CN101347392A - Attapulgite lupulus anti-dandruff shampoo - Google Patents
Attapulgite lupulus anti-dandruff shampoo Download PDFInfo
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- CN101347392A CN101347392A CNA2008100218260A CN200810021826A CN101347392A CN 101347392 A CN101347392 A CN 101347392A CN A2008100218260 A CNA2008100218260 A CN A2008100218260A CN 200810021826 A CN200810021826 A CN 200810021826A CN 101347392 A CN101347392 A CN 101347392A
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- lupuli
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Abstract
The invention discloses an attapulgite hop anti-dandruff shampoo; the key point of the technical proposal is that the attapulgite hop anti-dandruff shampoo consists of modified pasty attapulgite clay, hop-alcohol mixed liquor, sodium lauryl sulfate, cocoanut amide propyl betaine, zinc pyrithione, salicylic acid, citric acid and deionized water; the production method of the attapulgite hop anti-dandruff shampoo comprises the steps of purifying, sodium treating, acidifying, mixing materials, socking, crushing and beating, grinding, stirring at high speed, emulsifying, vacuum degassing and filling and packaging to obtain the finished product of the attapulgite hop anti-dandruff shampoo. The zinc pyrithione in the attapulgite hop anti-dandruff shampoo is compatible with the salicylic acid, which can give full play to the beneficial effects of the zinc pyrithione and salicylic acid; the hop is added to the shampoo, which is helpful in adjusting oil balance of head skin, thus causing hair to be not oily and greasy, and deeply repairing the damaged hair. The attapulgite hop anti-dandruff shampoo is suitable for skin care and nursing for dandruff removal.
Description
Technical field
The present invention relates to shampoo, be specifically related to a kind of attapulgite lupulus anti-dandruff shampoo.
Background technology
The epidermis cell at scalp place because the cell of basal layer ceaselessly breeds, and releases to the surface, at last these cell maturations, become the horny layer that does not have life and come off.When scalp was very healthy, the cell that comes off was the powder that we are difficult for discovering, and also just can't see the dandruff.But when scalp went wrong, epidermal area just can not be ripe well, so peel off the dandruff that Here it is large stretch ofly.Seborrhea sicca goes out many sebaceous gland in the disease skin, ceaselessly sebum secreted prevents water evaporates, protection skin.If the sebum at scalp place is too much, the cell that comes off is attached on the scalp together, just become the dandruff in small, broken bits after the drying.
Chinese patent publication number CN1021385, open day is on October 12nd, 1988, name is called " a kind of highly effective liquid detergent and production method ", discloses " a kind of high-efficient washing spirit that is used for the sanitary purpose washing aspect of being made special auxiliary agent by inorganic mineral raw material bentonite and attapulgite.It is to make anion surfactant by preparing a certain amount of sodium lauryl sulphate, and CMC makes thickening, stabilizing agent, and lanoline is made conditioner and a certain amount of bentonite and attapulgite and made special auxiliary agent, spice, pigment and mix through heated and stirred.The present invention is cheap, and its cost of material only is about 75% of general shampoo and a shampoo paste.Strong detergency, consumption are few, nontoxic.”
The weak point of above-mentioned patent is not select for use in this technology to make special auxiliary agent through the inorganic mineral raw material bentonite and the attapulgite of purifying and modification is handled, and its dispersibility and suspendability are all poor, therefore can have influence on the product quality of highly effective liquid detergent.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of attapulgite lupulus anti-dandruff shampoo is provided.
Attapulgite lupulus anti-dandruff shampoo is made up of modified cream attapulgite clay, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor, sodium lauryl sulfate, cocamido propyl betaine, Zinc Pyrithione, salicylic acid, citric acid and deionized water.
The production method of attapulgite lupulus anti-dandruff shampoo is purification, sodium, acidify, batching, immersion, pulverizing making beating, grinding, high-speed stirred, emulsifying, vacuum outgas, cannedly is the finished product of attapulgite lupulus anti-dandruff shampoo.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m
2More than/the g.Use " wet beneficiation craft of attapulgite " and " attapulgite ore pul making production technology ", the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of attapulgite sludge slurry; Through the lip lipstick attapulgite clay after sodium processing and the acidification, it is the special good natural magnesium aluminium silicate gel of a kind of thixotropy and gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
The chemical constituent of Flos lupuli (Flos Humuli Lupuli) is known kind more than 200, comprises compositions such as protein, fat, wax, nitrogen-free extract, pectin fiber, aminoacid and inorganic substances, and special chemical component comprises essential oil of hop, bitter substance and polyphenol.Contain aromatic oil in the Flos lupuli (Flos Humuli Lupuli) body of gland, a kind of special Flos lupuli (Flos Humuli Lupuli) fragrant is arranged, the resin in the Flos lupuli (Flos Humuli Lupuli) has the antiseptical ability, helps regulating the oils and fats balance of skin of head.
Sodium lauryl sulfate series anion surfactant has good moistening, floatingization, decontamination foam performance, and is less to the zest of skin.
Cocamido propyl betaine is a kind of extremely gentle amphoteric surfactant, and to skin, non-stimulated, the no anaphylactic reaction of eye mucosa, its foam stabilization, exquisiteness can improve material body viscosity, and thickening effect is obvious; Having flexibility, bactericidal properties and antistatic property, is excellent hair conditioner.
Zinc Pyrithione is a kind of anti-dandruff and itching-relieving agent and high-effective broad-spectrum fungicide, it has powerful killing action to various antibacterials, especially fungus, mycete, yeast there is unique killing action, can effectively remove the dandruff, suppress seborrhea, prevent that scalp from itching, finally suppress or the generation of the prevention dandruff, delay the hair aging, reduce alopecia and produce poliosis.
Salicylic acid is soluble in ethanol, has outstanding exfoliation, the ability of Peppermint Extract, and is safe, and porous enters horny layer and pore depths, but can not cause stimulation to dermal tissue.Salicylic acid can also desalinate pigmented spots, dwindles pore, remove tiny wrinkle and improve the effect such as aging that hair causes because of Exposure to Sunlight.
Citric acid has gentle frank tart flavour, can improve and adjust the pH value of shampoo, improves the performance of surfactant.
The present invention is achieved by following technical proposals:
1, the batching of attapulgite lupulus anti-dandruff shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor 2～45%, sodium lauryl sulfate 0.1～5%, cocoyl CAB 0.1～5%, Zinc Pyrithione 0.1～5%, salicylic acid 0.01～3%, citric acid 0.01～3% and deionized water 10～40%.
Described modified cream attapulgite clay is on attapulgite ore pul making production technology basis, and attapulgite sludge slurry is carried out sodium processing, acidification, washing and sieve decontamination, and the mud of process post precipitation is modified cream attapulgite clay.
Attapulgite ore pul making production technology is: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is attapulgite sludge slurry finished product.
Above-mentioned production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%.
The pH value of the immersion water of emitting is neutral meta-acid, can be used to produce the raw material of transparent shampoo.
The batching of described Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor is made up of following component by weight percentage: Flos lupuli (Flos Humuli Lupuli) 15～55% and edible ethanol 45～85%, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor preparation method: 1. Flos lupuli (Flos Humuli Lupuli) is added and soak 3～7 days in the edible ethanol, 2. the Flos lupuli (Flos Humuli Lupuli) mixture input after soaking is pulverized in the beater and is pulverized, be Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor behind the pulverizing making beating mix homogeneously, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor fineness of the particles is less than 0.074 millimeter;
The alcohol concentration of described edible ethanol is 50%.
2, the production method of attapulgite lupulus anti-dandruff shampoo: 1. carry out stirring at low speed in the batching adding blender with attapulgite lupulus anti-dandruff shampoo, mix the back and be the mixture of attapulgite lupulus anti-dandruff shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite lupulus anti-dandruff shampoo.
Attapulgite lupulus anti-dandruff shampoo uses modified cream attapulgite clay to be primary raw material, does not need to add in addition thickening agent and wetting agent, not only can improve the quality of shampoo, can also reduce production costs greatly.
Behind the processing of attapulgite sludge slurry process sodium, acidification, washing and the sieve decontamination, lip lipstick attapulgite clay becomes a kind of thixotropy and the special good natural magnesium aluminium silicate gel of gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Zinc Pyrithione and salicylic acid in the attapulgite lupulus anti-dandruff shampoo are compatible, can give full play to both useful effects, fundamentally dispel dandruff, head pruritus and suppress dandruff regeneration, add Flos lupuli (Flos Humuli Lupuli), help regulating the oils and fats balance of skin of head, make hair not oily oiliness, the impaired hair quality of degree of depth maintenance.
The attapulgite lupulus anti-dandruff shampoo safety non-toxic, has exquisiteness and abundant foam, not only can make hair well absorb nutrition in the attapulgite lupulus anti-dandruff shampoo, relatively gentleer to eyes, hair and skin, nonirritant, and attapulgite lupulus anti-dandruff shampoo can also adsorb and remove foreign material such as sweat mixed with dirt on the hair, dust, microorganism, dandruff, abnormal flavour, the cleaning of maintenance scalp and hair and attractive in appearance, be easy to carry out rinsing after using the attapulgite lupulus anti-dandruff shampoo hair washing, impel hair softness Paint Gloss.
Attapulgite lupulus anti-dandruff shampoo is applicable to the hair caring nursing of removing dandruff.
The specific embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of attapulgite lupulus anti-dandruff shampoo is made up of following component by weight percentage: modified cream attapulgite clay 35%, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor 28%, sodium lauryl sulfate 3%, cocoyl CAB 2%, Zinc Pyrithione 1.3%, salicylic acid 0.5%, citric acid 0.2% and deionized water 30%.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 30% and water 70%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 3 days through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 98% and sodium hydroxide 2%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 2 days through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 97% after the sodium and concentration are 98% sulphuric acid 3%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 40 and water 60% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30% and water 70%.
The batching of described Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor is made up of following component by weight percentage: Flos lupuli (Flos Humuli Lupuli) 35% and edible ethanol 65%, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor preparation method: 1. Flos lupuli (Flos Humuli Lupuli) is added in the edible ethanol and soaked 4 days, 2. the Flos lupuli (Flos Humuli Lupuli) mixture input after soaking is pulverized in the beater and is pulverized, be Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor behind the pulverizing making beating mix homogeneously, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor fineness of the particles is less than 0.074 millimeter;
The alcohol concentration of described edible ethanol is 50%.
2, the production method of attapulgite lupulus anti-dandruff shampoo: 1. the batching adding of attapulgite lupulus anti-dandruff shampoo being pulverized in the beater and pulverize, is the mixture of attapulgite lupulus anti-dandruff shampoo behind the pulverizing making beating mix homogeneously; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite lupulus anti-dandruff shampoo.
Claims (1)
1, a kind of attapulgite lupulus anti-dandruff shampoo, it is characterized in that the batching of attapulgite lupulus anti-dandruff shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor 2～45%, sodium lauryl sulfate 0.1～5%, cocoyl CAB 0.1～5%, Zinc Pyrithione 0.1～5%, salicylic acid 0.01～3%, citric acid 0.01～3% and deionized water 10～40%;
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%;
The batching of described Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor is made up of following component by weight percentage: Flos lupuli (Flos Humuli Lupuli) 15～55% and edible ethanol 45～85%, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor preparation method: 1. Flos lupuli (Flos Humuli Lupuli) is added and soak 3～7 days in the edible ethanol, 2. the Flos lupuli (Flos Humuli Lupuli) mixture input after soaking is pulverized in the beater and is pulverized, be Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor behind the pulverizing making beating mix homogeneously, Flos lupuli (Flos Humuli Lupuli) alcohol mixed liquor fineness of the particles is less than 0.074 millimeter; The alcohol concentration of described edible ethanol is 50%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2008100218260A CN101347392B (en) | 2008-08-25 | 2008-08-25 | Attapulgite lupulus anti-dandruff shampoo |
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| CN2008100218260A CN101347392B (en) | 2008-08-25 | 2008-08-25 | Attapulgite lupulus anti-dandruff shampoo |
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| CN101347392A true CN101347392A (en) | 2009-01-21 |
| CN101347392B CN101347392B (en) | 2010-06-23 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468606A (en) * | 2017-08-02 | 2017-12-15 | 上海宏度精细化工有限公司 | One kind is without silicon beer shampoo and preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616632A (en) * | 2003-11-11 | 2005-05-18 | 刘秀珍 | Method for producing high efficiency detergent |
| CN100366236C (en) * | 2006-03-07 | 2008-02-06 | 许盛英 | Attapulgite sea salt health-care bathing powder |
| CN100549108C (en) * | 2007-12-28 | 2009-10-14 | 江苏南大紫金科技集团有限公司 | Organic surface modifying method of attapulgite |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468606A (en) * | 2017-08-02 | 2017-12-15 | 上海宏度精细化工有限公司 | One kind is without silicon beer shampoo and preparation method |
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| CN101347392B (en) | 2010-06-23 |
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