CN101352401B - Attapulgite green tea shampoo - Google Patents
Attapulgite green tea shampoo Download PDFInfo
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- CN101352401B CN101352401B CN2008100218203A CN200810021820A CN101352401B CN 101352401 B CN101352401 B CN 101352401B CN 2008100218203 A CN2008100218203 A CN 2008100218203A CN 200810021820 A CN200810021820 A CN 200810021820A CN 101352401 B CN101352401 B CN 101352401B
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- attapulgite
- green tea
- shampoo
- hair
- sludge slurry
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Abstract
The invention discloses an attapulgite green tea shampoo which has the key points of the technical proposal that: the attapulgite green tea shampoo consists of modified pasty attapulgite clay, mixed green tea liquid, honey, dodecyl dimethyl lycine, lauroyl diethanolameine, citric acid, methylparaben, spectrum chemical and deionized water. The production method of the attapulgite green tea shampoo is that the finished product of the attapulgite green tea shampoo is obtained by purification, sodium treatment, acidification, blending, shattering and pulping, stirring and bending, grinding, stirring at high speed, emulsification, vacuum degassing and can pack. The attapulgite green tea shampoo can provide multiple water miscible nutrient contents for the hair, maintain the balance of grease secretion, and permeate into the deeper layer of the hair shaft for hydrating and being silky, thus improving the hair quality. After the attapulgite green tea shampoo is used on the hair, the hair is easy to rinse as well as more smooth and soft; the attapulgite green tea shampoo is applicable to hairdressing and maintaining.
Description
Technical field
The present invention relates to shampoo, be specifically related to a kind of attapulgite green tea shampoo.
Background technology
Shampoo is a kind of oil-in-water type product, is opaque emulsion form, and it is with its strong detergency, and has the effect of hair care hair care concurrently and very popular.
In recent years, the inherent quality of people's pay attention to day by day shampoo, particularly the zest to eyes and skin is little, and require the oils and fats of shampoo removal skin within reason and hair, relatively gentleer to skin and mucosa, shampoo can impel hair soft and high resilience, and can increase the gloss of hair and be easy to rinsing.
A people's hair withered and flourishing reflects the nutriture of human body to a certain extent.Remove the physiological aging and cause outside the variation of hair, it is generally acknowledged that hair is dense, pitch-black, glossy, explanation is in a good state of nutrition; Otherwise hair is sparse, withered and yellow, matt, and comes off in a large number, fractures, and then is the not good enough performance of nutrition.The trophic factor relevant with hair removed outside energy, protein, the vitamin, also has a factor that can not be ignored---trace element.
Gong Ying shampoo is synthetic with industrial chemicals mostly in the market, is difficult to satisfy the demands of consumers, and improper use also can cause bad phenomenon generations such as the dry bifurcated of hair, easily broken, curling and scalp allergy.
Chinese patent publication number CN 1349792, open day is on May 22nd, 2002, name is called " a kind of composite shampoo with tea component and preparation method thereof ", discloses " a kind of composite shampoo with tea component and preparation method thereof.Contain in the present composition outside water component (D) and other component (C), also contain Aqua Folium Camelliae sinensis component (A) and tea saponin component (B); The weight ratio of component (A) in described compositions is: 30-90%; The weight ratio of component (B) in described compositions is: 5-20%.Its manufacture method is: with component (A) and component (D) mix homogeneously, and then add component (C) and component (B), the limit edged stirs, and promptly obtains compositions of the present invention.Method technology of the present invention is simple, extraction ratio is high, cost is low, prevents that tea polyphenols is subjected to the chemical contamination in the leaching process, makes the plurality of active ingredients that contains in the compositions of the present invention in the Folium Camelliae sinensis, has radioprotective, anti-aging, hair caring, hair care effect.”
The weak point of above-mentioned patent is to be to select for use Aqua Folium Camelliae sinensis as primary raw material merely in this technology, can not satisfy the demand of consumer to the shampoo quality.
Chinese patent publication number CN1021385, open day is on October 12nd, 1988, name is called " a kind of highly effective liquid detergent and production method ", discloses " a kind of high-efficient washing spirit that is used for the sanitary purpose washing aspect of being made special auxiliary agent by inorganic mineral raw material bentonite and attapulgite.It is to make anion surfactant by preparing a certain amount of sodium lauryl sulphate, and CMC makes thickening, stabilizing agent, and lanoline is made conditioner and a certain amount of bentonite and attapulgite and made special auxiliary agent, spice, pigment and mix through heated and stirred.The present invention is cheap, and its cost of material only is about 75% of general shampoo and a shampoo paste.Strong detergency, consumption are few, nontoxic.”
The weak point of above-mentioned patent is not select for use in this technology to make special auxiliary agent through the inorganic mineral raw material bentonite and the attapulgite of purifying and modification is handled, and its dispersibility and suspendability are all poor, therefore can have influence on the product quality of highly effective liquid detergent.
Summary of the invention
The objective of the invention is to overcome weak point in the prior art, a kind of attapulgite green tea shampoo is provided.
Attapulgite green tea shampoo is made up of modified cream attapulgite clay, green tea mixed liquor, Mel, dodecyldimethylammonium hydroxide inner salt, lauroyl diethanolamine, citric acid, methyl hydroxybenzoate, propylparaben and deionized water.
The production method of attapulgite green tea shampoo is that purification, sodium, acidify, batching, pulverizing are pulled an oar, mixed, grinding, high-speed stirred, emulsifying, vacuum outgas, cannedly be the finished product of attapulgite green tea shampoo.
Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m
2More than/the g.Use " wet beneficiation craft of attapulgite " and " attapulgite ore pul making production technology ", the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of attapulgite sludge slurry; Through the lip lipstick attapulgite clay after sodium processing and the acidification, it is the special good natural magnesium aluminium silicate gel of a kind of thixotropy and gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
Fresh tea leaf in its is meant the tender tip of in time plucking on the Camellia sinensis of bud-leaf, contains nutrient substance such as rich vegetable protein matter, tea saponin and several amino acids, and scalp, hair are all had good nursing role.
Contain reseda flavin, inositol, Saponin, chlorogenic acid and saccharide, protein, the multiple chemical compound of vitamin and various trace elements in the Flos Lonicerae, remove impurity after the harvesting, it is standby to clean chopping.
Flos Chrysanthemi Indici all has stronger inhibitory action to most dermatophytess, staphylococcus aureus, dysentery bacterium, bacillus pyocyaneus and influenza virus etc., removes impurity after the harvesting, and it is standby to clean chopping.
Herba Menthae is a herbaceos perennial, and stem and leaf contains phytoprotein, multivitamin, Oleum menthae and trace element, can quicken the scalp blood circulation, and refreshment is removed impurity after tapping, and it is standby to clean chopping.
Plurality of enzymes that contains in the Mel and mineral can strengthen the metabolism ability of hair, use the Mel hair conditioning to play and moisten and Nutrition, make hair light and high resilience.
Dodecyldimethylammonium hydroxide inner salt all has advantages of excellent stability under acidity and alkali condition, the detergency of its aqueous solution, foaming characteristic and permeability are all fine, anti-hard water, biological degradability is good, little to skin irritation, the performance gentleness, compatibility is good, also has good stain removal bactericidal, flexibility and antistatic behaviour.
Lauroyl diethanolamine has good foaming characteristic, stability, thickening property, permeability and washing performance, and is good with other active matter compatibilities, is a kind of foam stabiliser preferably.
Citric acid has gentle frank tart flavour, can improve and adjust the pH value of shampoo, improves the performance of surfactant.
Methyl hydroxybenzoate has the broad-spectrum antibacterial effect, to Gram-positive, and negative bacteria, yeast and mycete have very strong inhibitory action, and the low and safety economy of working concentration uses effect duration long.Methyl hydroxybenzoate is compatible with various chemical substances easily, and the composite use of methyl hydroxybenzoate and propylparaben is to reach better antiseptic effect.
The present invention is achieved by following technical proposals:
1, the batching of attapulgite green tea shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, green tea mixed liquor 20～55%, Mel 0.5～5%, dodecyldimethylammonium hydroxide inner salt 0.5～8%, lauroyl diethanolamine 0.5～10%, citric acid 0.01～1%, methyl hydroxybenzoate 0.05～0.5%, propylparaben 0.05～0.5% and deionized water 2～40%.
Described modified cream attapulgite clay is on attapulgite ore pul making production technology basis, and attapulgite sludge slurry is carried out sodium processing, acidification, washing and sieve decontamination, and the mud of process post precipitation is modified cream attapulgite clay.
Attapulgite ore pul making production technology is: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is attapulgite sludge slurry finished product.
Above-mentioned production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%.
The pH value of the immersion water of emitting is neutral meta-acid, can be used to produce the raw material of transparent shampoo.
The batching of described green tea mixed liquor is made up of following component by weight percentage: fresh tea leaf in its 10～45%, Flos Lonicerae 5～35%, Flos Chrysanthemi Indici 2～25%, Herba Menthae 1～10% and water 2～60%; The preparation method of green tea mixed liquor: the fresh tea leaf in its after 1. will plucking is carried out steam beating, and vapor (steam) temperature is controlled at 100～110 ℃, and fixation time was controlled at 6～60 seconds; 2. the batching of green tea mixed liquor is pulverized making beating, the mixing material after the making beating is the green tea mixed liquor, and the fineness of the particles of green tea mixed liquor is less than 0.074 millimeter;
Steam beating is the high temperature hyther of utilizing in the steam, has destroyed the activation of enzyme in the fresh tea leaf in its, has stoped the Main Ingredients and Appearance in the Folium Camelliae sinensis---the enzymatic oxidation of Polyphenols, more reservation original various chemical constituents in the fresh Folium Camelliae sinensis, keep leaf color jade green.
2, the production method of attapulgite green tea shampoo: 1. carry out stirring at low speed in the batching adding blender with attapulgite green tea shampoo, mix the back and be the mixture of attapulgite green tea shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite green tea shampoo.
Attapulgite green tea shampoo uses modified cream attapulgite clay to be primary raw material, does not need to add in addition thickening agent and wetting agent, not only can improve the quality of shampoo, can also reduce production costs greatly.
Behind the processing of attapulgite sludge slurry process sodium, acidification, washing and the sieve decontamination, lip lipstick attapulgite clay becomes a kind of thixotropy and the special good natural magnesium aluminium silicate gel of gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.
The green tea mixed liquor can provide water miscible multiple nutritional components to hair, keeps the fat secretion balance, and permeable dry deep moisturizing and submissive is to improve hair quality.
Attapulgite green tea shampoo is the auxotype shampoo, can provide desired nutritional to hair, makes that hair obtains further moistening, and strengthens the elasticity and the toughness of hair.People are in the hair washing process, attapulgite green tea shampoo has exquisiteness and abundant foam, not only can make hair well absorb nutrition in the attapulgite green tea shampoo, relatively gentleer to eyes, hair and skin, nonirritant, and attapulgite green tea shampoo can also adsorb and remove foreign material such as sweat mixed with dirt on the hair, dust, microorganism, dandruff, abnormal flavour, the cleaning of maintenance scalp and hair and attractive in appearance, be easy to carry out rinsing after using the attapulgite green tea shampoo hair washing, impel hair softness Paint Gloss.
Attapulgite green tea shampoo is applicable to the hair caring nursing.
The specific embodiment
The invention will be further described below in conjunction with embodiment:
1, the batching of attapulgite green tea shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30%, green tea mixed liquor 40%, Mel 2%, dodecyldimethylammonium hydroxide inner salt 4%, lauroyl diethanolamine 3.5%, citric acid 0.3%, methyl hydroxybenzoate 0.15%, propylparaben 0.05% and deionized water 20%.
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 30% and water 70%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 3 days through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 98% and sodium hydroxide 2%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 2 days through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 97% after the sodium and concentration are 98% sulphuric acid 3%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 40 and water 60% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30% and water 70%.
The batching of described green tea mixed liquor is made up of following component by weight percentage: fresh tea leaf in its 25%, Flos Lonicerae 15%, Flos Chrysanthemi Indici 10%, Herba Menthae 5% and water 45%; The preparation method of green tea mixed liquor: the fresh tea leaf in its after 1. will plucking is carried out steam beating, and vapor (steam) temperature is controlled at 100～110 ℃, and fixation time was controlled at 40 seconds; 2. the batching of green tea mixed liquor is pulverized making beating, the mixing material after the making beating is the green tea mixed liquor, and the fineness of the particles of green tea mixed liquor is less than 0.074 millimeter.
2, the production method of attapulgite green tea shampoo: 1. carry out stirring at low speed in the batching adding blender with attapulgite green tea shampoo, mix the back and be the mixture of attapulgite green tea shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite green tea shampoo.
Claims (1)
1. attapulgite green tea shampoo, it is characterized in that the batching of attapulgite green tea shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, green tea mixed liquor 20～55%, Mel 0.5～5%, dodecyldimethylammonium hydroxide inner salt 0.5～8%, lauroyl diethanolamine 0.5～10%, citric acid 0.01～1%, methyl hydroxybenzoate 0.05～0.5%, propylparaben 0.05～0.5% and deionized water 2～40%;
The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%;
The batching of described green tea mixed liquor is made up of following component by weight percentage: fresh tea leaf in its 10～45%, Flos Lonicerae 5～35%, Flos Chrysanthemi Indici 2～25%, Herba Menthae 1～10% and water 2～60%; The preparation method of green tea mixed liquor: the fresh tea leaf in its after 1. will plucking is carried out steam beating, and vapor (steam) temperature is controlled at 100～110 ℃, and fixation time was controlled at 6～60 seconds; 2. the batching of green tea mixed liquor is pulverized making beating, the mixing material after the making beating is the green tea mixed liquor, and the fineness of the particles of green tea mixed liquor is less than 0.074 millimeter.
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| CN102319190B (en) * | 2011-01-18 | 2013-09-11 | 朱绍华 | Pure plant hair dyeing method for blackening white hairs and shampoos used before dyeing |
| CN105342896A (en) * | 2015-08-06 | 2016-02-24 | 铜陵百锐设备配件有限公司 | Rabbit hair care solution |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1850026A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed rod medicinal health-care bathing-mud powder |
| CN101234072A (en) * | 2008-01-31 | 2008-08-06 | 许盛英 | Method for producing attapulgitehoneysuckle flower toothpaste |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1850026A (en) * | 2006-03-07 | 2006-10-25 | 许盛英 | Embossed rod medicinal health-care bathing-mud powder |
| CN101234072A (en) * | 2008-01-31 | 2008-08-06 | 许盛英 | Method for producing attapulgitehoneysuckle flower toothpaste |
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