 0 | 8 | 14 | 19 |
| Embodiment five | 0 | 9 | 14 | 18 |
| Embodiment six | 0 | 9 | 13 | 16 |
| Embodiment seven | 0 | 8 | 13 | 17 |
| Embodiment eight | 0 | 7 | 12 | 16 |
| Embodiment nine | 0 | 7 | 13 | 16 |
| Embodiment ten | 0 | 6 | 13 | 15 |
| Do not arrange | 0 | 3 | 5 | 5 |
Table three: dress implements to arrange rear underwear to improving the test result of emotional state
| 0 day | 30 days | 60 days | 90 days | |
| Embodiment mono- | 0 | 3 | 6 | 10 |
| Embodiment bis- | 0 | 3 | 5 | 11 |
| Embodiment tri- | 0 | 5 | 8 | 12 |
| Embodiment tetra- | 0 | 4 | 7 | 11 |
| Embodiment five | 0 | 6 | 10 | 15 |
| Embodiment six | 0 | 5 | 9 | 16 |
| Embodiment seven | 0 | 4 | 8 | 12 |
| Embodiment eight | 0 | 5 | 8 | 13 |
| Embodiment nine | 0 | 4 | 7 | 11 |
| Embodiment ten | 0 | 3 | 8 | 12 |
| Do not arrange | 0 | 2 | 3 | 3 |
The fabric preparing through the embodiment of the present invention is made underwear, after volunteer's dress, and women's skin and moodHave more obviously and to improve, skin condition is got better, and emotional change also has more obviously and relaxes, and some women dysmenorrhoea situation has and changesKind.
Anti-microbial property test: adopt the evaluation Part II of GB/T20944.2-2007 antibacterial textile performance (to absorbMethod) pure cotton fabric is carried out to antibacterial test, test it to staphylococcus aureus (ATCC6538) Gram-positiveThe bacteriostasis property of bacterium and Escherichia coli (ATCC11229) Gram-negative bacteria.
Antibacterial fabric washing resistance performance:
Test according to the experimental condition AIM in GB/T12490-1990, adopt the agent of ECE standard wash. Clean knotShu Zuowei 5 times washing (be equivalent to concrete operations condition and the step of 5 washings: 40 DEG C, 150mL cleaning solution, steel ball10, wash 45min, after washing, take out sample, in the water of 40 DEG C and 100mL, clean twice, each 1min),Reach after the washing times of regulation, fully clean sample with distilled water, dry.
Table four: embodiment arranges rear bafta Chinese People's Anti-Japanese Military and Political College enterobacteria the performance test results
Table five: embodiment arranges rear bafta anti-Staphylococcus aureus the performance test results
| 0 day | 30 days | 60 days | 90 days | |
| Embodiment mono- | 87.36±0.47 | 81.12±0.82 | 75.31±1.08 | 69.12±0.94 |
| Embodiment bis- | 86.03±0.91 | 80.04±0.78 | 74.91±0.52 | 68.12±0.43 |
| Embodiment tri- | 87.84±1.19 | 81.25±0.77 | 75.56±0.67 | 69.05±0.87 |
| Embodiment tetra- | 86.63±0.9 | 80.7±1 | 74.43±0.69 | 68.92±0.52 |
| Embodiment five | 89.2±0.91 | 83.26±0.61 | 77.99±0.72 | 71.83±0.78 |
| Embodiment six | 89.84±0.55 | 83.84±0.97 | 77.75±0.59 | 71.76±1.04 |
| Embodiment seven | 88.01±0.4 | 81.75±0.65 | 76.56±0.68 | 70.66±0.78 |
| Embodiment eight | 88.32±1.15 | 82.91±0.77 | 76.43±1.1 | 70.51±0.62 |
| Embodiment nine | 88.84±0.6 | 83.05±0.81 | 76.83±0.97 | 70.4±0.57 |
| Embodiment ten | 88.09±1.01 | 82.84±0.91 | 76±0.41 | 70.93±0.86 |
| Do not arrange | 18.84±0.55 | 16.08±0.5 | 14.39±1.11 | 12.21±0.98 |
Table six: embodiment arranges rear bafta washing times antagonism Escherichia coli performance test result
Table seven: embodiment arranges rear bafta washing times to anti-Staphylococcus aureus the performance test results
| 0 day | 10 times | 20 times | 30 times | |
| Embodiment mono- | 87.36±0.47 | 80.28±0.39 | 74.31±0.81 | 66.09±0.53 |
| Embodiment bis- | 86.03±0.91 | 79.14±0.47 | 73.82±0.6 | 65.52±0.54 |
| Embodiment tri- | 87.84±1.19 | 80.04±0.45 | 74.49±0.52 | 66.36±0.93 |
| Embodiment tetra- | 86.63±0.9 | 78.69±1.13 | 72.42±1.09 | 64.17±1.17 |
| Embodiment five | 89.2±0.91 | 81.64±0.99 | 75.93±0.82 | 67.68±0.97 |
| Embodiment six | 89.84±0.55 | 81.82±0.55 | 75.5±1.19 | 67.89±1.08 |
| Embodiment seven | 88.01±0.4 | 80.23±0.72 | 74.54±1.17 | 66.99±0.9 |
| Embodiment eight | 88.32±1.15 | 80.98±0.78 | 74.85±1.11 | 66.53±0.63 |
| Embodiment nine | 88.84±0.6 | 80.96±0.9 | 74.35±0.63 | 66.19±0.71 |
| Embodiment ten | 88.09±1.01 | 80.11±0.32 | 73.89±1 | 65.9±0.5 |
| Do not arrange | 18.84±0.55 | 14.28±0.31 | 11.32±0.52 | 7.39±0.76 |
Above content is only preferred embodiments of the present invention, for those of ordinary skill in the art, according to the present inventionThought, all will change in specific embodiments and applications, this description should not be construed as rightRestriction of the present invention.
Claims (7)
1. a preparation method for rose essential-oil microcapsule finishing agent, is characterized in that, comprises following stepRapid:
The first step: prepare rose essential-oil microcapsule:
By 10-20g pulullan polysaccharide, add in 1000ml distilled water, in 30 DEG C of water-baths, dissolveCompletely, prepare pulullan polysaccharide solution;
Take out 100ml-300ml pulullan polysaccharide solution, add 10-30g Rosa Damascana, in temperatureAt 30-50 DEG C, stir 1-3h;
At 4 DEG C, refrigeration leaves standstill 24h, suction filtration upper strata distilled water, then use petroleum ether, collect lower floor's bagTolerant, be placed in the dry 12h of baking oven of 35 DEG C, gained powdered substance is rose essential-oil microcapsule;
Second step: prepare rose essential-oil microcapsule finishing agent:
25-35g microcapsules are dissolved in 1L purified water, add pulullan polysaccharide 2-4g, make microcapsulesBe dispersed in uniformly in dressing liquid, mix and obtain composite essential oil microcapsule dressing agent.
2. the preparation method of a kind of rose essential-oil microcapsule finishing agent according to claim 1, itsBe characterised in that: the first step is prepared in rose essential-oil microcapsule 10-15g pulullan polysaccharide, adds 1000mlIn distilled water, in 30 DEG C of water-baths, dissolve completely, prepare pulullan polysaccharide solution.
3. the preparation method of a kind of rose essential-oil microcapsule finishing agent according to claim 1, itsBe characterised in that: the first step prepares that in rose essential-oil microcapsule, to take out 100ml-200ml pulullan polysaccharide moltenLiquid, adds 20-30g Rosa Damascana to stir.
4. the preparation method of a kind of rose essential-oil microcapsule finishing agent according to claim 1, itsBe characterised in that: the first step is prepared in rose essential-oil microcapsule and added after Rosa Damascana, at 30-40 DEG C, stirMix 2-3h.
5. the preparation method of a kind of rose essential-oil microcapsule finishing agent according to claim 1, itsBe characterised in that: second step is prepared in rose essential-oil microcapsule finishing agent 30-35g microcapsules are dissolved in to 1LIn purified water, add pulullan polysaccharide 3-4g, microcapsules are dispersed in dressing liquid uniformly, mixEvenly obtain composite essential oil microcapsule dressing agent.
6. the application of the rose essential-oil microcapsule finishing agent described in one of claim 1 to 5, its featureBe: microcapsule dressing agent solution is sprayed on bafta with watering can, rose essential-oil microcapsule is arrangedAgent evenly soaks pure cotton fabric, dries at 50-70 DEG C, makes pure cotton fabric.
7. the application of rose essential-oil microcapsule finishing agent according to claim 6, is characterized in that:Microcapsule dressing agent solution is sprayed on bafta with watering can, makes rose essential-oil microcapsule finishing agent to pureBafta evenly soaks, and dries at 60-70 DEG C, makes bafta.
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