CN103835126B - A kind of anti-mildew agent for textiles and preparation method thereof - Google Patents
A kind of anti-mildew agent for textiles and preparation method thereof Download PDFInfo
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- CN103835126B CN103835126B CN201310671046.1A CN201310671046A CN103835126B CN 103835126 B CN103835126 B CN 103835126B CN 201310671046 A CN201310671046 A CN 201310671046A CN 103835126 B CN103835126 B CN 103835126B
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Abstract
The invention provides a kind of anti-mildew agent for textiles and preparation method thereof, the material of following weight portion be prepared from: Radix Salviae Miltiorrhizae 0.1 0.5 parts, Huang Fen 0.2 0.6 parts；The Fructus Kochiae 0.3 0.7 parts；Rhizoma Coptidis 0.1 0.5 parts；The Radix Stemonae 0.8 1.5 parts；White Herba Pogostemonis 0.4 0.9 parts；Rhizoma Smilacis Glabrae 1.2 1.8 parts；Section's 0.5 1.5 parts；Folium Perillae 0.1 1.0 parts；Folium Artemisiae Argyi 0.5 1.5 parts；0.7 1.4 parts of Lignum Santali Albi；Propanoic acid 8.5 12.5 parts；Triclosan 5 10 parts；8 15 parts of benzoic acid.Anti-mold effect of the present invention is good, and low cost, safety and environmental protection.It includes Chinese medicine ingredients green safety, not damaged corrosion-free to textile, textile can be made to keep being dried and fine air permeability, and can act on the most equably, good combination property, be suitable to industrial applications.
Description
Technical fieldThe present invention relates to a kind of anti-mildew agent for textiles and preparation method thereof.
Background technology
Textile has long history.As far back as the Stone Age southern Europe occurred as soon as linen, to the Bronze Age, Northern Europe creates wool fabric.China is world-famous silk big country, before thousand of years, just has sericulture to control an industry, and the silk that many ancient tombs, ancient site are unearthed is exactly best witness.In the Neolithic Age (the being equivalent to the Shang dynasty) ruins that Wu County, Zhejiang is excavated out, occur in that large quantities of silk and silkworm silk.To the Zhou Dynasty, existing in a large number about the literature record of silk thing.Mawangdui, Changsha 1 tomb of Han dynasty opens a underground " silk treasure-house " for us especially and has been unearthed the silk linen fabrics such as a large amount of intact thin,tough silk, yarn, sieve, figured woven silk material, silk floss, fluffing silk floss, embroidery, burlap.Textile is of a great variety, and in addition to the artificial synthetic fiber that modern age occurs, the textile in ancient times mainly has silk, woolen knitwear, cotton goods and the linen fabrics.Front two generic animal fibers, rear two generic Plant fiber.Textile is by the organic substance of the atomic buildings such as carbon, hydrogen, oxygen, nitrogen; humidity, warm, improper ventilation, radiation and oxidizing atmosphere are easy to oxidation reaction and hydrolysis occur; cause its rot mouldy, lose intensity, therefore the mildew-resistant of textile is protected particularly important.
Along with the development of society, the raising of economic level, the particularly textile enterprise's quantity substantial increase of large-scale light industry enterprise.Textile is various in style, and majority easily goes mouldy, such as cotton, fiber crops, hair, vinylon, nylon, acrylon spray webbing etc..Thus the storage of textile product and raw material also becomes a difficult problem for these enterprises.The preventing and treating gone mouldy for textile product, many factories have to strengthen the administration of health of whole process from raw material to Product processing.But under many circumstances, control the initial contamination amount of microorganism or arrange what all environmental conditions being unfavorable for growth of microorganism typically can not be accomplished, in addition it is also necessary to using antifungus agent to control microorganism to production environment, material, the pollution of product and infringement.
Along with, the enhancing of people's environmental consciousness, the effect antifungus agent significantly of the low cost studying a kind of environmental protection becomes important topic.
Summary of the inventionThe invention provides a kind of anti-mildew agent for textiles and preparation method thereof.
The present invention is achieved in that a kind of anti-mildew agent for textiles, the material of following weight portion be prepared from: Radix Salviae Miltiorrhizae 0.1-0.5 part, Huang Fen 0.2-0.6 part；Fructus Kochiae 0.3-0.7 part；Rhizoma Coptidis 0.1-0.5 part；Radix Stemonae 0.8-1.5 part；White Herba Pogostemonis 0.4-0.9 part；Rhizoma Smilacis Glabrae 1.2-1.8 part；Section's sub-0.5-1.5 part；Folium Perillae 0.1-1.0 part；Folium Artemisiae Argyi 0.5-1.5 part；Lignum Santali Albi 0.7-1.4 part；Propanoic acid 8.5-12.5 part；Triclosan 5-10 part；Benzoic acid 8-15 part；Water 15-30 part.
The method preparing antifungus agent as claimed in claim 1, it is characterised in that including:
A) respectively Radix Salviae Miltiorrhizae, Huang Fen, the Fructus Kochiae, Rhizoma Coptidis, the Radix Stemonae, white Herba Pogostemonis, Rhizoma Smilacis Glabrae, section's, Folium Perillae, Folium Artemisiae Argyi, Lignum Santali Albi are cleaned, cold water soak, pulverize；
B) by A) in pulverized product put into mix homogeneously in blender, be sequentially added into propanoic acid, triclosan, benzoic acid, water, in whipping process, be heated to 70-80 DEG C, insulation simultaneously；
C) by B) in the mixture that obtains dry, cooling.
Preferably, A) described in the cold water soak time be 120-140min.Preferably, A) described in cold water temperature be 8-10 DEG C.Preferably, B) in temperature retention time be 130-160min.
The invention have the advantage that anti-mold effect of the present invention is good, and low cost, safety and environmental protection.It includes Chinese medicine ingredients green safety, not damaged corrosion-free to textile, textile can be made to keep being dried and fine air permeability, and can act on the most equably, good combination property, be suitable to industrial applications.
Detailed description of the inventionEmbodiment 1
Prepare the material of following weight portion: Radix Salviae Miltiorrhizae 0.1 part, Huang Fen 0.2 part；The Fructus Kochiae 0.3 part；Rhizoma Coptidis 0.1 part；The Radix Stemonae 0.8 part；White Herba Pogostemonis 0.4 part；Rhizoma Smilacis Glabrae 1.2 parts；Section's 0.5 part；Folium Perillae 0.1 part；Folium Artemisiae Argyi 0.5 part；0.7 part of Lignum Santali Albi；Propanoic acid 8.5 parts；Triclosan 5 parts；8 parts of benzoic acid；15 parts of water.
The method of the antifungus agent described in preparation, including:
A) respectively Radix Salviae Miltiorrhizae, Huang Fen, the Fructus Kochiae, Rhizoma Coptidis, the Radix Stemonae, white Herba Pogostemonis, Rhizoma Smilacis Glabrae, section's, Folium Perillae, Folium Artemisiae Argyi, Lignum Santali Albi are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize；
B) by A) in pulverized product put into mix homogeneously in blender, be sequentially added into propanoic acid, triclosan, benzoic acid, water, in whipping process, be heated to 70-80 DEG C simultaneously, be incubated 130-160min；
C) by B) in the mixture that obtains dry, cooling.
Embodiment 2
Prepare the material of following weight portion: Radix Salviae Miltiorrhizae 0.3 part, Huang Fen 0.5 part；The Fructus Kochiae 0.5 part；Rhizoma Coptidis 0.4 part；The Radix Stemonae 1.0 parts；White Herba Pogostemonis 0.6 part；Rhizoma Smilacis Glabrae 1.5 parts；Section's 1.0 parts；Folium Perillae 0.8 part；Folium Artemisiae Argyi 1.0 parts；1.0 parts of Lignum Santali Albi；Propanoic acid 10 parts；Triclosan 7 parts；10 parts of benzoic acid；25 parts of water.
The method of the antifungus agent described in preparation, including:
A) respectively Radix Salviae Miltiorrhizae, Huang Fen, the Fructus Kochiae, Rhizoma Coptidis, the Radix Stemonae, white Herba Pogostemonis, Rhizoma Smilacis Glabrae, section's, Folium Perillae, Folium Artemisiae Argyi, Lignum Santali Albi are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize；
B) by A) in pulverized product put into mix homogeneously in blender, be sequentially added into propanoic acid, triclosan, benzoic acid, water, in whipping process, be heated to 70-80 DEG C simultaneously, be incubated 130-160min；
C) by B) in the mixture that obtains dry, cooling.
Embodiment 3
Prepare the material of following weight portion: Radix Salviae Miltiorrhizae 0.5 part, Huang Fen 0.6 part；The Fructus Kochiae 0.7 part；Rhizoma Coptidis 0.5 part；The Radix Stemonae 1.5 parts；White Herba Pogostemonis 0.9 part；Rhizoma Smilacis Glabrae 1.8 parts；Section's 1.5 parts；Folium Perillae 1.0 parts；Folium Artemisiae Argyi 1.5 parts；1.4 parts of Lignum Santali Albi；Propanoic acid 12.5 parts；Triclosan 10 parts；15 parts of benzoic acid；30 parts of water.The method of the antifungus agent described in preparation, including:
A) respectively Radix Salviae Miltiorrhizae, Huang Fen, the Fructus Kochiae, Rhizoma Coptidis, the Radix Stemonae, white Herba Pogostemonis, Rhizoma Smilacis Glabrae, section's, Folium Perillae, Folium Artemisiae Argyi, Lignum Santali Albi are cleaned, be placed in 8-10 DEG C of cold water soak 120-140min, pulverize；
B) by A) in pulverized product put into mix homogeneously in blender, be sequentially added into propanoic acid, triclosan, benzoic acid, water, in whipping process, be heated to 70-80 DEG C simultaneously, be incubated 130-160min；
C) by B) in the mixture that obtains dry, cooling.
Last it is noted that above example only in order to the present invention is described and and unrestricted technical scheme described in the invention；Therefore, although this specification with reference to each above-mentioned embodiment to present invention has been detailed description, but, it will be understood by those within the art that, still the present invention can be modified or equivalent；And all are without departing from spirit and the technical scheme of scope and improvement thereof, it all should be contained in the middle of scope of the presently claimed invention.
Claims (1)
1. an anti-mildew agent for textiles, it is characterised in that be prepared from by the material of following weight portion: Radix Salviae Miltiorrhizae 0.1-0.5 part；Yellow fragrant 0.2-0.6 part；Fructus Kochiae 0.3-0.7 part；Rhizoma Coptidis 0.1-0.5 part；Radix Stemonae 0.8-1.5 part；White Herba Pogostemonis 0.4-0.9 part；Rhizoma Smilacis Glabrae 1.2-1.8 part；Section's sub-0.5-1.5 part；Folium Perillae 0.1-1.0 part；Folium Artemisiae Argyi 0.5-1.5 part；Lignum Santali Albi 0.7-1.4 part；Propanoic acid 8.5-12.5 part；Triclosan 5-10 part；Benzoic acid 8-15 part；Water 15-30 part；
The preparation method of above-mentioned antifungus agent includes: A) Radix Salviae Miltiorrhizae, Huang Fen, the Fructus Kochiae, Rhizoma Coptidis, the Radix Stemonae, white Herba Pogostemonis, Rhizoma Smilacis Glabrae, section's, Folium Perillae, Folium Artemisiae Argyi, Lignum Santali Albi are cleaned respectively, cold water soak, pulverizes；
B) by A) in pulverized product put into mix homogeneously in blender, be sequentially added into propanoic acid, triclosan, benzoic acid, water, simultaneously
70-80 DEG C it is heated to, insulation in whipping process；
C) by B) in the mixture that obtains dry, cooling；
Above-mentioned A) described in the cold water soak time be 120-140min；
Above-mentioned A) described in cold water temperature be 8-10 DEG C；
Above-mentioned B) in temperature retention time be 130-160min.
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| CN103835126B true CN103835126B (en) | 2016-08-17 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104389169A (en) * | 2014-11-18 | 2015-03-04 | 太仓市宏亿化纤有限公司 | Mildew preventive used for textiles and preparation method thereof |
| CN105274835A (en) * | 2015-12-01 | 2016-01-27 | 江苏太林纺织品有限公司 | Grey fabric |
| CN105401436A (en) * | 2015-12-18 | 2016-03-16 | 苏州富美纺织科技有限公司 | Preparation method for flame-retardation finishing liquid for fabrics |
| CN105369603A (en) * | 2015-12-22 | 2016-03-02 | 常熟市泽众家用纺织品有限公司 | Pillow interior fabric |
| CN105401439A (en) * | 2015-12-24 | 2016-03-16 | 常熟市馨格家纺有限公司 | Lambwool fabric |
| CN106351001A (en) * | 2016-08-26 | 2017-01-25 | 相里海霞 | Method for manufacturing ultraviolet-proof textile fabric based on moxa |
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| CN101077079A (en) * | 2006-05-25 | 2007-11-28 | 西安格润森生物制药股份有限公司 | Plant-type antibacterial agent |
| CN101215781A (en) * | 2007-12-27 | 2008-07-09 | 浙江嘉得莱有限公司 | Chinese herbal medicine antibiotic finishing method for knitting plus material |
| CN102071573A (en) * | 2009-11-20 | 2011-05-25 | 戚冬梅 | Anti-mildew agent for textiles |
| CN102561029A (en) * | 2010-12-15 | 2012-07-11 | 戚冬梅 | Mildew-proof agent for textile |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5641257A (en) * | 1979-09-08 | 1981-04-17 | Nissan Chem Ind Ltd | Industrial antifungal agent |
| CN102310966A (en) * | 2010-07-01 | 2012-01-11 | 郑州大学 | Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101077079A (en) * | 2006-05-25 | 2007-11-28 | 西安格润森生物制药股份有限公司 | Plant-type antibacterial agent |
| CN101215781A (en) * | 2007-12-27 | 2008-07-09 | 浙江嘉得莱有限公司 | Chinese herbal medicine antibiotic finishing method for knitting plus material |
| CN102071573A (en) * | 2009-11-20 | 2011-05-25 | 戚冬梅 | Anti-mildew agent for textiles |
| CN102561029A (en) * | 2010-12-15 | 2012-07-11 | 戚冬梅 | Mildew-proof agent for textile |
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Inventor after: Shi Hongsheng Inventor after: Ma Ningning Inventor after: Li Zhengrong Inventor before: Li Benming |
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Effective date of registration: 20170504 Address after: 528400 Guangdong province Zhongshan City Triangle Town Hing Road No. 18 first floor Patentee after: Zhongshan Zhongke Chemical Co., Ltd. Address before: Room 2, building 158, Haier Road, Laoshan District, Shandong, Qingdao, 266061 Patentee before: QINGDAO WUWEI INSULATION MATERIAL CO., LTD. |
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Effective date of registration: 20220329 Address after: 528437 room H40, building 7, Rhine garden, Ligang City, Torch Development Zone, Zhongshan City, Guangdong Province Patentee after: Wang Weixia Address before: 528400 first floor, No. 18, Tongxing Road, Sanjiao Town, Zhongshan City, Guangdong Province Patentee before: ZHONGSHAN ZHONGKE CHEMICAL Co.,Ltd. |