CN101985584A - Detergent composition for silk and woolen clothes and preparation method thereof - Google Patents

Detergent composition for silk and woolen clothes and preparation method thereof Download PDF

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Publication number
CN101985584A
CN101985584A CN 201010563310 CN201010563310A CN101985584A CN 101985584 A CN101985584 A CN 101985584A CN 201010563310 CN201010563310 CN 201010563310 CN 201010563310 A CN201010563310 A CN 201010563310A CN 101985584 A CN101985584 A CN 101985584A
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China
Prior art keywords
retort
fatty alcohol
polyoxyethylene ether
silk
detergent composition
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CN 201010563310
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CN101985584B (en
Inventor
王耀
巨江理
赵福泰
任春喜
高磊
姜军锋
孙晓勇
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SHAANXI YONGTAI BIOENGINEERING CO Ltd
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SHAANXI YONGTAI BIOENGINEERING CO Ltd
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Publication of CN101985584B publication Critical patent/CN101985584B/en
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Abstract

The invention discloses a detergent composition for silk and woolen clothes, which consists of water, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, lauryl alcoholpolyoxyethylene ether sodium sulfate, amphiprotic imidazoline, alkylphenol polyoxyethylene (TX-10), coconut oleic acid diethanol amide, essence, edetic acid (EDTA) and sodium chloride in part by weigh. The detergent composition has washing broad-spectrum performance, has a good removal and washing effect on dirt, grease, fruit juice, bloodstain and harmful microbes adhered to the silk and woolen clothes, does not damage and fade clothes, is safe and environmental-friendly, has no toxicity or residue and avoids injuring the skin of users. The invention also discloses a method for preparing the detergent composition for the silk and woolen clothes, which comprises the steps of weighing the components first and then processing the components in a reactor. The detergent composition for the silk and woolen clothes prepared by the method is homogenous in component, the steps and implementation are easy and a process is stable.

Description

A kind of sweater detergent composition and preparation method thereof
Technical field
The invention belongs to the washing technology field, be specifically related to a kind of sweater detergent composition, the invention still further relates to the preparation method of this kind silk sweater detergent composition.
Background technology
China raises the country that silkworm and filature are knitted silk fabric in the world the earliest, the ancestors of the Chinese nation have not only invented silk, and flourishing silk, utilize silk, make its on the dress ornament, economically, on the art and all give out magnificent radiance in the culture, and then the silk clothing is draped over one's shoulders all over the world.Silk is said in some sense, has represented Chinese long brilliant cultures.
Silk is made up of thiozell, with human body fabulous biocompatibility is arranged, its smooth surface, and comfort is good.Hydrophilic radicals such as fibroin fiber enrichment amido, amino can absorb moisture or distribute moisture in air, moisture adsorption and releasing are good.In addition, silk is to be made of the multi-void fiber structure, in these spaces, exist a large amount of air, these air have stoped distributing of heat, make and have heat dispersion and good heat retention preferably, not only can play sound-absorbing, dust suction, uvioresistant, insulation effect, play anti-flaming function in addition.Therefore, the silk fabric softness is smooth, graceful magnificent, bright in colour, bright and glittering, moisture absorption, heat-resisting, water-fast, alkaline-resisting.With silk is the clothes that dress material is made, and human body is had health-care effect.The fiber of wool fabric is a protein fibre, and the soft nature of gloss is soft, and is more flexible than other natural fibers such as cotton, fiber crops, silks, anti-crease property is good, and fold moulding preferably and model keeping character are arranged after the flatiron, and absorbing sweat and ventilation property are better, it is good, comfortable and easy to wear to protect dim property, not fugitive color.
The washing of silk sweater thing is different from the washing of other fabrics.Though the silk weaving fabric is alkaline-resisting, the woolens fabric is not alkaline-resisting, therefore, select neutral detergent for use when silk sweater thing washs, to protect their protein fibre.
Like product of the prior art, washing silk sweater thing washing effect is poor, the various spots of thoroughly flush away that have, the destructive force that has is strong, and is gentle inadequately, and damage silk sweater is looked for coloured silk and fiber easily in washing process.Silk sweater detergent composition of the present invention; the washing soil removability is strong; can effectively remove dirt, grease, fruit juice, bloodstain, harmful microorganism etc. on the sweater thing; and have do not injure a sweater fibres, protective clothing is looked for coloured silk; low bubble is easily rinsed, and smell is pure and fresh, does not hinder skin; safety and environmental protection, characteristics such as polluted source not have bright development prospect and huge market development potentiality.
Summary of the invention
The purpose of this invention is to provide a kind of sweater detergent composition, it is not thorough to have overcome existing cleaning product washing, and greasy dirt can not thoroughly be removed, and damages the shortcoming of silk sweater thing easily.
Another object of the present invention provides the preparation method of above-mentioned silk sweater detergent composition.
The technical solution adopted in the present invention is, a kind of sweater detergent composition, it is characterized in that, by weight percentage, composed of the following components: 50%~75% water, 1%~10% fatty alcohol-polyoxyethylene ether AEO9,1%~5% fatty alcohol-polyoxyethylene ether AEO7,5%~15% lauryl alcohol polyethenoxy ether sodium sulfate, 1%~5% amphoteric imidazoline, 1%~5% TX-10,1%~5% coconut acid diethanolamide, 0.1%~1% essence, 0.1%~1%EDTA, 1%~6% sodium-chlor, the mass percent summation of above each component is 100%.
Another technical scheme of the present invention is that the preparation method of silk sweater detergent composition may further comprise the steps:
Step 1: take by weighing following component by weight percentage: 50%~75% water, 1%~10% fatty alcohol-polyoxyethylene ether AEO9,1%~5% fatty alcohol-polyoxyethylene ether AEO7,5%~15% lauryl alcohol polyethenoxy ether sodium sulfate, 1%~5% amphoteric imidazoline, 1%~5% TX-10,1%~5% coconut acid diethanolamide, 0.1%~1% essence, 0.1%~1%EDTA, 1%~6% sodium-chlor, the mass percent summation of above each component is 100%;
Step 2: each component that takes by weighing in the step 1 is processed in reactor: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, make and be warming up to 50 ℃ in the retort, open the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
The beneficial effect of silk sweater detergent composition of the present invention is: have the washing broad spectrum, for the dirt, grease and the harmful microorganism that are attached on the sweater thing good washing effect is arranged all; And safe, nontoxic residue-free is free from side effects, and does not injure a sweater thing, does not fade, and does not injure cleaning staff's skin, and it is healthy to be of value to people, has good practical value, and application prospect is extremely wide.
The preparation method of silk sweater detergent composition of the present invention, step is simple, implements easily, process stabilizing, and the silk sweater detergent composition composition that makes is even.
Embodiment
The present invention is described in detail below in conjunction with embodiment.
Silk sweater detergent composition of the present invention, by weight percentage, composed of the following components: 50%~75% water, 1%~10% fatty alcohol-polyoxyethylene ether AEO9,1%~5% fatty alcohol-polyoxyethylene ether AEO7,5%~15% lauryl alcohol polyethenoxy ether sodium sulfate, 1%~5% amphoteric imidazoline, 1%~5% TX-10,1%~5% coconut acid diethanolamide, 0.1%~1% essence, 0.1%~1%EDTA, 1%~6% sodium-chlor, the mass percent summation of above each component is 100%.
Wherein, TX-10, name is called alkylphenol polyoxyethylene, also is polyoxyethylene nonylphenol ether, and is soluble in water, has good emulsification washing ability.EDTA, product are called ethylenediamine tetraacetic acid (EDTA), and the popular name edetic acid is a kind of important complexing agent.
The preparation method of silk sweater detergent composition of the present invention may further comprise the steps:
Step 1: take by weighing following component by weight percentage: 50%~75% water, 1%~10% fatty alcohol-polyoxyethylene ether AEO9,1%~5% fatty alcohol-polyoxyethylene ether AEO7,5%~15% lauryl alcohol polyethenoxy ether sodium sulfate, 1%~5% amphoteric imidazoline, 1%~5% TX-10,1%~5% coconut acid diethanolamide, 0.1%~1% essence, 0.1%~1%EDTA, 1%~6% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: each component that takes by weighing in the step 1 is processed in reactor: in reactor, add water as solvent, open the retort steam valve, the retort interlayer advances steam, make and be warming up to 50 ℃ in the retort, open the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
Embodiment 1
Step 1: take by weighing following component by weight percentage: 54% water, 8% fatty alcohol-polyoxyethylene ether AEO9,1% fatty alcohol-polyoxyethylene ether AEO7,15% lauryl alcohol polyethenoxy ether sodium sulfate, 5% amphoteric imidazoline, 5% TX-10,5% coconut acid diethanolamide, 1% essence, 1%EDTA, 5% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, makes to be warming up to 50 ℃ in the retort, opens the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
Embodiment 2
Step 1: take by weighing following component by weight percentage: 72.9% water, 9% fatty alcohol-polyoxyethylene ether AEO9,3% fatty alcohol-polyoxyethylene ether AEO7,5% lauryl alcohol polyethenoxy ether sodium sulfate, 4% amphoteric imidazoline, 3% TX-10,1% coconut acid diethanolamide, 0.1% essence, 1%EDTA, 1% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, makes to be warming up to 50 ℃ in the retort, opens the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
Embodiment 3
Step 1: take by weighing following component by weight percentage: 60.9% water, 1% fatty alcohol-polyoxyethylene ether AEO9,5% fatty alcohol-polyoxyethylene ether AEO7,15% lauryl alcohol polyethenoxy ether sodium sulfate, 1% amphoteric imidazoline, 5% TX-10,5% coconut acid diethanolamide, 1% essence, 0.1%EDTA, 6% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, makes to be warming up to 50 ℃ in the retort, opens the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
Embodiment 4
Step 1: take by weighing following component by weight percentage: 75% water, 5% fatty alcohol-polyoxyethylene ether AEO9,5% fatty alcohol-polyoxyethylene ether AEO7,7.5% lauryl alcohol polyethenoxy ether sodium sulfate, 1% amphoteric imidazoline, 1% TX-10,3% coconut acid diethanolamide, 0.2% essence, 0.3%EDTA, 2% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, makes to be warming up to 50 ℃ in the retort, opens the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
Embodiment 5
Step 1: take by weighing following component by weight percentage: 50% water, 10% fatty alcohol-polyoxyethylene ether AEO9,5% fatty alcohol-polyoxyethylene ether AEO7,15% lauryl alcohol polyethenoxy ether sodium sulfate, 3% amphoteric imidazoline, 5% TX-10,5% coconut acid diethanolamide, 0.5% essence, 1%EDTA, 5.5% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, makes to be warming up to 50 ℃ in the retort, opens the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
Embodiment 6
Step 1: take by weighing following component by weight percentage: 71% water, 6% fatty alcohol-polyoxyethylene ether AEO9,2% fatty alcohol-polyoxyethylene ether AEO7,11% lauryl alcohol polyethenoxy ether sodium sulfate, 1% amphoteric imidazoline, 2% TX-10,3% coconut acid diethanolamide, 0.3% essence, 0.7%EDTA, 3% sodium-chlor, the mass percent summation of above each component is 100%.
Step 2: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, makes to be warming up to 50 ℃ in the retort, opens the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.

Claims (2)

1. a silk sweater detergent composition is characterized in that, by weight percentage, composed of the following components: 50%~75% water, 1%~10% fatty alcohol-polyoxyethylene ether AEO9,1%~5% fatty alcohol-polyoxyethylene ether AEO7,5%~15% lauryl alcohol polyethenoxy ether sodium sulfate, 1%~5% amphoteric imidazoline, 1%~5% TX-10,1%~5% coconut acid diethanolamide, 0.1%~1% essence, 0.1%~1%EDTA, 1%~6% sodium-chlor, the mass percent summation of above each component is 100%.
2. the preparation method of described sweater detergent composition of a claim 1, it is characterized in that, may further comprise the steps: step 1: take by weighing following component by weight percentage: 50%~75% water, 1%~10% fatty alcohol-polyoxyethylene ether AEO9,1%~5% fatty alcohol-polyoxyethylene ether AEO7,5%~15% lauryl alcohol polyethenoxy ether sodium sulfate, 1%~5% amphoteric imidazoline, 1%~5% TX-10,1%~5% coconut acid diethanolamide, 0.1%~1% essence, 0.1%~1%EDTA, 1%~6% sodium-chlor, the mass percent summation of above each component is 100%;
Step 2: each component that takes by weighing in the step 1 is processed in reactor: in reactor, add entry, open the retort steam valve, the retort interlayer advances steam, make and be warming up to 50 ℃ in the retort, open the retort feed port, drop into EDTA, stirred 20 minutes, and dropped into the lauryl alcohol polyethenoxy ether sodium sulfate, fatty alcohol-polyoxyethylene ether AEO9, fatty alcohol-polyoxyethylene ether AEO7, coconut acid diethanolamide, amphoteric imidazoline and TX-10, off-response jar feed port, stirred 30 minutes, off-response jar steam valve is opened retort recirculated cooling water turnover valve, advances water coolant to the retort interlayer, make and be cooled to 30 ℃ in the retort, off-response jar recirculated cooling water turnover valve, and keep temperature in the retort, open the retort feed port, drop into sodium-chlor, stirring and dissolving 30 minutes drops into essence, off-response jar feed valve, stirred 20 minutes, and promptly made.
CN 201010563310 2010-11-29 2010-11-29 Detergent composition for silk and woolen clothes and preparation method thereof Expired - Fee Related CN101985584B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102943002A (en) * 2012-11-21 2013-02-27 浙江雀屏纺织化工股份有限公司 Formula and synthesis process of cashmere environment-friendly swelling agent
CN103695198A (en) * 2013-12-10 2014-04-02 常熟虞贵人家居用品有限公司 Cloth cleaning agent
CN105154244A (en) * 2015-07-25 2015-12-16 罗贵全 Cleaning liquid for rabbit hair knitted fabric
CN105861176A (en) * 2016-05-11 2016-08-17 张丽鹏 Clothes washing gel and preparation method thereof
CN107385974A (en) * 2017-06-26 2017-11-24 苏州威尔德工贸有限公司 A kind of silk fabric printing with reactive dye soaping agent and preparation method thereof

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CN1322802A (en) * 2001-06-04 2001-11-21 贾发颂 Phosphate-free liquid detergent and its compounding process
CN1357613A (en) * 2001-11-22 2002-07-10 成都洁利康实业发展有限公司 Completely fused paper soap and its making process
CN1401753A (en) * 2002-09-23 2003-03-12 辽宁北方华兴机械有限公司 Multifunctional phosphateless washing agent
CN101642415A (en) * 2008-08-04 2010-02-10 河南瑞贝卡发制品股份有限公司 Detergent for human hairs and fiber hairs

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1322802A (en) * 2001-06-04 2001-11-21 贾发颂 Phosphate-free liquid detergent and its compounding process
CN1357613A (en) * 2001-11-22 2002-07-10 成都洁利康实业发展有限公司 Completely fused paper soap and its making process
CN1401753A (en) * 2002-09-23 2003-03-12 辽宁北方华兴机械有限公司 Multifunctional phosphateless washing agent
CN101642415A (en) * 2008-08-04 2010-02-10 河南瑞贝卡发制品股份有限公司 Detergent for human hairs and fiber hairs

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102943002A (en) * 2012-11-21 2013-02-27 浙江雀屏纺织化工股份有限公司 Formula and synthesis process of cashmere environment-friendly swelling agent
CN102943002B (en) * 2012-11-21 2014-04-16 浙江雀屏纺织化工股份有限公司 Formula and synthesis process of cashmere environment-friendly swelling agent
CN103695198A (en) * 2013-12-10 2014-04-02 常熟虞贵人家居用品有限公司 Cloth cleaning agent
CN105154244A (en) * 2015-07-25 2015-12-16 罗贵全 Cleaning liquid for rabbit hair knitted fabric
CN105861176A (en) * 2016-05-11 2016-08-17 张丽鹏 Clothes washing gel and preparation method thereof
CN107385974A (en) * 2017-06-26 2017-11-24 苏州威尔德工贸有限公司 A kind of silk fabric printing with reactive dye soaping agent and preparation method thereof

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