CN100528133C - Method for producing attapulgite shiny pricklyash toothpaste - Google Patents

Abstract

The invention discloses a method for producing attapulgite pricklyash root toothpaste, which has the following key points of the technical proposal: the ingredients is carried out the processes of proportioning, stirring at low speed, crushing and pulping, grinding, stirring at high speed, vacuum degassing and then is canned for obtaining the finished products of the attapulgite pricklyash root toothpaste. The attapulgite pricklyash root toothpaste is consisted of pasty attapulgite clay, fresh stems and leaves of the pricklyash root, sodium dodecyl sulfate, potassium sorbate, mint oil and demin-water. The attapulgite pricklyash root toothpaste is characterized by having clean, soft and smoothness, strong foaming power, good stability, being cool and refreshing, as well as that paste does not overflow out of the toothpaste, no water is separated, fragrance, color and luster are normal and no mark is left on slides. The attapulgite pricklyash root toothpaste is able to directly adsorb and clear away a plurality of offensive odor and tastes in mouth cavities, reduce dental plaque, prevent bleeding gum and has certain auxiliary effects for preventing mouth diseases. The production method is applicable to producing the attapulgite pricklyash root toothpaste, Chinese herbal toothpastes and other medicated toothpastes.

Description

The production method of attapulgite shiny pricklyash toothpaste

Technical field:

The present invention relates to toothpaste, be specifically related to a kind of production method of attapulgite shiny pricklyash toothpaste.

Background technology:

Chinese herbal medicine is abundant in the China source, and a lot of ancient prescription curative effects are all very definite, and toxic and side effects is littler than Western medicine, and common people also accept, so Chinese herbal medicine is preventing that the oral disease field has the excellent research DEVELOPMENT PROSPECT really.

Chinese herbal medicine adding ingredient in the toothpaste relates to processes such as Chinese herbal medicine collection, processing, effective ingredient refinement, and it has determined directly whether the elite composition that adds in the toothpaste can play a role.

The Chinese herbal medicine that is adopted in the Chinese herbal toothpaste is the Chinese herbal medicine finished product after drying mostly, also has the infusion method of employing to extract its soak or its concentrated solution, still contains a large amount of effective ingredient in the garbage behind the medicinal herb soak, causes bigger economic loss.

The abrasivus that Chinese herbal toothpaste is commonly used has calcium carbonate, calcium phosphate dibasic dihydrate, no hydration calcium hydrogen phosphate, calcium pyrophosphate, anhydride silica, aluminium hydroxide etc., because these abrasivus hardness height, granule is coarse, there is not stickiness, absorption property is poor, and life-time service easily causes wearing and tearing to the enamel of dental surface.

Summary of the invention:

The objective of the invention is to overcome weak point in the prior art, a kind of production method that contains the attapulgite shiny pricklyash toothpaste of fresh Radix Zanthoxyli stem and leaf is provided.

The production method of attapulgite shiny pricklyash toothpaste is, batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgas, canned be the finished product of attapulgite shiny pricklyash toothpaste.

Attapulgite shiny pricklyash toothpaste is made up of lip lipstick attapulgite clay, fresh Radix Zanthoxyli stem and leaf, sodium lauryl sulphate, potassium sorbate, Oleum menthae and deionized water.

Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m ²More than/the g, most cation, hydrone and a certain size organic molecule all can directly be adsorbed in the duct.

Use attapulgite ore pul making production technology, the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of lip lipstick attapulgite clay, have the characteristics of ultrafine dust, friction little, the no sand feeling of hardness and soft fine and smooth free from extraneous odour.

Lip lipstick attapulgite clay is through powerful stirring at a high speed, become the special good natural gelinite of a kind of thixotropy and gumminess, viscosity is up to more than the 10000mPas, absorption property and performance of keeping humidity have all obtained further raising, attapulgite clay after the high-speed stirred, total characteristic with abrasivus, adhesive and wetting agent, use lip lipstick attapulgite clay to produce toothpaste and do not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.

Radix Zanthoxyli is root or the branch and leaf of dicotyledon medicine rutaceae Radix Zanthoxyli, have dispel the wind, collateral dredging, detumescence, analgesic effect.Can gather and purchase the tender Radix Zanthoxyli stem and leaf of fresh matter annual May to October, and it is the effective ingredient that can make full use of Radix Zanthoxyli that the present invention adopts fresh Radix Zanthoxyli stem and leaf purpose, reduces pollution in the dry in the sun process, goes mouldy and production cost.

Sodium lauryl sulphate belongs to anion surfactant, and is soluble in water, and compatibility is good again with anion, nonionic, has good emulsifying, foaming, infiltration, decontamination and dispersive property, and foaming power is strong.

Potassium sorbate is mould fungus inhibition effectively, the activity of yeast and aerobic bacteria, can also prevent harmful microbe growth and breedings such as bacillus botulinus, staphylococcus, Salmonella, it is stronger than bactericidal action that it restrains the effect of growing, thereby reach the holding time that prolongs toothpaste effectively, and the local flavor of maintenance toothpaste, its antiseptic effect is 5-10 a times of like product sodium benzoate.

Oleum menthae is to evaporate the liquid that contains menthol from Herba Menthae, has refrigerant and special Herba Menthae fragrance fragrance.

The present invention is achieved by following technical proposals:

The production method of attapulgite shiny pricklyash toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite shiny pricklyash toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite shiny pricklyash toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; The purpose of stirring at low speed is that various batchings are stirred, and helps pulverizing the operate as normal of beater; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; Multi-functional colloid grinding tool has functions such as the pulverizing of wet processed fluid ultra micron, grinding, emulsifying, dispersion, homogenizing, stirring, mixing, can replace and be better than stone grinder, sand mill, ball mill, dispersing emulsification machine, shearing disperse pump, work efficiencies such as homogeneous emulsifying machine, three-roller, tissue mashing machine; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; The ultrahigh speed blender has unique blade design and stepless speed-regulating device, can select optimal speed according to manufacturing technique requirent, and after the pasty mixture after the grinding stirred through ultrahigh speed, viscosity was up to more than the 10000mPas; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite shiny pricklyash toothpaste.

The batching of described attapulgite shiny pricklyash toothpaste is made up of following component: lip lipstick attapulgite clay 30～60%, fresh Radix Zanthoxyli stem and leaf 5～25%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.05～0.5%, Oleum menthae 0.05～0.5% and deionized water 25～55% by weight percentage.

The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay.

This production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15～35%, water 65～85%.

Attapulgite shiny pricklyash toothpaste uses lip lipstick attapulgite clay to be primary raw material, does not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.

Attapulgite shiny pricklyash toothpaste uses fresh Radix Zanthoxyli stem and leaf, not only can make full use of the effective ingredient of Radix Zanthoxyli, reduce pollution in the dry in the sun process, go mouldy and production cost, and kept the Plant fiber of Radix Zanthoxyli, can increase the denseness of lotion of toothpaste, help increasing the friction of toothpaste, improve the friction effect and the stability of toothpaste.

The cleaning of attapulgite shiny pricklyash toothpaste mastic, soft fine and smooth, strong, refrigerant tasty and refreshing, the good stability of foaming power; Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal, the slide no marking.

Attapulgite shiny pricklyash toothpaste can directly adsorb and remove multiple foreign odor flavor, minimizing dental plaque and the prevention gingival hemorrhage in the oral cavity, and the prevention oral disease is had certain assosting effect.

The present invention is applicable to and produces attapulgite shiny pricklyash toothpaste, Chinese herbal toothpaste and other medicines toothpaste.

The specific embodiment:

The invention will be further described below in conjunction with embodiment:

The production method of attapulgite shiny pricklyash toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite shiny pricklyash, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite shiny pricklyash, the speed controlling of blender is at 600 rev/mins, the stirring at low speed time was controlled at 8 minutes, and the speed controlling of pulverizing beater is at 2800 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 8000 rev/mins, and the high-speed stirred time was controlled at 20 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite shiny pricklyash.

The batching of described attapulgite shiny pricklyash toothpaste is made up of following component: lip lipstick attapulgite clay 50.0%, fresh Radix Zanthoxyli stem and leaf 16.0%, sodium lauryl sulphate 1.6%, potassium sorbate 0.3%, Oleum menthae 0.1% and deionized water 32.0% by weight percentage.

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30%, water 70%.

Main physical and chemical index testing result

Claims (1)

1, a kind of production method of attapulgite shiny pricklyash toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite shiny pricklyash toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite shiny pricklyash toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite shiny pricklyash toothpaste;

The batching of described attapulgite shiny pricklyash toothpaste is made up of following component: lip lipstick attapulgite clay 30～60%, fresh Radix Zanthoxyli stem and leaf 5～25%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.05～0.5%, Oleum menthae 0.05～0.5% and deionized water 25～55% by weight percentage;

The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay;

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 15～35%, water 65～85%.