CN100528137C - Preparing method of attapulgite Chinese traditional medicine toothpaste - Google Patents
Preparing method of attapulgite Chinese traditional medicine toothpaste Download PDFInfo
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- CN100528137C CN100528137C CNB2008100189126A CN200810018912A CN100528137C CN 100528137 C CN100528137 C CN 100528137C CN B2008100189126 A CNB2008100189126 A CN B2008100189126A CN 200810018912 A CN200810018912 A CN 200810018912A CN 100528137 C CN100528137 C CN 100528137C
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- 239000000606 toothpaste Substances 0.000 title claims abstract description 46
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- 238000000034 method Methods 0.000 title claims abstract description 9
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
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- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims abstract description 6
- 241000628997 Flos Species 0.000 claims abstract description 6
- 235000003143 Panax notoginseng Nutrition 0.000 claims abstract description 6
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- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 5
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 5
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- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 abstract 1
- 235000009917 Crataegus X brevipes Nutrition 0.000 abstract 1
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- 235000009685 Crataegus X maligna Nutrition 0.000 abstract 1
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- 235000009486 Crataegus bullatus Nutrition 0.000 abstract 1
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 abstract 1
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- 240000000171 Crataegus monogyna Species 0.000 abstract 1
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- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 abstract 1
- 240000002924 Platycladus orientalis Species 0.000 abstract 1
- 229940116229 borneol Drugs 0.000 abstract 1
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 abstract 1
- 238000009924 canning Methods 0.000 abstract 1
- 230000005574 cross-species transmission Effects 0.000 abstract 1
- 238000007872 degassing Methods 0.000 abstract 1
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 abstract 1
- 238000009775 high-speed stirring Methods 0.000 abstract 1
- 229940010454 licorice Drugs 0.000 abstract 1
- 235000019645 odor Nutrition 0.000 abstract 1
- 238000004537 pulping Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 12
- 239000008280 blood Substances 0.000 description 6
- 210000004369 blood Anatomy 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
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- 230000023597 hemostasis Effects 0.000 description 4
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
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- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 241000193155 Clostridium botulinum Species 0.000 description 1
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- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
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- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
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- 241001148470 aerobic bacillus Species 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
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- 150000001450 anions Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
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- 230000000740 bleeding effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- JUNWLZAGQLJVLR-UHFFFAOYSA-J calcium diphosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])(=O)OP([O-])([O-])=O JUNWLZAGQLJVLR-UHFFFAOYSA-J 0.000 description 1
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 description 1
- XAAHAAMILDNBPS-UHFFFAOYSA-L calcium hydrogenphosphate dihydrate Chemical compound O.O.[Ca+2].OP([O-])([O-])=O XAAHAAMILDNBPS-UHFFFAOYSA-L 0.000 description 1
- 229940043256 calcium pyrophosphate Drugs 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000000812 cholinergic antagonist Substances 0.000 description 1
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- 210000003298 dental enamel Anatomy 0.000 description 1
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- 235000019821 dicalcium diphosphate Nutrition 0.000 description 1
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000005360 mashing Methods 0.000 description 1
- 239000013521 mastic Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000011022 opal Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
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- 238000012216 screening Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
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- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
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- Cosmetics (AREA)
Abstract
The invention discloses a production method of an attapulgite traditional Chinese medicine toothpaste. The key point of the technical proposal of the production method is that the method consists of the steps of ingredients preparing, low-speed stirring, crushing and pulping, grinding, high-speed stirring, vacuum degasification and the canning of the finished product. The attapulgite traditional Chinese medicine toothpaste consists of paste attapulgite clay, herba cirsii japenici, flos sophorae, hawthorn, baked rhizoma zingiberis, rhizoma imperatae, Chinese arborvitae twig, notoginseng, licorice, borneol, lauryl sodium sulfate, potassium sorbate and deionized water. The attapulgite traditional Chinese medicine toothpaste is characterized by softness, delicacy, small friction hardness, clean and uniformity, good absorption ability and no roughness; the invention is also characterized in that the paste does not spill over the tube, no water is separated, the flavor and color is normal, and the glassslide does not have any nick. The attapulgite traditional Chinese medicine toothpaste can absorb and remove various odors in oral cavity and also contributes to oral diseases prevention. The invention is suitable for producing attapulgite traditional Chinese medicine toothpaste, traditional Chinese medicine toothpaste and other medicinal toothpastes.
Description
Technical field:
The present invention relates to toothpaste, be specifically related to a kind of production method of attapulgite Chinese herbal toothpaste.
Background technology:
Chinese herbal medicine is abundant in the China source, a lot of ancient prescription curative effects are all very definite, toxic and side effects is littler than Western medicine, and the Chinese herbal medicine adding ingredient in the toothpaste relates to processes such as Chinese herbal medicine collection, concocting method, effective ingredient refinement, and it has determined directly whether the elite composition that adds in the toothpaste can play a role.
The Chinese herbal medicine that is adopted in the Chinese herbal toothpaste is to adopt infusion method mostly, extracts its soak or its concentrated solution, still contains a large amount of effective ingredient in the garbage behind the medicinal herb soak, causes bigger economic loss.
The abrasivus that Chinese herbal toothpaste is commonly used has calcium carbonate, calcium phosphate dibasic dihydrate, no hydration calcium hydrogen phosphate, calcium pyrophosphate, anhydride silica, aluminium hydroxide etc., because these abrasivus hardness height, granule is coarse, there is not stickiness, absorption property is poor, and life-time service easily causes wearing and tearing to the enamel of dental surface.
Summary of the invention:
The objective of the invention is to overcome weak point in the prior art, a kind of production method of attapulgite Chinese herbal toothpaste is provided.
The production method of attapulgite Chinese herbal toothpaste is batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgas, cannedly is the finished product of attapulgite Chinese herbal toothpaste.
The attapulgite Chinese herbal toothpaste is made up of lip lipstick attapulgite clay, Radix Cirsii Japonici, Flos Sophorae, Fructus Crataegi, Rhizoma Zingiberis Preparatum, Rhizoma Imperatae, Cacumen Platycladi, Radix Notoginseng, Radix Glycyrrhizae, Borneolum Syntheticum, sodium lauryl sulphate, potassium sorbate and deionized water.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m
2More than/the g, most cation, hydrone and a certain size organic molecule all can directly be adsorbed in the duct.
Use attapulgite ore pul making production technology, the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of lip lipstick attapulgite clay.Lip lipstick attapulgite clay is through powerful stirring at a high speed, become the special good natural gelinite of a kind of thixotropy and gumminess, viscosity is up to more than the 10000mPas, absorption property and performance of keeping humidity have all obtained further raising, attapulgite clay after the high-speed stirred has the total characteristic of abrasivus, adhesive and wetting agent.
Radix Cirsii Japonici has cooling blood for hemostasis, the function of removing blood stasis to reduce swelling;
Flos Sophorae has heat clearing away, removing heat from blood, hemostatic effect;
Fructus Crataegi has promoting blood circulation to remove blood stasis, changes the effect of the removing food stagnancy that stagnates;
Rhizoma Zingiberis Preparatum has warming spleen and stomach for dispelling cold, the effect of warming the meridian for stopping bleeding;
Rhizoma Imperatae has cooling blood for hemostasis, clearing away heat-damp and promoting diuresis, the effect of promoting the production of body fluid to quench thirst;
Cacumen Platycladi has removing heat from blood, hemostasis, wind-damp dispelling, the effect of the toxic swelling that looses;
Radix Notoginseng has the effect of antiinflammatory, hemostasis, pain relieving, raising human body immunocompetence;
Effects such as Radix Glycyrrhizae has eliminating fire and detoxication, coordinating the actions of various ingredients in a prescription, eliminates the phlegm, pain relieving and spasmolytic;
Borneolum Syntheticum has antiinflammatory, antibiotic, pain relieving and antisepsis.
Sodium lauryl sulphate belongs to anion surfactant, and is soluble in water, and compatibility is good again with anion, nonionic, has good emulsifying, foaming, infiltration, decontamination and dispersive property, and foaming power is strong.
Potassium sorbate is mould fungus inhibition effectively, the activity of yeast and aerobic bacteria, can also prevent harmful microbe growth and breedings such as bacillus botulinus, staphylococcus, Salmonella, it is stronger than bactericidal action that it restrains the effect of growing, thereby reach the holding time that prolongs toothpaste effectively, and the local flavor of maintenance toothpaste, its antiseptic effect is 5-10 a times of like product sodium benzoate.
The present invention is achieved by following technical proposals:
The production method of attapulgite Chinese herbal toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with the attapulgite Chinese herbal toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite Chinese herbal toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; The purpose of stirring at low speed is that various batchings are stirred, and helps pulverizing the operate as normal of beater; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; Multi-functional colloid grinding tool has functions such as the pulverizing of wet processed fluid ultra micron, grinding, emulsifying, dispersion, homogenizing, stirring, mixing, can replace and be better than stone grinder, sand mill, ball mill, dispersing emulsification machine, shearing disperse pump, work efficiencies such as homogeneous emulsifying machine, three-roller, tissue mashing machine; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; The ultrahigh speed blender has unique blade design and stepless speed-regulating device, can select optimal speed according to manufacturing technique requirent, and after the pasty mixture after the grinding stirred through ultrahigh speed, viscosity was up to more than the 10000mPas; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite Chinese herbal toothpaste.
The batching of described attapulgite Chinese herbal toothpaste is made up of following component: lip lipstick attapulgite clay 30～55%, Radix Cirsii Japonici 1～5%, Flos Sophorae 1～5%, Fructus Crataegi 1～5%, Rhizoma Zingiberis Preparatum 1～5%, Rhizoma Imperatae 1～5%, Cacumen Platycladi 1～5%, Radix Notoginseng 1～5%, Radix Glycyrrhizae 1～5%, Borneolum Syntheticum 0.05～0.5%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.05～0.5% and deionized water 15～45% by weight percentage;
The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay;
This production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, and Granted publication day: on December 6th, 2006;
Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15～35%, water 65～85%.
The attapulgite Chinese herbal toothpaste uses lip lipstick attapulgite clay to be primary raw material, does not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.
The Plant fiber of the Chinese herbal medicine that the attapulgite Chinese herbal toothpaste adopts after pulverizing and grinding not only can increase the denseness of lotion of toothpaste, can also improve the friction effect and the stability of toothpaste.
That the attapulgite Chinese herbal toothpaste has is soft fine and smooth, friction hardness is little, clean evenly, good, the no sand feeling of absorption property, mastic do not overflow the mouth of pipe, do not separate water outlet, the fragrance color and luster normally and the characteristics of slide no marking.
The multiple foreign odor that the attapulgite Chinese herbal toothpaste can adsorb and remove in the oral cavity is distinguished the flavor of, the prevention oral disease is had certain assosting effect.
The present invention is applicable to and produces attapulgite Chinese herbal toothpaste, Chinese herbal toothpaste and other medicines toothpaste.
The specific embodiment:
The invention will be further described below in conjunction with embodiment:
The production method of attapulgite Chinese herbal toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with the attapulgite Chinese herbal toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite Chinese herbal toothpaste, the speed controlling of blender is at 600 rev/mins, the stirring at low speed time was controlled at 6 minutes, and the speed controlling of pulverizing beater is at 2800 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.010 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 6000 rev/mins; The high-speed stirred time was controlled at 25 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite Chinese herbal toothpaste.
The batching of described attapulgite Chinese herbal toothpaste is made up of following component: lip lipstick attapulgite clay 38.0%, Radix Cirsii Japonici 4.0%, Flos Sophorae 4.0%, Fructus Crataegi 4.0%, Rhizoma Zingiberis Preparatum 3.0%, Rhizoma Imperatae 3.0%, Cacumen Platycladi 2.5%, Radix Notoginseng 2.0%, Radix Glycyrrhizae 2.0%, Borneolum Syntheticum 0.1%, sodium lauryl sulphate 1.3%, potassium sorbate 0.1% and deionized water 36.0% by weight percentage.
Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30%, water 70%.
Main physical and chemical index testing result
Claims (1)
1, a kind of production method of attapulgite Chinese herbal toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with the attapulgite Chinese herbal toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite Chinese herbal toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite Chinese herbal toothpaste;
The batching of described attapulgite Chinese herbal toothpaste is made up of following component: lip lipstick attapulgite clay 30～55%, Radix Cirsii Japonici 1～5%, Flos Sophorae 1～5%, Fructus Crataegi 1～5%, Rhizoma Zingiberis Preparatum 1～5%, Rhizoma Imperatae 1～5%, Cacumen Platycladi 1～5%, Radix Notoginseng 1～5%, Radix Glycyrrhizae 1～5%, Borneolum Syntheticum 0.05～0.5%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.05～0.5% and deionized water 15～45% by weight percentage;
The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay;
Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15～35%, water 65～85%.
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