CN103468446A - Soap base surfactant-containing laundry detergent and preparation method thereof - Google Patents
Soap base surfactant-containing laundry detergent and preparation method thereof Download PDFInfo
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- CN103468446A CN103468446A CN2013104229547A CN201310422954A CN103468446A CN 103468446 A CN103468446 A CN 103468446A CN 2013104229547 A CN2013104229547 A CN 2013104229547A CN 201310422954 A CN201310422954 A CN 201310422954A CN 103468446 A CN103468446 A CN 103468446A
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Abstract
The invention discloses a soap base surfactant-containing laundry detergent and a preparation method thereof. The soap base surfactant-containing laundry detergent is composed of a soap base surfactant, an anionic surfactant, a nonionic surfactant, a skin care agent, a fluorescent brightener, a water softener, a chelating agent, a preservative, a pH value regulator and essences. The laundry detergent is characterized in that the soap base surfactant is added to the system so that multiple surfactants are compounded in the laundry detergent system, and the skin care agent is also contained, therefore, the laundry detergent has the advantages of high detersive power, low foam, easy rinsing, no harm on hand, stable storage at low temperatures and the like.
Description
Technical field
The invention belongs to detergent applications, be specifically related to a kind of soap base surfactant washing liquid and preparation method thereof that contains.
Background technology
Along with the raising of living standards of the people and the quickening of rhythm of life, also more and more higher to the requirement of washing liquid, develop also very soon, decontamination is strong, easily rinsing, do not hinder hand, cleaning product easy to use more and more enjoys human consumer's favor.Aggravated like this environmental pollution caused therefrom, therefore, the washing liquid of exploitation efficient context, the consumption of the main component tensio-active agent of the consumption of reduction washing liquid or reduction washing liquid is the effective way of environmental contamination reduction.At present, the washing liquid product category on market is various, a feast for the eyes, and great majority washings clean effects are better, but it is many to use foam, is not easy rinsing, and time-consuming water wasting more or less causes certain stimulation to skin on hand during the hand washing clothing.
Summary of the invention
The objective of the invention is for above-mentioned the deficiencies in the prior art, a kind of high-effective cleansing, easily rinsing be provided, do not hinder hand, effectively reduce the quantity discharged of actives in the washing liquid discharge process, environmental contamination reduction contain the soap base surfactant washing liquid.
Another goal of the invention of the present invention is to provide the preparation method of this Xian's clothing liquid.
The technical solution adopted in the present invention is:
A kind of soap base surfactant washing liquid that contains, by the component of following mass percent, made:
Soap base surfactant 5%～20%, anion surfactant 5%～20%, nonionogenic tenside 2%～10%, skin-protecting agent 2%～5%, white dyes 0.01%～0.2%, water softener 2%～10%, sequestrant 0.1%～0.5%, sanitas 0.05%～0.1%, pH value conditioning agent 0.2%～1%, essence 0.2%～0.8%; Water surplus.
Further, described soap base surfactant is one or both the mixture in oleic acid potash soap, palmitinic acid potash soap.
Described anion surfactant is two or more mixture of alkylbenzene sulfonate (LAS), fatty alcohol polyoxyethylene ether sulfate (AES), ɑ-alkenyl sulphonate (AOS).
Described nonionogenic tenside is one or both the mixture of fatty alcohol-polyoxyethylene ether AEO-9, AEO-7.
Described skin-protecting agent is one or both mixtures in glycerol (glycerine) and sorbic alcohol.
Described white dyes be double styrene-biphenyl type optical whitening agent with two triazines diphenyl ethylene derivatives in one or both mixture.
Described water softener is Citrate trianion.
Described sequestrant is one or both mixture of disodium EDTA, tetrasodium salt of EDTA.
Described PH conditioning agent is any one in citric acid, trolamine, sodium hydroxide.
A kind of preparation method who contains the soap base surfactant washing liquid of the present invention, comprise the following steps
Step 1: each component is got the raw materials ready according to following mass percent:
Soap base surfactant 5%～20%, anion surfactant 5%～20%, nonionogenic tenside 2%～10%, skin-protecting agent 2%～5%, white dyes 0.01%～0.2%, water softener 2%～10%, sequestrant 0.1%～0.5%, sanitas 0.05%～0.1%, pH value conditioning agent 0%～1%, essence 0.2%～0.8%; Water surplus.
Step 2: the soap base surfactant in filling a prescription, add in reactor and add the water of surplus, start to stir, and be warming up to 50～55 ℃, then stir 30 minutes;
Step 3: added successively again anion surfactant, nonionogenic tenside, skin-protecting agent, white dyes, water softener, sequestrant, PH conditioning agent every 5 minutes, after adding, stir again 20 minutes, regulating pH value is 8.5～9.5, be cooled to 35～40 ℃, add sanitas and essence, then continue to stir 20 minutes;
Step 4: work in-process carry out ripening and make evenly bright washing liquid.
The present invention compared with prior art, have the following advantages: 1, soap base surfactant adds the polynary surfactant compound that made System forming, effectively improved the soil removability of washing liquid, the more important thing is the latherability that has reduced the washing liquid system, under the prerequisite that keeps the soluble characteristics of washing liquid, especially easily rinsing, water saving, save time, soap base surfactant is lower to skin irritation simultaneously, added in addition the glycerine of skin care composition in system, the hand washing clothing has played the effect that hand is not hindered in skin care.2, production technique is simple, and cost is low, soluble in water, and to fabric noresidue not damaged, easy to use, market potential is large.
Embodiment
Embodiment 1:
A kind of preparation method who contains the soap base surfactant washing liquid of the present invention, comprise the following steps
Step 1: each component is got the raw materials ready according to following mass percent:
Get fatty alcohol-polyoxyethylene ether AEO-9, glycerol (glycerine) 2%, double styrene-biphenyl type optical whitening agent 0.01%, Citrate trianion 2%, disodium EDTA 0.1%, sanitas 0.05%, citric acid 0.2%, essence 0.2%, the water 83% of oleic acid potash soap 5%, alkylbenzene sulfonate (LAS) and fatty alcohol polyoxyethylene ether sulfate (AES) mixture 5%, 2%.
Step 2: the oleic acid potash soap in filling a prescription, add in reactor and add 83% water, start to stir, and be warming up to 50 ℃, then stir 30 minutes;
Step 3: added successively again alkylbenzene sulfonate (LAS) and fatty alcohol polyoxyethylene ether sulfate (AES) mixture, fatty alcohol-polyoxyethylene ether AEO-9, glycerol (glycerine), double styrene-biphenyl type optical whitening agent, Citrate trianion, disodium EDTA, citric acid every 5 minutes, after adding, stir again 20 minutes, regulating pH value is 8.5, be cooled to 35 ℃, add sanitas and essence, then continue to stir 20 minutes;
Step 4: work in-process carry out ripening and make evenly bright washing liquid.
Embodiment 2:
A kind of preparation method who contains the soap base surfactant washing liquid of the present invention, comprise the following steps
Step 1: each component is got the raw materials ready according to following mass percent:
The AEO-7 of palmitinic acid potash soap 20%, ɑ-alkenyl sulphonate (AOS) 20%, 10%, sorbic alcohol 5%, two triazines diphenyl ethylene derivatives 0.2%, Citrate trianion 10%, tetrasodium salt of EDTA 0.5%, sanitas 0.1%, trolamine 1%, essence 0.8%; Water 67%.
Step 2: the palmitinic acid potash soap in filling a prescription, add in reactor and add the water of surplus, start to stir, and be warming up to 55 ℃, then stir 30 minutes;
Step 3: added successively again ɑ-alkenyl sulphonate (AOS), AEO-7, sorbic alcohol, two triazines diphenyl ethylene derivatives, Citrate trianion, tetrasodium salt of EDTA, trolamine every 5 minutes, after adding, stir again 20 minutes, regulating pH value is 9.5, be cooled to 40 ℃, add sanitas and essence, then continue to stir 20 minutes;
Step 4: work in-process carry out ripening and make evenly bright washing liquid.
Embodiment 3:
A kind of preparation method who contains the soap base surfactant washing liquid of the present invention, comprise the following steps
Step 1: each component is got the raw materials ready according to following mass percent:
The oleic acid potash soap, the mixture 15% of palmitinic acid potash soap, alkylbenzene sulfonate (LAS), the mixture 15% of fatty alcohol polyoxyethylene ether sulfate (AES) and ɑ-alkenyl sulphonate (AOS), the mixture 7% of fatty alcohol-polyoxyethylene ether AEO-9 and AEO-7, the mixture 4% of glycerol (glycerine) and sorbic alcohol, the mixture 0.1% of double styrene-biphenyl type optical whitening agent and two triazines diphenyl ethylene derivatives, Citrate trianion 6%, the mixture 0.3% of disodium EDTA and tetrasodium salt of EDTA, sanitas 0.08%, sodium hydroxide 0.05%, essence 0.6%, water 50%.
Step 2: the oleic acid potash soap in filling a prescription, the mixture of palmitinic acid potash soap, add in reactor and add the water of surplus, start to stir, and be warming up to 52 ℃, then stir 30 minutes;
Step 3: the mixture, Citrate trianion, sequestrant, the sodium hydroxide that added successively again mixture, double styrene-biphenyl type optical whitening agent and two triazines diphenyl ethylene derivatives of mixture, glycerol (glycerine) and the sorbic alcohol of mixture, fatty alcohol-polyoxyethylene ether AEO-9 and the AEO-7 of fatty alcohol polyoxyethylene ether sulfate (AES) and ɑ-alkenyl sulphonate (AOS) every 5 minutes, after adding, stir again 20 minutes, regulating pH value is 9, be cooled to 37 ℃, add sanitas and essence, then continue to stir 20 minutes;
Step 4: work in-process carry out ripening and make evenly bright washing liquid.
Claims (10)
1. one kind contains the soap base surfactant washing liquid, it is characterized in that: the component by following mass percent is made:
Soap base surfactant 5%～20%, anion surfactant 5%～20%, nonionogenic tenside 2%～10%, skin-protecting agent 2%～5%, white dyes 0.01%～0.2%, water softener 2%～10%, sequestrant 0.1%～0.5%, sanitas 0.05%～0.1%, pH value conditioning agent 0.2%～1%, essence 0.2%～0.8%; Water surplus.
2. a kind of soap base surfactant washing liquid that contains according to claim 1 is characterized in that: described soap base surfactant is one or both the mixture in oleic acid potash soap, palmitinic acid potash soap.
3. a kind of soap base surfactant washing liquid that contains according to claim 1, it is characterized in that: described anion surfactant is two or more mixture of alkylbenzene sulfonate (LAS), fatty alcohol polyoxyethylene ether sulfate (AES), ɑ-alkenyl sulphonate (AOS).
4. a kind of soap base surfactant washing liquid that contains according to claim 1 is characterized in that: described nonionogenic tenside is one or both the mixture of fatty alcohol-polyoxyethylene ether AEO-9, AEO-7.
5. a kind of soap base surfactant washing liquid that contains according to claim 1 is characterized in that: described skin-protecting agent be glycerol (glycerine) with sorbic alcohol in one or both mixtures.
6. a kind of soap base surfactant washing liquid that contains according to claim 1 is characterized in that: described white dyes be double styrene-biphenyl type optical whitening agent with two triazines diphenyl ethylene derivatives in one or both mixture.
7. a kind of soap base surfactant washing liquid that contains according to claim 1, it is characterized in that: described water softener is Citrate trianion.
8. a kind of soap base surfactant washing liquid that contains according to claim 1 is characterized in that: described sequestrant is one or both mixture of disodium EDTA, tetrasodium salt of EDTA.
9. a kind of soap base surfactant washing liquid that contains according to claim 1, it is characterized in that: described PH conditioning agent is any one in citric acid, trolamine, sodium hydroxide.
10. a preparation method who contains the soap base surfactant washing liquid, is characterized in that: comprise the following steps
Step 1: each component is got the raw materials ready according to following mass percent:
Soap base surfactant 5%～20%, anion surfactant 5%～20%, nonionogenic tenside 2%～10%, skin-protecting agent 2%～5%, white dyes 0.01%～0.2%, water softener 2%～10%, sequestrant 0.1%～0.5%, sanitas 0.05%～0.1%, pH value conditioning agent 0.2%～1%, essence 0.2%～0.8%; Water surplus.
Step 2: the soap base surfactant in filling a prescription, add in reactor and add the water of surplus, start to stir, and be warming up to 50～55 ℃, then stir 30 minutes;
Step 3: added successively again anion surfactant, nonionogenic tenside, skin-protecting agent, white dyes, water softener, sequestrant, PH conditioning agent every 5 minutes, after adding, stir again 20 minutes, regulating pH value is 8.5～9.5, be cooled to 35～40 ℃, add sanitas and essence, then continue to stir 20 minutes;
Step 4: work in-process carry out ripening and make evenly bright washing liquid.
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Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104087453A (en) * | 2014-07-16 | 2014-10-08 | 福建广和堂生物科技有限公司 | Naringin-containing strong-decontamination antibacterial liquid detergent and preparation method thereof |
| CN104232359A (en) * | 2014-09-28 | 2014-12-24 | 山西青山化工有限公司 | Stilbene bistriazine liquid whitening agent and preparation method thereof |
| CN104845781A (en) * | 2015-06-15 | 2015-08-19 | 马建剑 | Novel towel decontamination liquid soap and preparation method thereof |
| CN105238099A (en) * | 2015-10-12 | 2016-01-13 | 山西青山化工有限公司 | Liquid fluorescent whitening agent for whitening soup and preparation method thereof |
| CN105386315A (en) * | 2015-12-07 | 2016-03-09 | 常熟市永新印染有限公司 | After-finishing process for knitted fabric |
| CN105505606A (en) * | 2015-12-21 | 2016-04-20 | 王旭明 | Laundry detergent |
| CN106281819A (en) * | 2016-08-09 | 2017-01-04 | 冯鲜花 | A kind of suction color laundry sheet and manufacture method thereof |
| CN106318734A (en) * | 2015-06-19 | 2017-01-11 | 镇江市润州金山包装厂 | Cloth wrapper cleaning compound |
| CN106566686A (en) * | 2016-10-12 | 2017-04-19 | 重庆市五洁新材料有限公司 | Efficient and environment-friendly laundry detergent and preparation method thereof |
| CN107254374A (en) * | 2017-07-27 | 2017-10-17 | 合肥远科服装设计有限公司 | A kind of multifunctional laundry liquid |
| CN108865535A (en) * | 2018-04-20 | 2018-11-23 | 中山市美而廉清洁用品有限公司 | A kind of three-in-one bleaching laundry soap lye |
| CN109055058A (en) * | 2018-08-24 | 2018-12-21 | 中山市洁莹生物科技有限公司 | A kind of plant bacteriostatic hand sanitizer and preparation method thereof |
| CN109072139A (en) * | 2016-05-24 | 2018-12-21 | 荷兰联合利华有限公司 | detergent composition |
| CN110408487A (en) * | 2019-08-27 | 2019-11-05 | 如皋市涤诺皂业有限公司 | A kind of padded equipment liquid detergent and preparation method thereof with pearly-lustre |
| CN111269764A (en) * | 2020-02-28 | 2020-06-12 | 山东丽波日化股份有限公司 | Hand washing liquid detergent and preparation method thereof |
| CN111286426A (en) * | 2019-12-24 | 2020-06-16 | 纳爱斯浙江科技有限公司 | Neutral soap-based easy-rinsing liquid detergent composition |
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| CN103013723A (en) * | 2012-12-21 | 2013-04-03 | 纳爱斯集团有限公司 | Low-foam laundry detergent composite facilitating rinsing |
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Patent Citations (2)
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| CN1218106A (en) * | 1997-11-25 | 1999-06-02 | 李言松 | Liquid soap |
| CN103013723A (en) * | 2012-12-21 | 2013-04-03 | 纳爱斯集团有限公司 | Low-foam laundry detergent composite facilitating rinsing |
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104087453A (en) * | 2014-07-16 | 2014-10-08 | 福建广和堂生物科技有限公司 | Naringin-containing strong-decontamination antibacterial liquid detergent and preparation method thereof |
| CN104232359A (en) * | 2014-09-28 | 2014-12-24 | 山西青山化工有限公司 | Stilbene bistriazine liquid whitening agent and preparation method thereof |
| CN104845781A (en) * | 2015-06-15 | 2015-08-19 | 马建剑 | Novel towel decontamination liquid soap and preparation method thereof |
| CN106318734A (en) * | 2015-06-19 | 2017-01-11 | 镇江市润州金山包装厂 | Cloth wrapper cleaning compound |
| CN105238099A (en) * | 2015-10-12 | 2016-01-13 | 山西青山化工有限公司 | Liquid fluorescent whitening agent for whitening soup and preparation method thereof |
| CN105238099B (en) * | 2015-10-12 | 2017-07-07 | 山西青山化工有限公司 | One kind brightens soap liquid fluorescent whitening agent and preparation method thereof |
| CN105386315A (en) * | 2015-12-07 | 2016-03-09 | 常熟市永新印染有限公司 | After-finishing process for knitted fabric |
| CN105505606A (en) * | 2015-12-21 | 2016-04-20 | 王旭明 | Laundry detergent |
| CN109072139A (en) * | 2016-05-24 | 2018-12-21 | 荷兰联合利华有限公司 | detergent composition |
| CN106281819A (en) * | 2016-08-09 | 2017-01-04 | 冯鲜花 | A kind of suction color laundry sheet and manufacture method thereof |
| CN106566686A (en) * | 2016-10-12 | 2017-04-19 | 重庆市五洁新材料有限公司 | Efficient and environment-friendly laundry detergent and preparation method thereof |
| CN107254374A (en) * | 2017-07-27 | 2017-10-17 | 合肥远科服装设计有限公司 | A kind of multifunctional laundry liquid |
| CN108865535A (en) * | 2018-04-20 | 2018-11-23 | 中山市美而廉清洁用品有限公司 | A kind of three-in-one bleaching laundry soap lye |
| CN109055058A (en) * | 2018-08-24 | 2018-12-21 | 中山市洁莹生物科技有限公司 | A kind of plant bacteriostatic hand sanitizer and preparation method thereof |
| CN110408487A (en) * | 2019-08-27 | 2019-11-05 | 如皋市涤诺皂业有限公司 | A kind of padded equipment liquid detergent and preparation method thereof with pearly-lustre |
| CN111286426A (en) * | 2019-12-24 | 2020-06-16 | 纳爱斯浙江科技有限公司 | Neutral soap-based easy-rinsing liquid detergent composition |
| CN111286426B (en) * | 2019-12-24 | 2021-01-15 | 纳爱斯浙江科技有限公司 | Neutral soap-based easy-rinsing liquid detergent composition |
| CN111269764A (en) * | 2020-02-28 | 2020-06-12 | 山东丽波日化股份有限公司 | Hand washing liquid detergent and preparation method thereof |
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Application publication date: 20131225 |