CN100584313C - Attapulgite black sesame shampoo - Google Patents

Abstract

The invention discloses attapulgite black sesame shampoo, which has the technical proposal that the attapulgite black sesame shampoo is composed of modified pasty attapulgite clay, black sesame paste, black date, fresh mulberry, honey, dodecyl dimethyl betaine, lauryl diethanol amide, citric acid, nipagin methyl ester, nipagine propyl ester and deionized water. The attapulgite black sesame shampoo has the manufacturing method of purification, sodium modification, acidification, feed proportioning, pulverization, pulverization and beating, stirring and mixing, grinding, high-speed stirring, emulsification, vacuum degassing and canning for obtaining the finished product of attapulgite black sesame shampoo. The attapulgite black sesame shampoo contains rich high-quality protein, unsaturated fatty acid and a plurality of mineral compositions such as calcium, phosphorus, iron, etc., repairs lipide and protein lost by damaged hair, supplements water for the hair, deeply moistens hair from inside to outside to cause the hair naturally black, bright and pliancy, and keeps the hair in health. The attapulgite black sesame shampoo is suitable for hairdressing and nursing.

Description

Concave-convex stick niger seed shampoo

Technical field

The present invention relates to shampoo, be specifically related to a kind of concave-convex stick niger seed shampoo.

Background technology

Shampoo is a kind of oil-in-water type product, is opaque emulsion form, and it is with its strong detergency, and has the effect of hair care hair care concurrently and very popular.

In recent years, the inherent quality of people's pay attention to day by day shampoo, particularly the zest to eyes and skin is little, and require the oils and fats of shampoo removal skin within reason and hair, relatively gentleer to skin and mucosa, shampoo can impel hair soft and high resilience, and can increase the gloss of hair and be easy to rinsing.A people's hair withered and flourishing reflects the nutriture of human body to a certain extent.Remove the physiological aging and cause outside the variation of hair, it is generally acknowledged that hair is dense, pitch-black, glossy, explanation is in a good state of nutrition; Otherwise hair is sparse, withered and yellow, matt, and comes off in a large number, fractures, and then is the not good enough performance of nutrition.The trophic factor relevant with hair removed outside energy, protein, the vitamin, also has a factor that can not be ignored---trace element.

Chinese patent publication number CN1097591, open day be January 25 nineteen ninety-five, is called " black sesame shampoo ", discloses that " black sesame shampoo is to be made of one-tenth branch such as natural plants Semen Sesami Nigrum, detergent, thickening foaming aids, penetrating agent.The maximum characteristics of this product are the medicinal efficacies that contain Semen Sesami Nigrum, can nourishing hairs, and promote the hair quality blackout fast long, can control again and shave one's head, give birth to the curative effect of alopecia and anti-early whitening of beard and hair, good combination property, can integrate hair washing, hair care, hair care, hair growth promoting, make things convenient for user to use, have no side effect again.”

The weak point of above-mentioned patent is that to select Oleum sesami in this technology merely for use be primary raw material, and its nutritional labeling can not well promote the hair quality blackout fast long.

Chinese patent publication number CN1021385, open day is on October 12nd, 1988, name is called " a kind of highly effective liquid detergent and production method ", discloses " a kind of high-efficient washing spirit that is used for the sanitary purpose washing aspect of being made special auxiliary agent by inorganic mineral raw material bentonite and attapulgite.It is to make anion surfactant by preparing a certain amount of sodium lauryl sulphate, and C M C makes thickening, stabilizing agent, and lanoline is made conditioner and a certain amount of bentonite and attapulgite and made special auxiliary agent, spice, pigment and mix through heated and stirred.The present invention is cheap, and its cost of material only is about 75% of general shampoo and a shampoo paste.Strong detergency, consumption are few, nontoxic.”

The weak point of above-mentioned patent is not select for use in this technology to make special auxiliary agent through the inorganic mineral raw material bentonite and the attapulgite of purifying and modification is handled, and its dispersibility and suspendability are all poor, therefore can have influence on the product quality of highly effective liquid detergent.

Summary of the invention

The objective of the invention is to overcome weak point in the prior art, a kind of concave-convex stick niger seed shampoo is provided.

Concave-convex stick niger seed shampoo is made up of modified cream attapulgite clay, black sesame paste, Semen Sesami Nigrum powder, Fructus Jujubae, bright Fructus Mori, Mel, dodecyldimethylammonium hydroxide inner salt, lauroyl diethanolamine, citric acid, methyl hydroxybenzoate, propylparaben and deionized water.

The production method of concave-convex stick niger seed shampoo is that purification, sodium, acidify, batching, pulverizing, pulverizing are pulled an oar, mixed, grinding, high-speed stirred, emulsifying, vacuum outgas, cannedly be the finished product of concave-convex stick niger seed shampoo.

Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m ²More than/the g.Use " wet beneficiation craft of attapulgite " and " attapulgite ore pul making production technology ", the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of attapulgite sludge slurry; Through the lip lipstick attapulgite clay after sodium processing and the acidification, it is the special good natural magnesium aluminium silicate gel of a kind of thixotropy and gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.

Semen Sesami Nigrum contains the required essential fatty acid of natural on-off cycles of hair growth, protein, vitamin and aminoacid, and Semen Sesami Nigrum also contains calcium, phosphorus, the multiple trace mineral of ferrum, helps the maintenance hair, and anti-loss and poliosis makes hair keep pitch-black beautiful.It is the highest in all foods that Semen Sesami Nigrum contains vitamin E, and vitamin E mainly is an antioxidant, can defying age.

Semen sojae atricolor contains multiple trace minerals such as abundant unsaturated fatty acid, carotene, vitamin, calcium, phosphorus, ferrum.

The nutritive value of fructus zizaniae caduciflorae contains multivitamin, aminoacid, zinc, ferrum, molybdenum and selenium and other trace elements than general rice height.

Auricularia contains protein, fat, lecithin, sphingomyelins, multivitamin, and inorganic constituents such as calcium, phosphorus, ferrum; Colloid in the Auricularia helps the normal growth of hair, promotes that hair is pitch-black glossy.

Contain protein, fat, saccharide, multivitamin, pectin and mineral etc. in the seedless Fructus Jujubae.With contain vitamin C and calcareous, irony is maximum, and the effect of immunity in the extremely strong enhancing body is arranged, Fructus Jujubae has strengthens the effect of enriching blood, and makes hair keep pitch-black beautiful.

Bright Fructus Mori rich in proteins, multiple human body essential amino acid, fructose, glucose, carotene, vitamin also contain ferrum, calcium and selenium and other trace elements, and bright juice of Fructus Mori can be by improving the effect that immune function plays antioxidation, skin moistening hair caring.

Plurality of enzymes that contains in the Mel and mineral can strengthen the metabolism ability of hair, use the Mel hair conditioning to play and moisten and Nutrition, make hair light and high resilience.

Dodecyldimethylammonium hydroxide inner salt all has advantages of excellent stability under acidity and alkali condition, the detergency of its aqueous solution, foaming characteristic and permeability are all fine, anti-hard water, biological degradability is good, little to skin irritation, the performance gentleness, compatibility is good, also has good stain removal bactericidal, flexibility and antistatic behaviour.

Lauroyl diethanolamine has good foaming characteristic, stability, thickening property, permeability and washing performance, and is good with other active matter compatibilities, is a kind of foam stabiliser preferably.

Citric acid has gentle frank tart flavour, can improve and adjust the pH value of shampoo, improves the performance of surfactant.

Methyl hydroxybenzoate has the broad-spectrum antibacterial effect, to Gram-positive, and negative bacteria, yeast and mycete have very strong inhibitory action, and the low and safety economy of working concentration uses effect duration long.Methyl hydroxybenzoate is compatible with various chemical substances easily, and the composite use of methyl hydroxybenzoate and propylparaben is to reach better antiseptic effect.

The present invention is achieved by following technical proposals:

1, the batching of concave-convex stick niger seed shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, black sesame paste 10～45%, Semen Sesami Nigrum powder 5～25%, Fructus Jujubae 2～1O%, bright Fructus Mori 2～10%, Mel 0.5～5%, dodecyldimethylammonium hydroxide inner salt 0.5～8%, lauroyl diethanolamine 0.5～10%, citric acid 0.01～1%, methyl hydroxybenzoate 0.05～0.5%, propylparaben 0.05～0.5% and deionized water 2～40%.

Described modified cream attapulgite clay is on attapulgite ore pul making production technology basis, and attapulgite sludge slurry is carried out sodium processing, acidification, washing and sieve decontamination, and the mud of process post precipitation is modified cream attapulgite clay.

Attapulgite ore pul making production technology is: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is attapulgite sludge slurry finished product.

Above-mentioned production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.

The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%.

The pH value of the immersion water of emitting is neutral meta-acid, can be used to produce the raw material of transparent shampoo.

Described Fructus Jujubae is selected seedless Fructus Jujubae for use, and bright Fructus Mori is selected the sophisticated bright Fructus Mori of atropurpureus for use.

The batching of described black sesame paste is made up of following component by weight percentage: Semen Sesami Nigrum 30～65%, fructus zizaniae caduciflorae 5～30%, Semen sojae atricolor 2～25% and Auricularia 1～20%; The preparation method of black sesame paste: Semen Sesami Nigrum, fructus zizaniae caduciflorae, Semen sojae atricolor and Auricularia after 1. will screening are put respectively and are soaked 1～8 hour in the clear water; 2. steam in the rustless steel food steamer to thoroughly cooked adding after the batch mixes of black sesame paste; 3. the compound after will cooking is pulverized making beating, and the colloidal liquid after the making beating is a black sesame paste, and the black sesame paste fineness of the particles is less than 0.074 millimeter;

The batching of described Semen Sesami Nigrum powder is made up of following component by weight percentage: Semen Sesami Nigrum 45～65%, fructus zizaniae caduciflorae 10～45% and Semen sojae atricolor 5～30%, the preparation method of Semen Sesami Nigrum powder: 1. the batch mixes with Semen Sesami Nigrum, fructus zizaniae caduciflorae and Semen sojae atricolor is placed in the frying pan, with the slow fire heating, fry to savory; 2. the compound after will frying is pulverized, and the powder after the pulverizing is a Semen Sesami Nigrum powder, and the Semen Sesami Nigrum powder fineness of the particles is less than 0.074 millimeter.

2, the production method of concave-convex stick niger seed shampoo: 1. carry out stirring at low speed in the batching adding blender with concave-convex stick niger seed shampoo, mix the back and be the mixture of concave-convex stick niger seed shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick niger seed shampoo.

Concave-convex stick niger seed shampoo uses modified cream attapulgite clay to be primary raw material, does not need to add in addition thickening agent and wetting agent, not only can improve the quality of shampoo, can also reduce production costs greatly.

Behind the processing of attapulgite sludge slurry process sodium, acidification, washing and the sieve decontamination, lip lipstick attapulgite clay becomes a kind of thixotropy and the special good natural magnesium aluminium silicate gel of gumminess, it is neutral that pH value is, and the viscosity of attapulgite clay, expansion capacity, colloid index, whiteness, specific surface area, absorption property, suspensibility and dirt-removing power all are greatly improved.

Black sesame paste can provide water miscible multiple nutritional components to hair, permeable dry deep moisturizing and submissive, to improve hair quality; The Semen Sesami Nigrum powder of parch can provide human nutrition essential unsaturated fatty acid to hair meticulously, makes the more pitch-black light of healthy hair.

Concave-convex stick niger seed shampoo is the auxotype shampoo, helps the blood circulation in the scalp, promotes the vitality of hair, and the moist effect of correct initiation, prevents hair drying and embrittlement.The high quality protein that is rich in the concave-convex stick niger seed shampoo, unsaturated fatty acid and calcium, phosphorus, the multiple trace mineral of ferrum, repair lipid and protein that damaged hair ran off, keep the skin wet, deep layer is moistened healthy hair from the inside to the outside, make healthy hair pitch-black naturally, glossy submissive, keep healthy hair health.

People are in the hair washing process, concave-convex stick niger seed shampoo has exquisiteness and abundant foam, not only can make hair well absorb nutrition in the concave-convex stick niger seed shampoo, relatively gentleer to eyes, hair and skin, nonirritant, and concave-convex stick niger seed shampoo can also adsorb and remove foreign material such as sweat mixed with dirt on the hair, dust, microorganism, dandruff, abnormal flavour, the cleaning of maintenance scalp and hair and attractive in appearance, be easy to carry out rinsing after using the concave-convex stick niger seed shampoo hair washing, impel hair softness Paint Gloss.

Concave-convex stick niger seed shampoo is applicable to the hair caring nursing.

The specific embodiment

The invention will be further described below in conjunction with embodiment:

1, the batching of concave-convex stick niger seed shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30%, black sesame paste 20%, Semen Sesami Nigrum powder 10%, Fructus Jujubae 5%, bright Fructus Mori 4%, Mel 3%, dodecyldimethylammonium hydroxide inner salt 4%, lauroyl diethanolamine 3.5%, citric acid 0.3%, methyl hydroxybenzoate 0.15%, propylparaben 0.05% and deionized water 20%.

The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 30% and water 70%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 3 days through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 98% and sodium hydroxide 2%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 2 days through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 97% after the sodium and concentration are 98% sulphuric acid 3%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 40 and water 60% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30% and water 70%.

The batching of described black sesame paste is made up of following component by weight percentage: Semen Sesami Nigrum 55%, fructus zizaniae caduciflorae 25%, Semen sojae atricolor 15% and Auricularia 5%; The preparation method of black sesame paste: Semen Sesami Nigrum, fructus zizaniae caduciflorae, Semen sojae atricolor and the Auricularia after 1. will screening put respectively in the clear water and soaked 4 hours; 2. steam in the rustless steel food steamer to thoroughly cooked adding after the batch mixes of black sesame paste; 3. the compound after will cooking is pulverized making beating, and the colloidal liquid after the making beating is a black sesame paste, and the black sesame paste fineness of the particles is less than 0.074 millimeter;

The batching of described Semen Sesami Nigrum powder is made up of following component by weight percentage: Semen Sesami Nigrum 50%, fructus zizaniae caduciflorae 35% and Semen sojae atricolor 15%, the preparation method of Semen Sesami Nigrum powder: 1. the batch mixes with Semen Sesami Nigrum, fructus zizaniae caduciflorae and Semen sojae atricolor is placed in the frying pan, with the slow fire heating, fry to savory; 2. the compound after will frying is pulverized, and the powder after the pulverizing is a Semen Sesami Nigrum powder, and the Semen Sesami Nigrum powder fineness of the particles is less than 0.074 millimeter.

2, the production method of concave-convex stick niger seed shampoo: 1. carry out stirring at low speed in the batching adding blender with concave-convex stick niger seed shampoo, mix the back and be the mixture of concave-convex stick niger seed shampoo; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of concave-convex stick niger seed shampoo.

Claims (1)

1, a kind of concave-convex stick niger seed shampoo, it is characterized in that the batching of concave-convex stick niger seed shampoo is made up of following component by weight percentage: modified cream attapulgite clay 30～60%, black sesame paste 10～45%, Semen Sesami Nigrum powder 5～25%, Fructus Jujubae 2～10%, bright Fructus Mori 2～10%, Mel 0.5～5%, dodecyldimethylammonium hydroxide inner salt 0.5～8%, lauroyl diethanolamine 0.5～10%, citric acid 0.01～1%, methyl hydroxybenzoate 0.05～0.5%, propylparaben 0.05～0.5% and deionized water 2～40%;

The production technology of described modified cream attapulgite clay is: (1) selects for use attapulgite sludge slurry to be body material, and attapulgite sludge slurry is made up of following component by weight percentage: attapulgite clay 15～35% and water 65～85%; (2) sodium is handled: attapulgite sludge slurry is transported in the blender, stirs after adding sodium hydroxide, be transported in the sodium pond ageing 1～7 day through the attapulgite sludge slurry after stirring; The sodium batching is made up of following component by weight percentage: attapulgite sludge slurry 95～99.5% and sodium hydroxide 0.5～5%; (3) acidification: attapulgite sludge slurry after the sodium is transported in the blender, stirs after adding concentration and be 98% sulphuric acid, be transported in the acidification pool ageing 1～3 day through the attapulgite sludge slurry after stirring; The acidify batching is made up of following component by weight percentage: attapulgite sludge slurry 92～99.5% after the sodium and concentration are 98% sulphuric acid 0.5～8%; (4) washing and sieve decontamination: the slurry of the attapulgite sludge after the acidify is transported in the sedimentation tank, soaks again, dash with air pump and turn over, the sieve decontamination, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, and the mud of post precipitation is lip lipstick attapulgite clay; The washing batching is made up of following component by weight percentage: attapulgite sludge slurry 25～65% and water 35～75% after the acidify; Lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 5～40% and water 60～95%;

The batching of described black sesame paste is made up of following component by weight percentage: Semen Sesami Nigrum 30～65%, fructus zizaniae caduciflorae 5～30%, Semen sojae atricolor 2～25% and Auricularia 1～20%; The preparation method of black sesame paste: Semen Sesami Nigrum, fructus zizaniae caduciflorae, Semen sojae atricolor and Auricularia after 1. will screening are put respectively and are soaked 1～8 hour in the clear water; 2. steam in the rustless steel food steamer to thoroughly cooked adding after the batch mixes of black sesame paste; 3. the compound after will cooking is pulverized making beating, and the colloidal liquid after the making beating is a black sesame paste, and the black sesame paste fineness of the particles is less than 0.074 millimeter;

The batching of described Semen Sesami Nigrum powder is made up of following component by weight percentage: Semen Sesami Nigrum 45～65%, fructus zizaniae caduciflorae 10～45% and Semen sojae atricolor 5～30%, the preparation method of Semen Sesami Nigrum powder: 1. the batch mixes with Semen Sesami Nigrum, fructus zizaniae caduciflorae and Semen sojae atricolor is placed in the frying pan, with the slow fire heating, fry to savory; 2. the compound after will frying is pulverized, and the powder after the pulverizing is a Semen Sesami Nigrum powder, and the Semen Sesami Nigrum powder fineness of the particles is less than 0.074 millimeter.