CN101342133B - Concave-convex stick walnut shampoo - Google Patents
Concave-convex stick walnut shampoo Download PDFInfo
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- CN101342133B CN101342133B CN2008100218222A CN200810021822A CN101342133B CN 101342133 B CN101342133 B CN 101342133B CN 2008100218222 A CN2008100218222 A CN 2008100218222A CN 200810021822 A CN200810021822 A CN 200810021822A CN 101342133 B CN101342133 B CN 101342133B
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- attapulgite
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- semen juglandis
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Abstract
The invention discloses attapulgite walnut shampoo, which has the technical proposal that the attapulgite walnut shampoo is composed of modified pasty attapulgite clay, walnut mixed solution, walnut mixed powder, honey, dodecyl dimethyl betaine, lauryl diethanol amide, citric acid, nipagin methyl ester, nipagine propyl ester and deionized water. The attapulgite walnut shampoo has the manufacturing method of purification, sodium modification, acidification, feed proportioning, pulverization, pulverization and beating, stirring and mixing, grinding, high-speed stirring, emulsification, vacuum degassing and canning for obtaining the finished product of attapulgite walnut shampoo. The attapulgite walnut shampoo provides a plurality of water-soluble nutrient components for hair, and can deeply penetrate into hair bodies to moisturize and supple the hair so as to improve hair quality; the carefully stir-fried walnut powder provides essential unsaturated fatty acid for a human body to cause hair more black and bright. The attapulgite walnut shampoo is suitable for hairdressing and nursing.
Description
Technical field
The present invention relates to shampoo, be specifically related to a kind of concave-convex stick walnut shampoo.
Background technology
Shampoo is a kind of oil-in-water type product, is opaque emulsion form, and it is with its strong detergency, and has the effect of hair care hair care concurrently and very popular.
In recent years, the inherent quality of people's pay attention to day by day shampoo, particularly the zest to eyes and skin is little, and require the oils and fats of shampoo removal skin within reason and hair, relatively gentleer to skin and mucosa, shampoo can impel hair soft and high resilience, and can increase the gloss of hair and be easy to rinsing.A people's hair withered and flourishing reflects the nutriture of human body to a certain extent.Remove the physiological aging and cause outside the variation of hair, it is generally acknowledged that hair is dense, pitch-black, glossy, explanation is in a good state of nutrition; Otherwise hair is sparse, withered and yellow, matt, and comes off in a large number, fractures, and then is the not good enough performance of nutrition.The trophic factor relevant with hair removed outside energy, protein, the vitamin, also has a factor that can not be ignored---trace element.
Gong Ying shampoo is synthetic with industrial chemicals mostly in the market, is difficult to satisfy the demands of consumers, and improper use also can cause bad phenomenon generations such as the dry bifurcated of hair, easily broken, curling and scalp allergy.
Chinese patent publication number CN1021385, open day is on October 12nd, 1988, name is called " a kind of highly effective liquid detergent and production method ", discloses " a kind of high-efficient washing spirit that is used for the sanitary purpose washing aspect of being made special auxiliary agent by inorganic mineral raw material bentonite and attapulgite.It is to make anion surfactant by preparing a certain amount of sodium lauryl sulphate, and CMC makes thickening, stabilizing agent, and lanoline is made conditioner and a certain amount of bentonite and attapulgite and made special auxiliary agent, spice, pigment and mix through heated and stirred.The present invention is cheap, and its cost of material only is about 75% of general shampoo and a shampoo paste.Strong detergency, consumption are few, nontoxic.”
The weak point of above-mentioned patent is not select for use in this technology to make special auxiliary agent through the inorganic mineral raw material bentonite and the attapulgite of purifying and modification is handled, and its dispersibility and suspendability are all poor, therefore can have influence on the product quality of highly effective liquid detergent.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of concave-convex stick walnut shampoo is provided.
Concave-convex stick walnut shampoo is made up of modified cream attapulgite clay, Semen Juglandis mixed liquor, Semen Juglandis mixed powder, Mel, dodecyldimethylammonium hydroxide inner salt, lauroyl diethanolamine, citric acid, methyl hydroxybenzoate, propylparaben and deionized water.
The production method of concave-convex stick walnut shampoo is that purification, sodium, acidify, batching, pulverizing, pulverizing are pulled an oar, mixed, grinding, high-speed stirred, emulsifying, vacuum outgas, cannedly be the finished product of concave-convex stick walnut shampoo.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m
2More than/the g.Use " wet beneficiation craft of attapulgite " and " attapulgite ore pul making production technology ", the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of attapulgite sludge slurry; Through the lip lipstick attapulgite clay after sodium processing and the acidification, it is the special good natural magnesium aluminium silicate gel of a kind of thixotropy and gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Semen Juglandis contains mineral and the essential unsaturated fatty acids of human nutrition such as more protein, vitamin E, calcium, phosphorus, zinc, manganese, chromium, and energy skin whitening, moist hair and increase elasticity make submissive, the good combing of hair.
Contain in the Semen pini koraiensis than polyunsaturated fatty acid, high quality protein, multivitamin and mineral, help nourishing hair, reduce the dry bifurcated of hair and fracture.
Nutritional labelings such as Semen Armeniacae Amarum rich in proteins, fat, saccharide, carotene, vitamin and calcium, phosphorus, ferrum, Semen Armeniacae Amarum can provide desired nutritional to hair, makes the more pitch-black light of healthy hair.
Semen arachidis hypogaeae contains amounts of protein, and particularly the content of unsaturated fatty acid is very high, also contains vitamin E and zinc, makes that hair obtains further moistening.
Plurality of enzymes that contains in the Mel and mineral can strengthen the metabolism ability of hair, use the Mel hair conditioning to play and moisten and Nutrition, make hair light and high resilience.
Dodecyldimethylammonium hydroxide inner salt all has advantages of excellent stability under acidity and alkali condition, the detergency of its aqueous solution, foaming characteristic and permeability are all fine, anti-hard water, biological degradability is good, little to skin irritation, the performance gentleness, compatibility is good, also has good stain removal bactericidal, flexibility and antistatic behaviour.
Lauroyl diethanolamine has good foaming characteristic, stability, thickening property, permeability and washing performance, and is good with other active matter compatibilities, is a kind of foam stabiliser preferably.
Citric acid has gentle frank tart flavour, can improve and adjust the pH value of shampoo, improves the performance of surfactant.
Methyl hydroxybenzoate has the broad-spectrum antibacterial effect, to Gram-positive, and negative bacteria, yeast and mycete have very strong inhibitory action, and the low and safety economy of working concentration uses effect duration long.Methyl hydroxybenzoate is compatible with various chemical substances easily, and the composite use of methyl hydroxybenzoate and propylparaben is to reach better antiseptic effect.
The present invention is achieved by following technical proposals:
1, the batching of concave-convex stick walnut shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30~60%, Semen Juglandis mixed liquor 10~45%, Semen Juglandis mixed powder 5~25%, Mel 0.5~5%, dodecyldimethylammonium hydroxide inner salt 0.5~8%, lauroyl diethanolamine 0.5~10%, citric acid 0.01~1%, methyl hydroxybenzoate 0.05~0.5%, propylparaben 0.05~0.5% and deionized water 2~40%.
Described modified cream attapulgite clay is on attapulgite ore pul making production technology basis, and attapulgite sludge slurry is carried out sodium processing, acidification, washing and sieve decontamination, and the mud of process post precipitation is modified cream attapulgite clay.
Attapulgite ore pul making production technology is: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is attapulgite sludge slurry finished product.
Above-mentioned production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15~35% and water 65~85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1~7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95~99.5% and sodium hydroxide 0.5~5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1~3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92~99.5% after the sodium and concentration are 98% sulphuric acid 0.5~8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25~65% and water 35~75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5~40% and water 60~95%.
The pH value of the immersion water of emitting is neutral meta-acid, can be used to produce the raw material of transparent shampoo.
The batching of described Semen Juglandis mixed liquor is made up of following component by weight percentage: Semen Juglandis 5~45%, Semen pini koraiensis 2~35%, Semen arachidis hypogaeae 2~25%, Semen Armeniacae Amarum 1~20% and water 2~80%; The preparation method of Semen Juglandis mixed liquor: 1. earlier Semen Juglandis, Semen pini koraiensis, Semen arachidis hypogaeae and Semen Armeniacae Amarum are put respectively and boiled 1~5 minute in the boiling water, pull out after the little wrinkle of peel, immerse again and slough peel in the cold water; 2. carry out steaming and decocting with adding in the rustless steel container after the batch mixes of Semen Juglandis mixed liquor, digestion time was controlled at 1~4 hour; 3. the compound after the steaming and decocting is pulverized making beating, the colloidal liquid after the making beating is the Semen Juglandis mixed liquor, and Semen Juglandis mixed liquor fineness of the particles is less than 0.074 millimeter;
The batching of described Semen Juglandis mixed powder is made up of following component by weight percentage: Semen Juglandis 35~65%, Semen pini koraiensis 10~35%, Semen arachidis hypogaeae 5~25% and Semen Armeniacae Amarum 3~20%, the preparation method of Semen Juglandis mixed powder: 1. the batch mixes with Semen Juglandis, Semen pini koraiensis, Semen arachidis hypogaeae and Semen Armeniacae Amarum is placed in the frying pan, heat with slow fire, stir-fry to surface is little yellow, 2. the compound after the parch is pulverized, powder after the pulverizing is the Semen Juglandis mixed powder, and Semen Juglandis mixed powder fineness of the particles is less than 0.074 millimeter.
2, the production method of concave-convex stick walnut shampoo: 1. carry out stirring at low speed in the batching adding blender with concave-convex stick walnut shampoo, mix the back and be the mixture of concave-convex stick walnut shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick walnut shampoo.
Concave-convex stick walnut shampoo uses modified cream attapulgite clay to be primary raw material, does not need to add in addition thickening agent and wetting agent, not only can improve the quality of shampoo, can also reduce production costs greatly.
Behind the processing of attapulgite sludge slurry process sodium, acidification, washing and the sieve decontamination, lip lipstick attapulgite clay becomes a kind of thixotropy and the special good natural magnesium aluminium silicate gel of gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
The Semen Juglandis mixed liquor can provide water miscible multiple nutritional components to hair, permeable dry deep moisturizing and submissive, to improve hair quality; The Semen Juglandis mixed powder of parch can provide human nutrition essential unsaturated fatty acid to hair meticulously, makes the more pitch-black light of healthy hair.
Concave-convex stick walnut shampoo is the auxotype shampoo, can provide desired nutritional to hair, makes the more pitch-black light of healthy hair, makes that hair obtains further moistening, and strengthens the elasticity and the toughness of hair.People are in the hair washing process, concave-convex stick walnut shampoo has exquisiteness and abundant foam, not only can make hair well absorb nutrition in the concave-convex stick walnut shampoo, relatively gentleer to eyes, hair and skin, nonirritant, and concave-convex stick walnut shampoo can also adsorb and remove foreign material such as sweat mixed with dirt on the hair, dust, microorganism, dandruff, abnormal flavour, the cleaning of maintenance scalp and hair and attractive in appearance, be easy to carry out rinsing after using the concave-convex stick walnut shampoo hair washing, impel hair softness Paint Gloss.
Concave-convex stick walnut shampoo is applicable to the hair caring nursing.
The specific embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of concave-convex stick walnut shampoo is made up of following component by weight percentage: modified cream attapulgite clay 35%, Semen Juglandis mixed liquor 24%, Semen Juglandis mixed powder 10%, Mel 3%, dodecyldimethylammonium hydroxide inner salt 4.4%, lauroyl diethanolamine 3%, citric acid 0.4%, methyl hydroxybenzoate 0.15%, propylparaben 0.05% and deionized water 20%.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 30% and water 70%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 3 days through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 98% and sodium hydroxide 2%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 2 days through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 97% after the sodium and concentration are 98% sulphuric acid 3%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 40 and water 60% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30% and water 70%.
The batching of described Semen Juglandis mixed liquor is made up of following component by weight percentage: Semen Juglandis 15%, Semen pini koraiensis 6%, Semen arachidis hypogaeae 5%, Semen Armeniacae Amarum 2% and water 72%; The preparation method of Semen Juglandis mixed liquor: 1. earlier Semen Juglandis, Semen pini koraiensis, Semen arachidis hypogaeae and Semen Armeniacae Amarum are put respectively and boiled 2 minutes in the boiling water, pull out after the little wrinkle of peel, immerse again and slough peel in the cold water; 2. carry out steaming and decocting with adding in the rustless steel container after the batch mixes of Semen Juglandis mixed liquor, digestion time was controlled at 2 hours; 3. the compound after the steaming and decocting is pulverized making beating, the colloidal liquid after the making beating is the Semen Juglandis mixed liquor, and Semen Juglandis mixed liquor fineness of the particles is less than 0.074 millimeter;
The batching of described Semen Juglandis mixed powder is made up of following component by weight percentage: Semen Juglandis 50%, Semen pini koraiensis 25%, Semen arachidis hypogaeae 15% and Semen Armeniacae Amarum 10%, the preparation method of Semen Juglandis mixed powder: 1. the batch mixes with Semen Juglandis, Semen pini koraiensis, Semen arachidis hypogaeae and Semen Armeniacae Amarum is placed in the frying pan, heat with slow fire, stir-fry to surface is little yellow, 2. the compound after the parch is pulverized, powder after the pulverizing is the Semen Juglandis mixed powder, and Semen Juglandis mixed powder fineness of the particles is less than 0.074 millimeter.
2, the production method of concave-convex stick walnut shampoo: 1. carry out stirring at low speed in the batching adding blender with concave-convex stick walnut shampoo, mix the back and be the mixture of concave-convex stick walnut shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick walnut shampoo.
Claims (1)
1. concave-convex stick walnut shampoo, it is characterized in that the batching of concave-convex stick walnut shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30~60%, Semen Juglandis mixed liquor 10~45%, Semen Juglandis mixed powder 5~25%, Mel 0.5~5%, dodecyldimethylammonium hydroxide inner salt 0.5~8%, lauroyl diethanolamine 0.5~10%, citric acid 0.01~1%, methyl hydroxybenzoate 0.05~0.5%, propylparaben 0.05~0.5% and deionized water 2~40%;
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15~35% and water 65~85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1~7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95~99.5% and sodium hydroxide 0.5~5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1~3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92~99.5% after the sodium and concentration are 98% sulphuric acid 0.5~8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25~65% and water 35~75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5~40% and water 60~95%;
The batching of described Semen Juglandis mixed liquor is made up of following component by weight percentage: Semen Juglandis 5~45%, Semen pini koraiensis 2~35%, Semen arachidis hypogaeae 2~25%, Semen Armeniacae Amarum 1~20% and water 2~80%; The preparation method of Semen Juglandis mixed liquor: 1. earlier Semen Juglandis, Semen pini koraiensis, Semen arachidis hypogaeae and Semen Armeniacae Amarum are put respectively and boiled 1~5 minute in the boiling water, pull out after the little wrinkle of peel, immerse again and slough peel in the cold water; 2. carry out steaming and decocting with adding in the rustless steel container after the batch mixes of Semen Juglandis mixed liquor, digestion time was controlled at 1~4 hour; 3. the compound after the steaming and decocting is pulverized making beating, the colloidal liquid after the making beating is the Semen Juglandis mixed liquor, and Semen Juglandis mixed liquor fineness of the particles is less than 0.074 millimeter;
The batching of described Semen Juglandis mixed powder is made up of following component by weight percentage: Semen Juglandis 35~65%, Semen pini koraiensis 10~35%, Semen arachidis hypogaeae 5~25% and Semen Armeniacae Amarum 3~20%, the preparation method of Semen Juglandis mixed powder: 1. the batch mixes with Semen Juglandis, Semen pini koraiensis, Semen arachidis hypogaeae and Semen Armeniacae Amarum is placed in the frying pan, heat with slow fire, stir-fry to surface is little yellow, 2. the compound after the parch is pulverized, powder after the pulverizing is the Semen Juglandis mixed powder, and Semen Juglandis mixed powder fineness of the particles is less than 0.074 millimeter.
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CN1743442A (en) * | 2005-09-26 | 2006-03-08 | 江南大学 | Method for synthesizing washing adjuvant using concave-convex rod day |
CN1850026A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed rod medicinal health-care bathing-mud powder |
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CN1743442A (en) * | 2005-09-26 | 2006-03-08 | 江南大学 | Method for synthesizing washing adjuvant using concave-convex rod day |
CN1850026A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed rod medicinal health-care bathing-mud powder |
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