CN101342125B - Attapulgite bead light shampoo - Google Patents
Attapulgite bead light shampoo Download PDFInfo
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- CN101342125B CN101342125B CN2008100218275A CN200810021827A CN101342125B CN 101342125 B CN101342125 B CN 101342125B CN 2008100218275 A CN2008100218275 A CN 2008100218275A CN 200810021827 A CN200810021827 A CN 200810021827A CN 101342125 B CN101342125 B CN 101342125B
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- attapulgite
- shampoo
- pearlescent
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- sludge slurry
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Abstract
The invention discloses attapulgite pearlescent shampoo, which has the technical proposal that the attapulgite pearlescent shampoo is composed of modified pasty attapulgite clay, orange peel, olive oil, glycol distearate, lauryl diethanol amide, cocamidopropyl betaine, citric acid, nipagin methyl ester, nipagine propyl ester and deionized water. The attapulgite pearlescent shampoo has the manufacturing method of purification, sodium modification, acidification, feed proportioning, pulverization and beating, heating, grinding, high-speed stirring, emulsification, vacuum degassing and canning for obtaining the finished product of the attapulgite pearlescent shampoo. The attapulgite pearlescent shampoo is the yellowish nontransparent emulsion shampoo, has obvious pearlescent color and more strong pearlescent sense during vibration, and has the characteristics of no break of milk, no separation, invariant color and no disappearance of the pearlescent color. The attapulgite pearlescent shampoo is suitable for hairdressing and nursing.
Description
Technical field
The present invention relates to shampoo, be specifically related to a kind of concave-convex stick bead light shampoo.
Background technology
Shampoo is a kind of oil-in-water type product, be opaque emulsion form, it is with its strong detergency, and have the effect of hair care hair care concurrently and very popular, bead light shampoo has a kind of exhilarating pearly luster, consumer there is bigger captivation, in producing the bead light shampoo process, because the selection of formula material and manufacturing condition is different, can cause pearly-lustre normally not separate out in heating with in stirring, cause the pearling agent separation and contain oarse-grained inhomogeneous appearance, making the pearly-lustre chap influences pearl effect.
Chinese patent publication number CN1021385, open day is on October 12nd, 1988, name is called " a kind of highly effective liquid detergent and production method ", discloses " a kind of high-efficient washing spirit that is used for the sanitary purpose washing aspect of being made special auxiliary agent by inorganic mineral raw material bentonite and attapulgite.It is to make anion surfactant by preparing a certain amount of sodium lauryl sulphate, and CMC makes thickening, stabilizing agent, and lanoline is made conditioner and a certain amount of bentonite and attapulgite and made special auxiliary agent, spice, pigment and mix through heated and stirred.The present invention is cheap, and its cost of material only is about 75% of general shampoo and a shampoo paste.Strong detergency, consumption are few, nontoxic.”
The weak point of above-mentioned patent is not select for use in this technology to make special auxiliary agent through the inorganic mineral raw material bentonite and the attapulgite of purifying and modification is handled, and its dispersibility and suspendability are all poor, therefore can have influence on the product quality of highly effective liquid detergent.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of concave-convex stick bead light shampoo is provided.
Concave-convex stick bead light shampoo is made up of modified cream attapulgite clay, Citrus pericarp, olive oil, Ethylene Glycol Distearate, lauroyl diethanolamine, cocamido propyl betaine, citric acid, methyl hydroxybenzoate, propylparaben and deionized water.
The production method of concave-convex stick bead light shampoo is purification, sodium, acidify, batching, pulverizing making beating, heating, grinding, high-speed stirred, emulsifying, vacuum outgas, cannedly is the finished product of concave-convex stick bead light shampoo.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m
2More than/the g.Use " wet beneficiation craft of attapulgite " and " attapulgite ore pul making production technology ", the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of attapulgite sludge slurry; Be stained with through the paste attapulgite after sodium processing and the acidification, it is the special good natural magnesium aluminium silicate gel of a kind of thixotropy and gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Citrus pericarp contains more crude protein, crude fat and cellulose, also contains various trace elements such as ferrum, manganese, zinc; Citrus pericarp is orange-yellow, is natural flavochrome, and citrus oils is a kind of volatile aromatic oil, be present in the pericarp membrane, contain in the Citrus pericarp, have good gelation and emulsion stability up to the pectin more than 15%, the Citrus pericarp that nothing is gone mouldy is cleaned with clear water, and it is standby to drain chopping.
Olive oil contains abundant unsaturated fatty acid and vitamin E, be easy to by skin absorbs, moisten nutrition skin matter, make skin gloss exquisiteness and high resilience, blood circulation promoting and skin metabolism, salubrious nature does not have greasy feeling extremely, bright and clean skin, bright healthy hair and slow down aging are the cosmetic good merchantable brands of pure natural.
Ethylene Glycol Distearate is used in the liquid scrubbing product can produce tangible pearl effect, and can increase the viscosity of product, also has skin care, hair care hair care and antistatic property.Good with the surfactant intermiscibility of other type, and can embody its stable pearl effect and thickening conditioning functions, non-stimulated to skin, to the hair not damaged, the pearly-lustre of generation is stronger.
Lauroyl diethanolamine has good foaming characteristic, stability, thickening property, permeability and washing performance, and is good with other active matter compatibilities, is a kind of foam stabiliser preferably.
Cocamido propyl betaine is a kind of amphoteric surfactant of gentleness, and to skin, non-stimulated, the no anaphylactic reaction of eye mucosa, its foam stabilization, exquisiteness can improve material body viscosity, and thickening effect is obvious; Having flexibility, bactericidal properties and antistatic property, is excellent hair conditioner.
Citric acid has gentle frank tart flavour, can improve and adjust the pH value of shampoo, improves the performance of surfactant.
Methyl hydroxybenzoate has the broad-spectrum antibacterial effect, to Gram-positive, and negative bacteria, yeast and mycete have very strong inhibitory action, and the low and safety economy of working concentration uses effect duration long.Methyl hydroxybenzoate is compatible with various chemical substances easily, and the composite use of methyl hydroxybenzoate and propylparaben is to reach better antiseptic effect.
The present invention is achieved by following technical proposals:
1, the batching of concave-convex stick bead light shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, Citrus pericarp 10～45%, Ethylene Glycol Distearate 0.1～5%, lauroyl diethanolamine 0.1～5%, cocoyl CAB 0.1～5%, olive oil 0.1～5%, citric acid 0.01～3%, methyl hydroxybenzoate 0.05～0.5%, propylparaben 0.05～0.5% and deionized water 10～40%.
Described modified cream attapulgite clay is on attapulgite ore pul making production technology basis, and attapulgite sludge slurry is carried out sodium processing, acidification, washing and sieve decontamination, and the mud of process post precipitation is modified cream attapulgite clay.
Attapulgite ore pul making production technology is: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is attapulgite sludge slurry finished product.
Above-mentioned production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite is stained with 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%.
2, the production method of concave-convex stick bead light shampoo: 1. the batching adding of concave-convex stick bead light shampoo being pulverized in the beater and pulverize, is the mixture of concave-convex stick bead light shampoo behind the pulverizing making beating mix homogeneously; 2. the mixture that 1. step is obtained is heated to 65～75 ℃ earlier, imports to grind in the multi-functional colloid mill to be pasty mixture again, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick bead light shampoo.
Concave-convex stick bead light shampoo uses modified cream attapulgite clay to be primary raw material, does not need to add in addition thickening agent and wetting agent, not only can improve the quality of shampoo, can also reduce production costs greatly.
Behind the processing of attapulgite sludge slurry process sodium, acidification, washing and the sieve decontamination, lip lipstick attapulgite clay becomes a kind of thixotropy and the special good natural magnesium aluminium silicate gel of gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Concave-convex stick bead light shampoo is a kind of faint yellow opaque emulsion form shampoo, and tangible pearly-lustre color is arranged, during vibration the pearly-lustre sense stronger, the characteristics that have breakdown of emulsion not, do not separate, invariant color and pearly-lustre do not disappear.Concave-convex stick bead light shampoo energy blood circulation promoting moistens the scalp soften cuticle, and the toughness of enhancing hair makes hair become soft, smooth and maintenance healthy hair water moistens glossy.
The concave-convex stick bead light shampoo safety non-toxic, has exquisiteness and abundant foam, not only can make hair well absorb nutrition in the concave-convex stick bead light shampoo, relatively gentleer to eyes, hair and skin, nonirritant, and concave-convex stick bead light shampoo can also adsorb and remove foreign material such as sweat mixed with dirt on the hair, dust, microorganism, dandruff, abnormal flavour, the cleaning of maintenance scalp and hair and attractive in appearance, be easy to carry out rinsing after using the concave-convex stick bead light shampoo hair washing, impel hair softness Paint Gloss.
Concave-convex stick bead light shampoo is applicable to the hair caring nursing.
The specific embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of concave-convex stick bead light shampoo is made up of following component by weight percentage: modified cream attapulgite clay 35%, Citrus pericarp 24%, Ethylene Glycol Distearate 3%, lauroyl diethanolamine 2.5%, cocoyl CAB 1.5%, olive oil 1.5%, citric acid 0.3%, methyl hydroxybenzoate 0.15%, propylparaben 0.05% and deionized water 32%.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 30% and water 70%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 3 days through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 98% and sodium hydroxide 2%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 2 days through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 97% after the sodium and concentration are 98% sulphuric acid 3%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 40 and water 60% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30% and water 70%.
2, the production method of concave-convex stick bead light shampoo: 1. the batching adding of concave-convex stick bead light shampoo being pulverized in the beater and pulverize, is the mixture of concave-convex stick bead light shampoo behind the pulverizing making beating mix homogeneously; 2. the mixture that 1. step is obtained is heated to 70 ℃ earlier, imports to grind in the multi-functional colloid mill to be pasty mixture again, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick bead light shampoo.
Claims (2)
1. concave-convex stick bead light shampoo, it is characterized in that the batching of concave-convex stick bead light shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, Citrus pericarp 10～45%, Ethylene Glycol Distearate 0.1～5%, lauroyl diethanolamine 0.1～5%, cocamido propyl betaine 0.1～5%, olive oil 0.1～5%, citric acid 0.01～3%, methyl hydroxybenzoate 0.05～0.5%, propylparaben 0.05～0.5% and deionized water 10～40%;
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%.
2. the production method of a kind of concave-convex stick bead light shampoo according to claim 1, it is characterized in that, 1. the batching adding of concave-convex stick bead light shampoo being pulverized in the beater and pulverize, is the mixture of concave-convex stick bead light shampoo behind the pulverizing making beating mix homogeneously; 2. the mixture that 1. step is obtained is heated to 65～75 ℃ earlier, imports to grind in the multi-functional colloid mill to be pasty mixture again, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick bead light shampoo.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2008100218275A CN101342125B (en) | 2008-08-25 | 2008-08-25 | Attapulgite bead light shampoo |
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| CN2008100218275A CN101342125B (en) | 2008-08-25 | 2008-08-25 | Attapulgite bead light shampoo |
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| CN101342125B true CN101342125B (en) | 2010-06-23 |
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| CN2008100218275A Expired - Fee Related CN101342125B (en) | 2008-08-25 | 2008-08-25 | Attapulgite bead light shampoo |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106924062A (en) * | 2017-04-11 | 2017-07-07 | 安徽省明美矿物化工有限公司 | A kind of shampoo containing attapulgite clay and preparation method thereof |
| CN107496337A (en) * | 2017-10-10 | 2017-12-22 | 广西三椿生物科技有限公司 | A kind of submissive tough profit hair agent and preparation method |
Citations (4)
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| CN1850029A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed-rod Chinese medicine-mud mask |
| CN1850026A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed rod medicinal health-care bathing-mud powder |
| CN1899256A (en) * | 2006-07-24 | 2007-01-24 | 重庆灵方生物技术有限公司 | Rice vinegar shampoo |
| CN1965783A (en) * | 2006-10-30 | 2007-05-23 | 云南龙润药业有限公司 | Scalp care hair shampoo and preparation method thereof |
-
2008
- 2008-08-25 CN CN2008100218275A patent/CN101342125B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1850029A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed-rod Chinese medicine-mud mask |
| CN1850026A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed rod medicinal health-care bathing-mud powder |
| CN1899256A (en) * | 2006-07-24 | 2007-01-24 | 重庆灵方生物技术有限公司 | Rice vinegar shampoo |
| CN1965783A (en) * | 2006-10-30 | 2007-05-23 | 云南龙润药业有限公司 | Scalp care hair shampoo and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| An Li et al.Studies on Poly(acrylic acid)/Attapulgite SuperabsorbentComposite. I. Synthesis and Characterization.Journal of Applied Polymer Science,92 3.2004,92(3),1596-1603. |
| An Li et al.Studies on Poly(acrylic acid)/Attapulgite SuperabsorbentComposite. I. Synthesis and Characterization.Journal of Applied Polymer Science,92 3.2004,92(3),1596-1603. * |
| 马玉恒等.凹凸棒土研究与应用进展.材料导报20 9.2006,20(9),43-46. |
| 马玉恒等.凹凸棒土研究与应用进展.材料导报20 9.2006,20(9),43-46. * |
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