CN100539994C - Concave-convex bar fluorine-containing green tea toothpaste and production method - Google Patents

Abstract

The invention discloses a kind of concave-convex bar fluorine-containing green tea toothpaste and production method, the main points of its technical scheme are, the production method of concave-convex bar fluorine-containing green tea toothpaste is steam beating, batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgas, cannedly is the finished product of concave-convex bar fluorine-containing green tea toothpaste.Concave-convex bar fluorine-containing green tea toothpaste is made up of lip lipstick attapulgite clay, fresh tea leaf in its, sodium monofluorophosphate, sodium lauryl sulphate, potassium sorbate, Borneolum Syntheticum and deionized water.Concave-convex bar fluorine-containing green tea toothpaste has the characteristics of soft fine and smooth, clean all even cool mouth, fluorion in the concave-convex bar fluorine-containing green tea toothpaste is free fully, can be absorbed by tooth better, reduce tooth wear, the enamel of enhancing and regeneration dental surface, thus the multiple foreign odor that reaches in better mothproof effect and absorption and the removing oral cavity is distinguished the flavor of.The present invention is applicable to and produces concave-convex bar fluorine-containing green tea toothpaste, fluorine-containing Chinese herbal toothpaste and other fluorine-containing medicated toothpaste.

Description

Concave-convex bar fluorine-containing green tea toothpaste and production method

Technical field

The present invention relates to toothpaste, be specifically related to a kind of concave-convex bar fluorine-containing green tea toothpaste and production method.

Background technology

Domestic had some manufacturers producing green tea toothpaste, abrasivus commonly used has calcium carbonate, calcium phosphate dibasic dihydrate, no hydration calcium hydrogen phosphate, calcium pyrophosphate, anhydride silica and aluminium hydroxide etc., because the hardness of these abrasivuss is higher relatively, granule is coarse, there is not stickiness, absorption property is poor, and life-time service easily causes wearing and tearing to the enamel of dental surface.

The main component of green tea toothpaste also has sorbitol, CMC, essence and green tea element etc.The production method of green tea element adopts methods such as soaking concentrated and chemical extraction mostly, and solvent consumption is big, and extraction ratio is low.

Chinese patent publication number CN1328816, open day is on January 2nd, 2002, name is called " articles for use such as health-care toothpaste that contain Radix Glycyrrhizae, green tea ", disclose a kind of " articles for use such as health-care toothpaste that contain Radix Glycyrrhizae, green tea belong to technology such as daily-use chemical industry; be used for the protection in tooth and oral cavity ", and required in the claims: " feature that contains the health-care toothpaste of Radix Glycyrrhizae, green tea is that this product contains Sucus Glycyrrhizae and the green tea water of weight more than 1% ".

The weak point of above-mentioned patent is to be to adopt decoction and Filtration to produce Sucus Glycyrrhizae and green tea water in this technology, there is not to make full use of the effective ingredient of Radix Glycyrrhizae and green tea, the employing calcium carbonate is an abrasivus, its hardness is higher relatively, granule is coarse, do not have stickiness, absorption property is poor, and life-time service easily causes wearing and tearing to the enamel of dental surface.

Summary of the invention

The objective of the invention is to overcome weak point in the prior art, a kind of concave-convex bar fluorine-containing green tea toothpaste and production method are provided.

The production method of concave-convex bar fluorine-containing green tea toothpaste is steam beating, batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgas, cannedly is the finished product of concave-convex bar fluorine-containing green tea toothpaste.

Concave-convex bar fluorine-containing green tea toothpaste is made up of lip lipstick attapulgite clay, fresh tea leaf in its, sodium monofluorophosphate, sodium lauryl sulphate, potassium sorbate, Borneolum Syntheticum and deionized water.

Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m ²More than/the g, most cation, hydrone and a certain size organic molecule all can directly be adsorbed in the duct, and its water absorption can reach more than 150%.

Use attapulgite ore pul making production technology, the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of lip lipstick attapulgite clay, have the characteristics of ultrafine dust, friction little, the no sand feeling of hardness and soft fine and smooth free from extraneous odour.

Lip lipstick attapulgite clay is through powerful stirring at a high speed, become the special good natural gelinite of a kind of thixotropy and gumminess, viscosity is up to more than the 10000mPas, absorption property and performance of keeping humidity have all obtained further raising, attapulgite clay after the high-speed stirred, total characteristic with abrasivus, adhesive and wetting agent, use lip lipstick attapulgite clay to produce toothpaste and do not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.

Fresh tea leaf in its is meant the tender tip of in time plucking on the Camellia sinensis of bud-leaf, and Folium Camelliae sinensis has the effect of releasing alimentary toxicosis, and the active component in the Folium Camelliae sinensis has Detoxication to toxin such as vibrio cholera, vibrio parahaemolytious, staphylococcus aureuses.

Steam beating is the high temperature hyther of utilizing in the steam, has destroyed the activation of enzyme in the fresh tea leaf in its, has stoped the Main Ingredients and Appearance in the Folium Camelliae sinensis---the enzymatic oxidation of Polyphenols, more reservation original various chemical constituents in the fresh Folium Camelliae sinensis, keep leaf color jade green.

The outstanding advantage of sodium monofluorophosphate is soluble in water, good stability, and the anti-caries effect is remarkable, and toxicity is little, is free from side effects, and does not have action of rust, and its chemical compound is stable, and is compatible good, and remarkable bactericidal action is arranged.

Sodium lauryl sulphate belongs to anion surfactant, and is soluble in water, and compatibility is good again with anion, nonionic, has good emulsifying, foaming, infiltration, decontamination and dispersive property, and foaming power is strong.

Borneolum Syntheticum has antiinflammatory, antibiotic, pain relieving and antisepsis.

The present invention is achieved by following technical proposals:

The production method of concave-convex bar fluorine-containing green tea toothpaste is characterized in that, the fresh tea leaf in its after 1. will plucking is carried out steam beating, and vapor (steam) temperature is controlled at 100～110 ℃, and fixation time was controlled at 6～60 seconds; 2. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with concave-convex bar fluorine-containing green tea toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of concave-convex bar fluorine-containing green tea toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; The purpose of stirring at low speed is that various batchings are stirred, and helps pulverizing the operate as normal of beater; 3. the mixture that 2. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; Multi-functional colloid grinding tool has functions such as the pulverizing of wet processed fluid ultra micron, grinding, emulsifying, dispersion, homogenizing, stirring, mixing, can replace and be better than stone grinder, sand mill, ball mill, dispersing emulsification machine, shearing disperse pump, work efficiencies such as homogeneous emulsifying machine, three-roller, tissue mashing machine; 4. the pasty mixture after the grinding that 3. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; The ultrahigh speed blender has unique blade design and stepless speed-regulating device, can select optimal speed according to manufacturing technique requirent, and after the pasty mixture after the grinding stirred through ultrahigh speed, viscosity was up to more than the 10000mPas; 5. the paste semi-finished product that 4. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex bar fluorine-containing green tea toothpaste.

The batching of described concave-convex bar fluorine-containing green tea toothpaste is made up of following component: lip lipstick attapulgite clay 30～60%, fresh tea leaf in its 2～25%, sodium monofluorophosphate 0.05～0.8%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.05～0.5%, Borneolum Syntheticum 0.05～0.5% and deionized water 15～45% by weight percentage.

The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay.

This production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15～35%, water 65～85%.

Concave-convex bar fluorine-containing green tea toothpaste uses lip lipstick attapulgite clay to be primary raw material, does not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.

Folium Camelliae sinensis Plant fiber after pulverizing and grinding not only can increase the denseness of lotion of toothpaste, can also improve the friction effect and the stability of toothpaste.

Concave-convex bar fluorine-containing green tea toothpaste steady chemical structure, mastic are not overflowed the mouth of pipe, do not separate water outlet, and the fragrance color and luster is normal, the slide no marking.

Concave-convex bar fluorine-containing green tea toothpaste has the characteristics of soft fine and smooth, clean all even cool mouth, fluorion in the concave-convex bar fluorine-containing green tea toothpaste is free fully, can be absorbed by tooth better, reduce tooth wear, the enamel of enhancing and regeneration dental surface, thus the multiple foreign odor that reaches in better mothproof effect and absorption and the removing oral cavity is distinguished the flavor of.

The present invention is applicable to and produces concave-convex bar fluorine-containing green tea toothpaste, fluorine-containing Chinese herbal toothpaste and other fluorine-containing medicated toothpaste.

The specific embodiment

The invention will be further described below in conjunction with embodiment:

The production method of concave-convex bar fluorine-containing green tea toothpaste is characterized in that, the fresh tea leaf in its after 1. will plucking is carried out steam beating, and vapor (steam) temperature is controlled at 105 ℃, and fixation time was controlled at 15 seconds; 2. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with concave-convex bar fluorine-containing green tea toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of concave-convex bar fluorine-containing green tea toothpaste, the speed controlling of blender is at 600 rev/mins, the stirring at low speed time was controlled at 10 minutes, and the speed controlling of pulverizing beater is at 2800 rev/mins; 3. the mixture that 2. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 4. the pasty mixture after the grinding that 3. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 10000 rev/mins, and the high-speed stirred time was controlled at 25 minutes; 5. the paste semi-finished product that 4. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex bar fluorine-containing green tea toothpaste.

The batching of described concave-convex bar fluorine-containing green tea toothpaste is made up of following component: lip lipstick attapulgite clay 50.0%, fresh tea leaf in its 10.0%, sodium monofluorophosphate 0.6%, sodium lauryl sulphate 1.2%, potassium sorbate 0.1%, Borneolum Syntheticum 0.1% and deionized water 38.0% by weight percentage.

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30%, water 70%.

Claims (1)

1, the production method of concave-convex bar fluorine-containing green tea toothpaste is characterized in that, the fresh tea leaf in its after 1. will plucking is carried out steam beating, and vapor (steam) temperature is controlled at 100～110 ℃, and fixation time was controlled at 6～60 seconds; 2. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with concave-convex bar fluorine-containing green tea toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of concave-convex bar fluorine-containing green tea toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; 3. the mixture that 2. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 4. the pasty mixture after the grinding that 3. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; 5. the paste semi-finished product that 4. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex bar fluorine-containing green tea toothpaste;

The batching of described concave-convex bar fluorine-containing green tea toothpaste is made up of following component: lip lipstick attapulgite clay 30～60%, fresh tea leaf in its 2～25%, sodium monofluorophosphate 0.05～0.8%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.05～0.5%, Borneolum Syntheticum 0.05～0.5% and deionized water 15～45% by weight percentage;

The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay;

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15～35%, water 65～85%.