CN102660397A - Detergent for cleaning underwear and preparation method thereof - Google Patents

Detergent for cleaning underwear and preparation method thereof Download PDF

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Publication number
CN102660397A
CN102660397A CN2012100931767A CN201210093176A CN102660397A CN 102660397 A CN102660397 A CN 102660397A CN 2012100931767 A CN2012100931767 A CN 2012100931767A CN 201210093176 A CN201210093176 A CN 201210093176A CN 102660397 A CN102660397 A CN 102660397A
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laureth
stirring
cooled
add
underwear
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CN102660397B (en
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吴巧玲
沈焱
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TIENS GROUP CO Ltd
Tianjin Tiens Biological Development Co Ltd
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TIENS GROUP CO Ltd
Tianjin Tiens Biological Development Co Ltd
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Abstract

The invention discloses a detergent for cleaning underwear and a preparation method thereof. The preparation method comprises the following steps of 1), dissolving triclosan in C9-11 alkanol polyether-3 and coco trimethyl ammonium chloride to obtain a mixed solution, 2), heating disinfected water to a temperature of 85 to 90 DEG C, adding sodium laureth sulfate into the heated disinfected water, carrying out heat preservation and stirring for dissolution, 3), cooling the solution obtained by the step 2 to a temperature of 68 to 72 DEG C, adding laureth-9 and laureth-7 into the solution, carrying out heat preservation, stirring for dissolution, adding borax and anhydrous calcium chloride into the solution and stirring for dissolution, 4), cooling the solution obtained by the step 3 to a temperature of 58 to 62 DEG C, adding C14-17 sodium secondary alkane sulfonate into the solution, and stirring for dissolution, 5), cooling the solution obtained by the step 4 to a temperature of 49 to 52 DEG C, adding the mixed solution obtained by the step 1 into the solution obtained by the step 4, and stirring for dissolution, 6), cooling the solution obtained by the step 5 to a temperature of 46 to 48 DEG C, adding sodium chloride into the solution, carrying out adjustment and uniformly stirring, and 7), cooling the solution obtained by the step 6 to a temperature of 40 to 45 DEG C, and adding alkali protease, methylchloroisothiazolinone, methylisothiazolinone and essence into the solution. The detergent for cleaning underwear can effectively remove blood stains, perspiration stains, milk stains and endocrine. The detergent for cleaning underwear does not contain components such as phosphates, aluminum and a fluorescent brightening agent harmful to the environment and the ecology.

Description

A kind of washing composition that is used to clean in underwear and preparation method thereof
Technical field
The invention belongs to the household cleaning product, clean washing composition of underwear and preparation method thereof specifically.
Background technology
Compare with solid detergent, the angle checking is produced or consumed to liquid washing agent no matter, all can become energy-conservation, economical product.Liquid washing agent has higher technology content, soil removability strong, is convenient to add multiple composition in the production process, the infringement that can effectively avoid high-alkali formulation that clothing and hand skin are caused; The utilization of without phosphorus prescription and tensio-active agent more meets the environment-friendly quality requirement.And pack superior, the convenient use.
Cotton system underwear is because good permeability enjoys people to favor.But the cotton fabric that passes is behind repetitive scrubbing, can occur turning to be yellow at neckline cuff place, the phenomenon of fading, harden, and all can't address these problems with commercially available common washing composition.
Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, the washing composition that is used to clean underwear that provides a kind of can avoid doing washing back neck span and cuff place phenomenon can occur turning to be yellow, fade, harden.
Second purpose of the present invention provides a kind of preparation method who is used to clean the washing composition of underwear.
Technical scheme of the present invention is summarized as follows:
A kind of preparation method who is used to clean the washing composition of underwear comprises the steps:
(1) take by weighing raw material by weight percentage:
Laureth sodium sulfovinate 12-16%; Laureth-94-6%; Laureth-71-3%; C14-17 SAS 1-3%; Sodium-chlor 1.3-3.3%; C9-11 alkanol polyethers-30.25-0.75%; Cocoyl trimethyl ammonium chloride 0.25-0.75%; Calcium Chloride Powder Anhydrous 0.01-0.02%; Sumizyme MP 0.2-0.4%; Triclosan 0.1-0.2%; Methylchloroisothiazandnone 0.01-0.03%; Methylisothiazolinone 0.01-0.03%; Borax 1-2%; Essence 0.1-0.3%; All the other are deionized water;
(2) put into ingredients pot by the accurate weighing deionized water of prescription, stir and be warming up to 78-82 ℃ of sterilization 10-15 minute;
(3) it is subsequent use triclosan to be joined in C9-11 alkanol polyethers-3, the cocoyl trimethyl ammonium chloride sealing of dissolving back;
(4) aqua sterilisa that step (2) is obtained is warming up to 85 ℃-90 ℃ and throws in the laureth sodium sulfovinate, insulation, and fully stirring is all dissolved material;
Add laureth-9, laureth-7 when (5) being cooled to 68-72 ℃, after the insulated and stirred dissolving, add borax, Calcium Chloride Powder Anhydrous, insulated and stirred dissolving;
Add C14-17 SAS, stirring and dissolving when (6) being cooled to 58-62 ℃;
Add the mixed solution that said step (3) obtains when (7) being cooled to 49-52 ℃, the insulated and stirred dissolving;
When (8) being cooled to 46-48 ℃, add sodium-chlor, regulate pH=6-8, stir with Hydrocerol A;
When (9) being cooled to 40~45 ℃, add Sumizyme MP, methylchloroisothiazandnone, methylisothiazolinone, essence, after stirring, be cooled to 36-38 ℃, store in the container after discharging to the sterilization, promptly get the washing composition that is used to clean underwear.
Said essence is orchid odor type essence or Flos Matricariae chamomillae flavor essence.
The washing composition that is used to clean underwear of method for preparing.
Can also add blueness or green pigment.
Can avoid behind the present invention's clothes capable of washing that turning to be yellow can appear in neck span and cuff place, the phenomenon of fading, harden, and effectively remove various fungies, and bloodstain, sweat stain, milk stain, increta etc., and can remove the foreign matter peculiar smell.Character is gentle, and the protection clothing does not damage the hand skin.The protective clothing fibres makes underwear soft, beautiful in colour after washing.Moderate foam is easy to flushing, and is time saving and energy saving.The environmental protection prescription adopts the composite prescription of polynary surface active ingredient, unique biolysis enzyme that adds, and tensio-active agent is biodegradable, not only not phosphorous hydrochlorate, nor contain aluminium, white dyes etc. to environment and ecological objectionable constituent.Add unique fragrance, smell is pure and fresh pleasant.
Embodiment
Embodiment below in conjunction with concrete is further described the present invention.
The proportioning raw materials of embodiment 1-embodiment 5 is seen table 1
Table 1:
Figure BDA0000149655730000021
Embodiment 6
A kind of preparation method who is used to clean the washing composition of underwear comprises the steps:
(1) takes by weighing embodiment 1 listed raw material by weight;
(2) put into ingredients pot by the accurate weighing deionized water of prescription, stir and be warming up to 80 ℃ of sterilizations 13 minutes;
(3) it is subsequent use triclosan to be joined in C9-11 alkanol polyethers-3, the cocoyl trimethyl ammonium chloride sealing of dissolving back;
(4) aqua sterilisa that step (2) is obtained is warming up to 87 ℃ and throws in the laureth sodium sulfovinate, insulation, and fully stirring is all dissolved material;
Add laureth-9, laureth-7 when (5) being cooled to 70 ℃, after the insulated and stirred dissolving, add borax, Calcium Chloride Powder Anhydrous, insulated and stirred dissolving;
Add C14-17 SAS, stirring and dissolving when (6) being cooled to 60 ℃;
Add the mixed solution that said step (3) obtains when (7) being cooled to 50 ℃, the insulated and stirred dissolving;
When (8) being cooled to 47 ℃, add sodium-chlor respectively, regulate pH=7, stir with Hydrocerol A;
When (9) being cooled to 43 ℃, add Sumizyme MP, methylchloroisothiazandnone, methylisothiazolinone, essence, pigment after stirring, is cooled to 37 ℃, stores in the container of discharging to sterilization back, promptly gets the clean-out system that is used for the underwear washing.
Embodiment 7
A kind of preparation method who is used to clean the washing composition of underwear comprises the steps:
(1) takes by weighing embodiment 2 listed raw materials by weight;
(2) put into ingredients pot by the accurate weighing deionized water of prescription, stir and be warming up to 78 ℃ of sterilizations 15 minutes;
(3) it is subsequent use triclosan to be joined in C9-11 alkanol polyethers-3, the cocoyl trimethyl ammonium chloride sealing of dissolving back;
(4) aqua sterilisa that step (2) is obtained is warming up to 85 ℃ and throws in the laureth sodium sulfovinate, insulation, and fully stirring is all dissolved material;
Add laureth-9, laureth-7 when (5) being cooled to 68 ℃, after the insulated and stirred dissolving, add borax, Calcium Chloride Powder Anhydrous, insulated and stirred dissolving;
Add C14-17 SAS, stirring and dissolving when (6) being cooled to 58 ℃;
Add the mixed solution that said step (3) obtains when (7) being cooled to 49 ℃, the insulated and stirred dissolving;
When (8) being cooled to 46 ℃, add sodium-chlor, regulate pH=8, stir with Hydrocerol A;
When (9) being cooled to 40 ℃, add Sumizyme MP, methylchloroisothiazandnone, methylisothiazolinone, essence, pigment after stirring, is cooled to 36 ℃, stores in the container after discharging to the sterilization, promptly gets the washing composition that is used to clean underwear.
Embodiment 8
A kind of preparation method who is used to clean the washing composition of underwear comprises the steps:
(1) takes by weighing embodiment 3 listed raw materials by weight;
(2) put into ingredients pot by the accurate weighing deionized water of prescription, stir and be warming up to 82 ℃ of sterilizations 10 minutes;
(3) it is subsequent use triclosan to be joined in C9-11 alkanol polyethers-3, the cocoyl trimethyl ammonium chloride sealing of dissolving back;
(4) aqua sterilisa that step (2) is obtained is warming up to 90 ℃ and throws in the laureth sodium sulfovinate, insulation, and fully stirring is all dissolved material;
Add laureth-9, laureth-7 when (5) being cooled to 72 ℃, after the insulated and stirred dissolving, add borax, Calcium Chloride Powder Anhydrous, insulated and stirred dissolving;
Add C14-17 SAS, stirring and dissolving when (6) being cooled to 62 ℃;
Add the mixed solution that said step (3) obtains when (7) being cooled to 52 ℃, the insulated and stirred dissolving;
When (8) being cooled to 48 ℃, add sodium-chlor, regulate pH=6, stir with Hydrocerol A;
When (9) being cooled to 45 ℃, add Sumizyme MP, methylchloroisothiazandnone, methylisothiazolinone, essence, pigment after stirring, is cooled to 38 ℃, stores in the container after discharging to the sterilization, promptly gets the washing composition that is used to clean underwear.
Embodiment 9
A kind of preparation method who is used to clean the washing composition of underwear comprises the steps:
(1) takes by weighing embodiment 4 listed raw materials by weight;
(2)-(9) with embodiment 6
Embodiment 10
A kind of preparation method who is used to clean the washing composition of underwear comprises the steps:
(1) takes by weighing embodiment 5 listed raw materials by weight;
(2)-(9) with embodiment 6
Embodiment 11
Effect experiment 1:
Get 18 underwears (upper and lower clothing one cover) of wearing 5 days, be divided into 6 groups at random, every group 3 cover, the 1st group is with commercially available common washing composition, machine washing, water consumption 10L, clean-out system consumption 20mL; The 2-6 group is followed successively by the washing composition that is used to clean underwear of embodiment 6-10 preparation, water consumption 10L, clean-out system consumption 10mL; Each warm water soaking 20 minutes before washing, the 1st group when using 20 minutes, underwear is cleaned, the 2-6 group time spent was followed successively by 14,15,15,14 and 15 minutes, and underwear is cleaned.
Experimental result shows, the washing composition soil removability that is used to clean underwear of the present invention is strong, the clean nondiscoloration in neckline and cuff place, and the soft smell of underwear is pure and fresh.
Effect experiment 2:
Get 36 blocks of cotton clothes, every 30cm * 30cm, 18 brush milk are placed 60mim, are divided into 6 groups at random, 3 every group; Catch chicken blood for 18, place 60mim, be divided into 6 groups at random, the 1st group (3 brush milk, 3 cotton cloths of catching chicken blood) with commercially available common washing composition, are machine-washed water consumption 10L, clean-out system consumption 20mL; 2-6 group (every group has 3 brush milk, 3 cotton cloths of catching chicken blood) is followed successively by the washing composition that is used to clean underwear of embodiment 6-10 preparation, water consumption 10L, clean-out system consumption 10mL; Each warm water soaking 20 minutes before washing, the 1st group when using 24 minutes, cloth is cleaned, 2-6 organize 18 minutes times spent, and cloth is clean.
Experimental result shows, the washing composition that is used to clean underwear of the present invention can be removed bloodstain and milk stain effectively.

Claims (3)

1. a preparation method who is used to clean the washing composition of underwear is characterized in that comprising the steps:
(1) take by weighing raw material by weight percentage:
Laureth sodium sulfovinate 12-16%; Laureth-94-6%; Laureth-71-3%; C14-17 SAS 1-3%; Sodium-chlor 1.3-3.3%; C9-11 alkanol polyethers-30.25-0.75%; Cocoyl trimethyl ammonium chloride 0.25-0.75%; Calcium Chloride Powder Anhydrous 0.01-0.02%; Sumizyme MP 0.2-0.4%; Triclosan 0.1-0.2%; Methylchloroisothiazandnone 0.01-0.03%; Methylisothiazolinone 0.01-0.03%; Borax 1-2%; Essence 0.1-0.3%; All the other are deionized water;
(2) put into ingredients pot by the accurate weighing deionized water of prescription, stir and be warming up to 78-82 ℃ of sterilization 10-15 minute;
(3) it is subsequent use triclosan to be joined in C9-11 alkanol polyethers-3, the cocoyl trimethyl ammonium chloride sealing of dissolving back;
(4) aqua sterilisa that step (2) is obtained is warming up to 85 ℃-90 ℃ and throws in the laureth sodium sulfovinate, insulation, and fully stirring is all dissolved material;
Add laureth-9, laureth-7 when (5) being cooled to 68-72 ℃, after the insulated and stirred dissolving, add borax, Calcium Chloride Powder Anhydrous, insulated and stirred dissolving;
Add C14-17 SAS, stirring and dissolving when (6) being cooled to 58-62 ℃;
Add the mixed solution that said step (3) obtains when (7) being cooled to 49-52 ℃, the insulated and stirred dissolving;
When (8) being cooled to 46-48 ℃, add sodium-chlor, regulate pH=6-8, stir with Hydrocerol A;
When (9) being cooled to 40~45 ℃, add Sumizyme MP, methylchloroisothiazandnone, methylisothiazolinone, essence, after stirring, be cooled to 36-38 ℃, store in the container after discharging to the sterilization, promptly get the washing composition that is used to clean underwear.
2. a kind of preparation method who is used to clean the washing composition of underwear according to claim 1 is characterized in that said essence is orchid odor type essence or Flos Matricariae chamomillae flavor essence.
3. the washing composition that is used to clean underwear of claim 1 or the preparation of 2 described methods.
CN201210093176.7A 2012-03-31 2012-03-31 A kind of for washing composition cleaning underwear and preparation method thereof Expired - Fee Related CN102660397B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103740492A (en) * 2013-12-27 2014-04-23 天津天狮生物发展有限公司 Concentrated washing solution and preparation method thereof
CN103897870A (en) * 2012-12-26 2014-07-02 青岛锦涟鑫商贸有限公司 Novel easily-degradable washing agent
CN104629956A (en) * 2013-11-12 2015-05-20 青岛锦涟鑫商贸有限公司 Woolen clothes cleaning compound
CN107603758A (en) * 2017-10-13 2018-01-19 洛娃科技实业集团有限公司 A kind of liquid detergent and preparation method
CN108913385A (en) * 2018-06-20 2018-11-30 深圳市三浦天然化妆品有限公司 A kind of antibacterial cleaning solution of plant herbal
CN112791206A (en) * 2021-03-29 2021-05-14 许卓辉 Production process flow of disposable underpants for first wearing

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102154068A (en) * 2011-03-03 2011-08-17 天津天狮生物发展有限公司 Multifunctional detergent and preparation method thereof
CN102242022A (en) * 2011-06-15 2011-11-16 于文 Environment-friendly type hyperconcentration biological enzyme liquid laundry detergent and preparation method thereof
CN102277241A (en) * 2011-07-20 2011-12-14 江苏爱特福84股份有限公司 Radiation-proof cleaning agent dedicated for clothes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102154068A (en) * 2011-03-03 2011-08-17 天津天狮生物发展有限公司 Multifunctional detergent and preparation method thereof
CN102242022A (en) * 2011-06-15 2011-11-16 于文 Environment-friendly type hyperconcentration biological enzyme liquid laundry detergent and preparation method thereof
CN102277241A (en) * 2011-07-20 2011-12-14 江苏爱特福84股份有限公司 Radiation-proof cleaning agent dedicated for clothes

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103897870A (en) * 2012-12-26 2014-07-02 青岛锦涟鑫商贸有限公司 Novel easily-degradable washing agent
CN104629956A (en) * 2013-11-12 2015-05-20 青岛锦涟鑫商贸有限公司 Woolen clothes cleaning compound
CN103740492A (en) * 2013-12-27 2014-04-23 天津天狮生物发展有限公司 Concentrated washing solution and preparation method thereof
CN107603758A (en) * 2017-10-13 2018-01-19 洛娃科技实业集团有限公司 A kind of liquid detergent and preparation method
CN108913385A (en) * 2018-06-20 2018-11-30 深圳市三浦天然化妆品有限公司 A kind of antibacterial cleaning solution of plant herbal
CN112791206A (en) * 2021-03-29 2021-05-14 许卓辉 Production process flow of disposable underpants for first wearing

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