CN106222791A - A kind of preparation method of the uvioresistant polyster fibre with permanent fragrant - Google Patents

A kind of preparation method of the uvioresistant polyster fibre with permanent fragrant Download PDF

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Publication number
CN106222791A
CN106222791A CN201610778632.XA CN201610778632A CN106222791A CN 106222791 A CN106222791 A CN 106222791A CN 201610778632 A CN201610778632 A CN 201610778632A CN 106222791 A CN106222791 A CN 106222791A
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CN
China
Prior art keywords
nidus vespae
polyster fibre
calcium carbonate
polyester slice
precipitated calcium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610778632.XA
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Chinese (zh)
Inventor
郑和德
陈义龙
刘树立
庞立志
曾静民
叶德晃
陈荣
王颜昌
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Huaxiang (china) High Fiber Co Ltd
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Huaxiang (china) High Fiber Co Ltd
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Application filed by Huaxiang (china) High Fiber Co Ltd filed Critical Huaxiang (china) High Fiber Co Ltd
Priority to CN201610778632.XA priority Critical patent/CN106222791A/en
Publication of CN106222791A publication Critical patent/CN106222791A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/88Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/92Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Artificial Filaments (AREA)

Abstract

The invention provides the preparation method of a kind of uvioresistant polyster fibre with permanent fragrant, Nidus Vespae and precipitated calcium carbonate are joined blend melt spinning in polyester slice.Containing effective ingredient such as larger molecular organicses in Nidus Vespae, can be fragrant;Use dry grinding, so on the one hand prevent the effective ingredient loss by dissolution in Nidus Vespae, on the other hand do not have large quantity of moisture and follow-up melt spinning is impacted;The effective ingredient such as the larger molecular organics primarily served the purpose of in protection Nidus Vespae of precipitated calcium carbonate; larger molecular organics molecular structure in the course of processing of melt spinning and subsequent fiber and fabric is prevented to be destroyed; the polyster fibre of the present invention; when perspiring; especially in motor process; precipitated calcium carbonate is dissolved, and will be discharged by the effective ingredient in Nidus Vespae, thus reaches the effect of permanent giving out fragrance;Adding nano-ceramic powder, uvioresistant effect is especially good.

Description

A kind of preparation method of the uvioresistant polyster fibre with permanent fragrant
Technical field
The present invention relates to polyster fibre technical field, especially, relate to a kind of uvioresistant terylene with permanent fragrant The preparation method of fiber.
Background technology
Polyster fibre is as most widely used chemical fibre, and it has good fibre-forming performance and mechanical performance, intensity High, fast light, heat-resisting and resistance to acids and bases is good, there is good processability and Yi Fangxing, can pure spin, blending and intertexture.Polyester fabric Washable and wearable, ironing and anti-crease, clothing, home textile, decoration and product with etc. field be widely used.But, polyster fibre is also deposited , fabric not absorbing sweat poor in hygroscopicity, dress have feeling of oppression and heat, anti-static ability difference and easily stain the shortcomings such as dust, the most significantly make The about application of polyster fibre and development.For improving the snugness of fit of polyster fibre, improve the application added value of polyster fibre, It is typically polyster fibre is carried out the improvement of chemically or physically aspect, and then the moisture absorbing and sweat releasing property that endowing terylene fiber is higher, carries High dacron wearing comfort.
Along with people are more and more higher to the requirement of fabric, other performance of polyster fibre is the most gradually subject to people's attention, Especially can odoriferous chemical fibre product, there is good market prospect.
Summary of the invention
Present invention aim at providing, to solve technical problem.
The preparation method of a kind of uvioresistant polyster fibre with permanent fragrant, comprises the following steps:
A, Nidus Vespae pulverizer is pulverized, and grind with mortar, obtain Nidus Vespae powder;
B, Nidus Vespae powder and precipitated calcium carbonate are mixed after, carry out ball milling with dry method ball mill, obtain mixing fine powders, at 35-45 DEG C Lower heated drying 8-12h, sieves;
C, polyester slice, at 160-180 DEG C, are dried 2-4h, carry out pre-crystallized under hot-air at dew point-70 DEG C;
D, mixing fine powders and nano-ceramic powder are added in polyester slice, mix homogeneously;
E, by polyester slice melt spinning on spinning-drawing machine, first oil tanker oils, boundling, twice drawing-off, curling, second spray Spoon oil, cut-out, loosening heat setting machine, packing, obtain the uvioresistant polyster fibre with permanent fragrant.
Preferably, in described step B, the mass ratio of Nidus Vespae powder and precipitated calcium carbonate is 1:(6-10).
Preferably, in described step B, mixing fine powders crosses 325 sieves.
Preferably, in the described uvioresistant polyster fibre with permanent fragrant, the percentage by weight of each raw material is as follows:
Polyester slice 94-96%
Nano-ceramic powder 1.5-2.5%
Nidus Vespae powder 0.3-0.5%
Precipitated calcium carbonate surplus.
Nidus Vespae, bee colony life and the place raised up seed, be made up of Nidus Vespae.Each Nidus Vespae space in Nidus Vespae is parallel to each other Hang, and perpendicular to the ground, and Nidus Vespae spacing is 7~10 millimeters, referred to as honeybee road.Every Nidus Vespae is linked together by thousands of lairs Composition, is that the Cera Flava secreted by the worker bee wax gland of self is built.Large and small hexagonal lair, be respectively cultivate drone and Worker bee, bottom surface is 3 lozenges.The lair of queen breeding, referred to as Nidus Vespae, shape, like sagging Semen arachidis hypogaeae, is that bee colony is swarmming Front interim build, how on Nidus Vespae bottom and corner.Between drone cell and worker cell, and the connection of Nidus Vespae and frame Place, has irregular transitional type lair, is used for storing Mel and reinforcing Nidus Vespae.
Research shows, Nidus Vespae preparation has the effect promoting Immune Function, and Nidus Vespae immersion is both to hepatitis B table Face antigen has deactivation, also to staphylococcus aureus, bacillus pyocyaneus, escherichia coli, dysentery bacterium, Bacillus typhi and common Bacillus proteuss etc. have the strongest restraint;The funguses such as Aspergillus fumigatus, Aspergillus flavus, eggplant sickle bacterium, leukonid also there is inhibitory action. The chemical composition of Nidus Vespae is the most complicated, mainly contains Cera Flava, resin, oils and fats, pigment, tannin, saccharide, organic acid, fatty acid, glycoside Class, enzyme and insect hormone etc..
The method have the advantages that the uvioresistant polyster fibre with permanent fragrant of the present invention, by Nidus Vespae Blend melt spinning in polyester slice is joined with precipitated calcium carbonate.
In order to protect the various larger molecular organicses such as organic acid in Nidus Vespae, fatty acid, glycoside, enzyme, after Nidus Vespae grinds Mixing homogeneously with precipitated calcium carbonate and rear melt spinning is blended with polyester slice, the effective ingredient in Nidus Vespae is along with precipitated calcium carbonate warp After human sweat is dissolved, light fragrant can be given out for a long time.
In the present invention, the processing mode to Nidus Vespae is dry grinding, so on the one hand prevents the effective ingredient in Nidus Vespae from dissolving Run off, on the other hand do not have large quantity of moisture and follow-up melt spinning is impacted.
Adding nano-ceramic powder, uvioresistant effect is especially good.
Precipitated calcium carbonate, at the effective ingredient such as larger molecular organics primarily served the purpose of in protection Nidus Vespae of the present invention, prevents In the course of processing of melt spinning and subsequent fiber and fabric, larger molecular organics molecular structure is destroyed, due to lightweight carbon Acid calcium is acid structure, does not mainly use the solution of acidity to process in the processing of fabric, and precipitated calcium carbonate would not be sent out Raw reaction, and in follow-up wearing process, owing to the perspiration of human body is acid, therefore when perspiring, especially in motor process, Human body is perspired in a large number, and precipitated calcium carbonate is dissolved, and will be discharged by the effective ingredient in Nidus Vespae, thus reaches to distribute for a long time The effect of delicate fragrance;Precipitated calcium carbonate can also promote nano-ceramic powder dispersion effect in polyester slice.
In addition to objects, features and advantages described above, the present invention also has other objects, features and advantages. The present invention is further detailed explanation below.
Detailed description of the invention
Hereinafter embodiments of the invention are described in detail, but the present invention can limit according to claim and cover Multitude of different ways implement.
Embodiment 1
The preparation method of a kind of uvioresistant polyster fibre with permanent fragrant, comprises the following steps:
A, Nidus Vespae pulverizer is pulverized, and grind with mortar, obtain Nidus Vespae powder;
B, Nidus Vespae powder and precipitated calcium carbonate are mixed after, carry out ball milling with dry method ball mill, obtain mixing fine powders, heat at 40 DEG C It is dried 10h, sieves;
C, polyester slice, at 170 DEG C, are dried 3h, carry out pre-crystallized under hot-air at dew point-70 DEG C;
D, mixing fine powders and nano-ceramic powder are added in polyester slice, mix homogeneously;
E, by polyester slice melt spinning on spinning-drawing machine, first oil tanker oils, boundling, twice drawing-off, curling, second spray Spoon oil, cut-out, loosening heat setting machine, packing, obtain the uvioresistant polyster fibre with permanent fragrant.
In described step B, mixing fine powders crosses 325 sieves.
In the described uvioresistant polyster fibre with permanent fragrant, the percentage by weight of each raw material is as follows:
Polyester slice 94%
Nano-ceramic powder 2%
Nidus Vespae powder 0.4%
Precipitated calcium carbonate surplus.
Embodiment 2
The preparation method of a kind of uvioresistant polyster fibre with permanent fragrant, comprises the following steps:
A, Nidus Vespae pulverizer is pulverized, and grind with mortar, obtain Nidus Vespae powder;
B, Nidus Vespae powder and precipitated calcium carbonate are mixed after, carry out ball milling with dry method ball mill, obtain mixing fine powders, heat at 35 DEG C It is dried 12h, sieves;
C, polyester slice, at 160 DEG C, are dried 4h, carry out pre-crystallized under hot-air at dew point-70 DEG C;
D, mixing fine powders and nano-ceramic powder are added in polyester slice, mix homogeneously;
E, by polyester slice melt spinning on spinning-drawing machine, first oil tanker oils, boundling, twice drawing-off, curling, second spray Spoon oil, cut-out, loosening heat setting machine, packing, obtain the uvioresistant polyster fibre with permanent fragrant.
In described step B, mixing fine powders crosses 325 sieves.
In the described uvioresistant polyster fibre with permanent fragrant, the percentage by weight of each raw material is as follows:
Polyester slice 94%
Nano-ceramic powder 2.5%
Nidus Vespae powder 0.5%
Precipitated calcium carbonate surplus.
Embodiment 3
The preparation method of a kind of uvioresistant polyster fibre with permanent fragrant, comprises the following steps:
A, Nidus Vespae pulverizer is pulverized, and grind with mortar, obtain Nidus Vespae powder;
B, Nidus Vespae powder and precipitated calcium carbonate are mixed after, carry out ball milling with dry method ball mill, obtain mixing fine powders, heat at 45 DEG C It is dried 8h, sieves;
C, polyester slice, at 180 DEG C, are dried 2h, carry out pre-crystallized under hot-air at dew point-70 DEG C;
D, mixing fine powders and nano-ceramic powder are added in polyester slice, mix homogeneously;
E, by polyester slice melt spinning on spinning-drawing machine, first oil tanker oils, boundling, twice drawing-off, curling, second spray Spoon oil, cut-out, loosening heat setting machine, packing, obtain the uvioresistant polyster fibre with permanent fragrant.
In described step B, mixing fine powders crosses 325 sieves.
In the described uvioresistant polyster fibre with permanent fragrant, the percentage by weight of each raw material is as follows:
Polyester slice 96%
Nano-ceramic powder 1.5%
Nidus Vespae powder 0.3%
Precipitated calcium carbonate surplus.
After testing, the polyester fabric that the uvioresistant polyster fibre with permanent fragrant of embodiment of the present invention 1-3 is made into In 1 year through soaping after 100 times, still can keep fragrance, especially when wearing next to the skin motion, delicate fragrance is pleasant, the most not Dissipate.
The polyester fabric that the uvioresistant polyster fibre with permanent fragrant of embodiment of the present invention 1-3 is made into is in 1 year Through soaping after 100 times, anti-ultraviolet index is UPF50+, and ultraviolet resistance is the best.
Comparative example 1
Precipitated calcium carbonate polyester slice in embodiment 1 is replaced.
After testing, the polyester fabric that the polyster fibre of comparative example is made into is soaped after 5 times, has slight fragrant to dissipate Sending out, anti-ultraviolet index is UPF25-30;Soaping after 30 times, fragrant disappears, and anti-ultraviolet index is still UPF25-30.
By the detection data of comparative example 1 it is recognised that in the present invention effect of precipitated calcium carbonate is clearly.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for the skill of this area For art personnel, the present invention can have various modifications and variations.All within the spirit and principles in the present invention, that is made any repaiies Change, equivalent, improvement etc., should be included within the scope of the present invention.

Claims (5)

1. the preparation method of a uvioresistant polyster fibre with permanent fragrant, it is characterised in that comprise the following steps:
A, Nidus Vespae pulverizer is pulverized, and grind with mortar, obtain Nidus Vespae powder;
B, Nidus Vespae powder and precipitated calcium carbonate are mixed after, carry out ball milling with dry method ball mill, obtain mixing fine powders, at 35-45 DEG C Lower heated drying 8-12h, sieves;
C, polyester slice, at 160-180 DEG C, are dried 2-4h, carry out pre-crystallized under hot-air at dew point-70 DEG C;
D, mixing fine powders and nano-ceramic powder are added in polyester slice, mix homogeneously;
E, by polyester slice melt spinning on spinning-drawing machine, first oil tanker oils, boundling, twice drawing-off, curling, second spray Spoon oil, cut-out, loosening heat setting machine, packing, obtain the uvioresistant polyster fibre with permanent fragrant.
There is the preparation method of the uvioresistant polyster fibre of permanent fragrant the most as claimed in claim 1, it is characterised in that institute In step B stated, the mass ratio of Nidus Vespae powder and precipitated calcium carbonate is 1:(6-10).
There is the preparation method of the uvioresistant polyster fibre of permanent fragrant the most as claimed in claim 1, it is characterised in that institute In step B stated, mixing fine powders crosses 325 sieves.
There is the preparation method of the uvioresistant polyster fibre of permanent fragrant the most as claimed in claim 1, it is characterised in that institute In the uvioresistant polyster fibre with permanent fragrant stated, the percentage by weight of each raw material is as follows:
Polyester slice 94-96%
Nano-ceramic powder 1.5-2.5%
Nidus Vespae powder 0.3-0.5%
Precipitated calcium carbonate surplus.
There is the preparation method of the uvioresistant polyster fibre of permanent fragrant the most as claimed in claim 1, it is characterised in that bag Include following steps:
A, Nidus Vespae pulverizer is pulverized, and grind with mortar, obtain Nidus Vespae powder;
B, Nidus Vespae powder and precipitated calcium carbonate are mixed after, carry out ball milling with dry method ball mill, obtain mixing fine powders, heat at 40 DEG C It is dried 10h, crosses 325 mesh sieves;
C, polyester slice, at 170 DEG C, are dried 3h, carry out pre-crystallized under hot-air at dew point-70 DEG C;
D, mixing fine powders and nano-ceramic powder are added in polyester slice, mix homogeneously;
E, by polyester slice melt spinning on spinning-drawing machine, first oil tanker oils, boundling, twice drawing-off, curling, second spray Spoon oil, cut-out, loosening heat setting machine, packing, obtain the uvioresistant polyster fibre with permanent fragrant;
In the described uvioresistant polyster fibre with permanent fragrant, the percentage by weight of each raw material is as follows:
Polyester slice 94%
Nano-ceramic powder 2%
Nidus Vespae powder 0.4%
Precipitated calcium carbonate surplus.
CN201610778632.XA 2016-08-31 2016-08-31 A kind of preparation method of the uvioresistant polyster fibre with permanent fragrant Pending CN106222791A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109763199A (en) * 2019-01-30 2019-05-17 刘奇 Honeycomb fiber producing processes and its application
CN112176449A (en) * 2020-11-19 2021-01-05 湖州欣缘纺织有限公司 Preparation method of fluffy warm-keeping fine denier polyester staple fiber

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105795536A (en) * 2016-05-18 2016-07-27 湖南细心信息科技有限公司 Pearl antibacterial sports bra and preparation method thereof
CN105821549A (en) * 2016-05-18 2016-08-03 湖南细心信息科技有限公司 Pearl anti-bacterial yarn with moisture absorbing and sweat releasing functions and manufacturing method thereof
CN105862159A (en) * 2016-05-05 2016-08-17 长兴宝福织造有限公司 Method for preparing ultraviolet-resistant and antistatic superfine-denier polyester fibers

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105862159A (en) * 2016-05-05 2016-08-17 长兴宝福织造有限公司 Method for preparing ultraviolet-resistant and antistatic superfine-denier polyester fibers
CN105795536A (en) * 2016-05-18 2016-07-27 湖南细心信息科技有限公司 Pearl antibacterial sports bra and preparation method thereof
CN105821549A (en) * 2016-05-18 2016-08-03 湖南细心信息科技有限公司 Pearl anti-bacterial yarn with moisture absorbing and sweat releasing functions and manufacturing method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109763199A (en) * 2019-01-30 2019-05-17 刘奇 Honeycomb fiber producing processes and its application
CN112176449A (en) * 2020-11-19 2021-01-05 湖州欣缘纺织有限公司 Preparation method of fluffy warm-keeping fine denier polyester staple fiber

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Application publication date: 20161214