CN103835126A - Novel mildew preventive for textile, and preparation method thereof - Google Patents

Novel mildew preventive for textile, and preparation method thereof Download PDF

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Publication number
CN103835126A
CN103835126A CN201310671046.1A CN201310671046A CN103835126A CN 103835126 A CN103835126 A CN 103835126A CN 201310671046 A CN201310671046 A CN 201310671046A CN 103835126 A CN103835126 A CN 103835126A
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parts
preparation
textile
mildew preventive
triclosan
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CN201310671046.1A
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CN103835126B (en
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李本明
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Wang Weixia
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QINGDAO WUWEI INSULATION MATERIAL Co Ltd
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Abstract

The invention provides a novel mildew preventive for textile, and a preparation method thereof. The novel mildew preventive is prepared from the following materials by weight: 0.1-0.5 part of salviae miltiorrhizae, 0.2-0.6 part of radix scutellariae, 0.3-0.7 part of fructus kochiae, 0.1-0.5 part of coptis chinensis, 0.8-1.5 parts of radix stemonae, 0.4-0.9 parts of white patchouli, 1.2-1.8 parts of rhizoma smilacis glabrae, 0.5-1.5 parts of terminalia chebuia, 0.1-1.0 part of purple perilla, 0.5-1.5 parts of folium artemisiae argyi, 0.7-1.4 parts of sanders, 8.5-12.5 parts of propionic acid, 5-10 parts of triclosan and 8-15 parts of benzoic acid. The mildew preventive has a good mildew prevention effect and low cost, and is safe and environment-friendly. The mildew preventive contains traditional Chinese medicine components, is green and safe, has no corrosion or damage to the textile, can make the textile keep dry and good breathability, can act durably and uniformly, has good comprehensive performance and is suitable for industrial application.

Description

A kind of textiles New Type Antiseptic Germicide and preparation method thereof
Technical field
The present invention relates to a kind of textiles New Type Antiseptic Germicide and preparation method thereof.
Background technology
Textiles has long history.As far back as the Stone Age southern Europe just there is linen, to the Bronze Age, Northern Europe has produced wool fabric.China is world-famous silk big country, and before several thousand, just having breeds silkworms controls an industry, and many ancient tombs, the silk goods that ancient site is unearthed are exactly best witness .in ruins, there is large quantities of silk goods and silk in the Neolithic Age (being equivalent to the Shang dynasty) of excavating out at Wu County, Zhejiang.To the Zhou Dynasty, existing a large amount of literature records about silk thing.No. 1, Mawangdui, Changsha tomb of Han dynasty is especially for we have opened one underground " silk treasure-house " silk such as a large amount of intact thin,tough silk, yarn, sieve, figured woven silk material, silk floss, fluffing silk floss, embroidery, the burlap linen fabrics that have been unearthed.Textiles is of a great variety, and except the artificial synthetic fiber who occurred modern age, the textiles in ancient times mainly contains silk goods, woolen knitwear, cotton goods and the linen fabrics.Front two generic animal fibers, rear two generic strings.Textiles is the organic substance by atomic buildings such as carbon, hydrogen, oxygen, nitrogen; in moist, warm, improper ventilation, light irradiation and oxidizing atmosphere, be easy to occur oxidation reaction and hydrolysis; cause its rot mouldy, lose intensity, therefore particularly important to the mildew-resistant protection of textiles.
Along with social development, the raising of economic level, large-scale light industry enterprise particularly textile enterprise's quantity rolls up.Textiles is various in style, and majority easily goes mouldy, as cotton, fiber crops, hair, vinylon, nylon, acrylic fibers spray silk etc.Thereby the storage of textile product and raw material also becomes a difficult problem for these enterprises.For the control that textile product goes mouldy, many factories have to strengthen expect that from former product processes the administration of health of whole process.But under many circumstances, control the initial contaminant capacity of microorganism or arrange that all environmental conditions that is unfavorable for growth of microorganism normally can not accomplish, also need to use mould inhibitor to control the pollution and harm of microorganism to production environment, material, product.
Along with, the enhancing of people's environmental consciousness, the effect cheaply of studying a kind of environmental protection significantly mould inhibitor becomes important topic.
Summary of the invention
The invention provides a kind of textiles New Type Antiseptic Germicide and preparation method thereof.
The present invention is achieved in that a kind of textiles New Type Antiseptic Germicide, is prepared from by the material of following weight portion: red sage root 0.1-0.5 part, Huang Fen 0.2-0.6 part; Fruit of summer cypress 0.3-0.7 part; Coptis 0.1-0.5 part; Tuber of stemona 0.8-1.5 part; White wrinkled giant hyssop 0.4-0.9 part; Smilax 1.2-1.8 part; The sub-0.5-1.5 part of section; Purple perilla 0.1-1.0 part; Tarragon 0.5-1.5 part; Santal 0.7-1.4 part; Propionic acid 8.5-12.5 part; Triclosan 5-10 part; Benzoic acid 8-15 part; Water 15-30 part.
The method of preparing mould inhibitor as claimed in claim 1, is characterized in that, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, cold water soak, pulverizes;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation;
C) by B) in the mixture that obtains dry, cooling.
Preferably, A) described in the cold water soak time be 120-140min.
Preferably, A) described in cold water temperature be 8-10 DEG C.
Preferably, B) in temperature retention time be 130-160min.
Advantage of the present invention is:
Anti-mold effect of the present invention is good, and cost is low, safety and environmental protection.It includes traditional Chinese medicine ingredients green safety, to the corrosion-free not damaged of textiles, can make textiles keep dry and fine air permeability, and can act on equably lastingly, and good combination property, is suitable for industrial applications.
Detailed description of the invention
Embodiment 1
Prepare the material of following weight portion: 0.1 part of the red sage root, 0.2 part of Huang Fen; 0.3 part of the fruit of summer cypress; 0.1 part of the coptis; 0.8 part of the tuber of stemona; 0.4 part of white wrinkled giant hyssop; 1.2 parts of smilaxs; 0.5 part of section's; 0.1 part of purple perilla; 0.5 part of tarragon; 0.7 part, santal; 8.5 parts of propionic acid; 5 parts of triclosans; 8 parts, benzoic acid; 15 parts, water.
The method of the mould inhibitor described in preparation, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation 130-160min;
C) by B) in the mixture that obtains dry, cooling.
Embodiment 2
Prepare the material of following weight portion: 0.3 part of the red sage root, 0.5 part of Huang Fen; 0.5 part of the fruit of summer cypress; 0.4 part of the coptis; 1.0 parts of the tubers of stemona; 0.6 part of white wrinkled giant hyssop; 1.5 parts of smilaxs; 1.0 parts of section's; 0.8 part of purple perilla; 1.0 parts of tarragons; 1.0 parts, santal; 10 parts of propionic acid; 7 parts of triclosans; 10 parts, benzoic acid; 25 parts, water.
The method of the mould inhibitor described in preparation, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation 130-160min;
C) by B) in the mixture that obtains dry, cooling.
Embodiment 3
Prepare the material of following weight portion: 0.5 part of the red sage root, 0.6 part of Huang Fen; 0.7 part of the fruit of summer cypress; 0.5 part of the coptis; 1.5 parts of the tubers of stemona; 0.9 part of white wrinkled giant hyssop; 1.8 parts of smilaxs; 1.5 parts of section's; 1.0 parts of purple perillas; 1.5 parts of tarragons; 1.4 parts, santal; 12.5 parts of propionic acid; 10 parts of triclosans; 15 parts, benzoic acid; 30 parts, water.
The method of the mould inhibitor described in preparation, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation 130-160min;
C) by B) in the mixture that obtains dry, cooling.
Finally it should be noted that: above embodiment is only in order to illustrate the present invention and unrestricted technical scheme described in the invention; Therefore, although this description has been described in detail the present invention with reference to each above-mentioned embodiment,, those of ordinary skill in the art should be appreciated that still and can modify or be equal to replacement the present invention; And all do not depart from technical scheme and the improvement thereof of invention spirit and scope, it all should be encompassed in the middle of claim scope of the present invention.

Claims (5)

1. a textiles New Type Antiseptic Germicide, is characterized in that, is prepared from by the material of following weight portion: red sage root 0.1-0.5 part, Huang Fen 0.2-0.6 part; Fruit of summer cypress 0.3-0.7 part; Coptis 0.1-0.5 part; Tuber of stemona 0.8-1.5 part; White wrinkled giant hyssop 0.4-0.9 part; Smilax 1.2-1.8 part; The sub-0.5-1.5 part of section; Purple perilla 0.1-1.0 part; Tarragon 0.5-1.5 part; Santal 0.7-1.4 part; Propionic acid 8.5-12.5 part; Triclosan 5-10 part; Benzoic acid 8-15 part; Water 15-30 part.
2. the method for preparation mould inhibitor as claimed in claim 1, is characterized in that, comprising:
A) respectively the red sage root, Huang Fen, the fruit of summer cypress, the coptis, the tuber of stemona, white wrinkled giant hyssop, smilax, section's, purple perilla, tarragon, santal are cleaned, cold water soak, pulverizes;
B) by A) in pulverized product put into blender and mix, add successively propionic acid, triclosan, benzoic acid, water is heated to 70-80 DEG C simultaneously in whipping process, insulation;
C) by B) in the mixture that obtains dry, cooling.
3. preparation method according to claim 2, is characterized in that, A) described in the cold water soak time be 120-140min.
4. preparation method according to claim 2, is characterized in that, A) described in cold water temperature be 8-10 DEG C.
5. preparation method according to claim 2, is characterized in that, B) in temperature retention time be 130-160min.
CN201310671046.1A 2013-12-12 2013-12-12 A kind of anti-mildew agent for textiles and preparation method thereof Active CN103835126B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104389169A (en) * 2014-11-18 2015-03-04 太仓市宏亿化纤有限公司 Mildew preventive used for textiles and preparation method thereof
CN105274835A (en) * 2015-12-01 2016-01-27 江苏太林纺织品有限公司 Grey fabric
CN105369603A (en) * 2015-12-22 2016-03-02 常熟市泽众家用纺织品有限公司 Pillow interior fabric
CN105401436A (en) * 2015-12-18 2016-03-16 苏州富美纺织科技有限公司 Preparation method for flame-retardation finishing liquid for fabrics
CN105401439A (en) * 2015-12-24 2016-03-16 常熟市馨格家纺有限公司 Lambwool fabric
CN106351001A (en) * 2016-08-26 2017-01-25 相里海霞 Method for manufacturing ultraviolet-proof textile fabric based on moxa

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5641257A (en) * 1979-09-08 1981-04-17 Nissan Chem Ind Ltd Industrial antifungal agent
CN101077079A (en) * 2006-05-25 2007-11-28 西安格润森生物制药股份有限公司 Plant-type antibacterial agent
CN101215781A (en) * 2007-12-27 2008-07-09 浙江嘉得莱有限公司 Chinese herbal medicine antibiotic finishing method for knitting plus material
CN102071573A (en) * 2009-11-20 2011-05-25 戚冬梅 Anti-mildew agent for textiles
CN102310966A (en) * 2010-07-01 2012-01-11 郑州大学 Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof
CN102561029A (en) * 2010-12-15 2012-07-11 戚冬梅 Mildew-proof agent for textile

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5641257A (en) * 1979-09-08 1981-04-17 Nissan Chem Ind Ltd Industrial antifungal agent
CN101077079A (en) * 2006-05-25 2007-11-28 西安格润森生物制药股份有限公司 Plant-type antibacterial agent
CN101215781A (en) * 2007-12-27 2008-07-09 浙江嘉得莱有限公司 Chinese herbal medicine antibiotic finishing method for knitting plus material
CN102071573A (en) * 2009-11-20 2011-05-25 戚冬梅 Anti-mildew agent for textiles
CN102310966A (en) * 2010-07-01 2012-01-11 郑州大学 Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof
CN102561029A (en) * 2010-12-15 2012-07-11 戚冬梅 Mildew-proof agent for textile

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104389169A (en) * 2014-11-18 2015-03-04 太仓市宏亿化纤有限公司 Mildew preventive used for textiles and preparation method thereof
CN105274835A (en) * 2015-12-01 2016-01-27 江苏太林纺织品有限公司 Grey fabric
CN105401436A (en) * 2015-12-18 2016-03-16 苏州富美纺织科技有限公司 Preparation method for flame-retardation finishing liquid for fabrics
CN105369603A (en) * 2015-12-22 2016-03-02 常熟市泽众家用纺织品有限公司 Pillow interior fabric
CN105401439A (en) * 2015-12-24 2016-03-16 常熟市馨格家纺有限公司 Lambwool fabric
CN106351001A (en) * 2016-08-26 2017-01-25 相里海霞 Method for manufacturing ultraviolet-proof textile fabric based on moxa

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Inventor after: Shi Hongsheng

Inventor after: Ma Ningning

Inventor after: Li Zhengrong

Inventor before: Li Benming

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Effective date of registration: 20170504

Address after: 528400 Guangdong province Zhongshan City Triangle Town Hing Road No. 18 first floor

Patentee after: Zhongshan Zhongke Chemical Co., Ltd.

Address before: Room 2, building 158, Haier Road, Laoshan District, Shandong, Qingdao, 266061

Patentee before: QINGDAO WUWEI INSULATION MATERIAL CO., LTD.

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Effective date of registration: 20220329

Address after: 528437 room H40, building 7, Rhine garden, Ligang City, Torch Development Zone, Zhongshan City, Guangdong Province

Patentee after: Wang Weixia

Address before: 528400 first floor, No. 18, Tongxing Road, Sanjiao Town, Zhongshan City, Guangdong Province

Patentee before: ZHONGSHAN ZHONGKE CHEMICAL Co.,Ltd.

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