CN104018232A - Degumming process of apocynum venetum fiber - Google Patents
Degumming process of apocynum venetum fiber Download PDFInfo
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- CN104018232A CN104018232A CN201410301221.2A CN201410301221A CN104018232A CN 104018232 A CN104018232 A CN 104018232A CN 201410301221 A CN201410301221 A CN 201410301221A CN 104018232 A CN104018232 A CN 104018232A
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Abstract
The invention discloses a degumming process of an apocynum venetum fiber, which belongs to the field of spinning. The apocynum venetum fiber is prepared by boiling wild apocynum venetum straw with water, degumming, beating, dehydrating, drying, nourishing, loosening, carding and packaging. By adopting the process, the apocynum venetum fiber is good in degumming effect, the apocynum venetum fiber yield is high, 1 ton of apocynum venetum fiber can be prepared from 2-2.5 tons of apocynum venetum peel, the apocynum venetum fiber can be blended with cotton to produce high count yarn more than 40S, a fabric can be made into various home textiles, paints, socks, quilts, summer sleeping mats, pillows and the like, and has the unique functions of natural bacteriostasis and human body beneficial far infrared ray emission.
Description
Technical field
The degumming tech of apocynum fibre of the present invention belongs to field of textiles.
Background technology
Present widely used cotton products are as cotton-wadded quilt, in the sombre moist environment in winter of south, and because easy moisture absorption very easily causes the moisture absorption, breed bacteria, growth mildew, has peculiar smell.Bluish dogbane (Apocynum venetum linn) is the distinctive wild plant of Xinjiang of China Lop Nur desert area, be called as " king of fiber ", in 530-531 pages of 1975-1979 " traditional Chinese medicine research " literature summaries that Beijing Science Press 1986 publishes, Liu Shoushan writes articles and points out: bluish dogbane is unique a kind of fibre plant that can natural emitting biological ripple, there is cotton softness, the gloss of silk, numb is smooth.Apocynum fibre is in the Wild fiber plant of having found, best in quality, is the superior raw material of weaving, papermaking, and apocynum fibre and cotton blending, can have the two advantage concurrently, becomes a desirable woven material.Bluish dogbane cold nature, bitter but sweet flavor, can heat-clearing and fire-reducing, and suppressing hyperactive liver for calming endogenous wind cures mainly the diseases such as headache, dizzy, insomnia, and numb leaf contains bluish dogbane flavones, has cardiotonic, and dogbane tea, bluish dogbane tablet and the bluish dogbane cigarette etc. made can be treated the diseases such as high blood pressure.
At present, the general method that bluish dogbane skin is put into the cuboid pond kiering that iron plate makes that adopts is obtained apocynum fibre, and there are the following problems for it:
1. the kiering time long because pool inner water does not circulate, jute fiber degumming degree is irregular, degumming effect is bad;
2. because can not pickling in iron pond, washing, must pull apocynum fibre out and drop into again the artificial pickling of cement pit, washing, both increased processing cost, increase again labor strength;
3. without comb suede, the flax fibre row yielding obtaining is not high, just can make 1 ton of shredding flax fibre through boiling 3.6 tons of numb skins of numb shredding, row yielding only 28%.Flax fibre number is low, below 2500 public.Flax fibre and cotton blended yarn, its proportion only reaches 35:65, can only spin 21 English and prop up following yarn.Prop up above high-count yarn owing to spinning 40 English, require apocynum fibre number to reach more than 4000 public, cannot realize this purpose therefore tradition is obtained the method for apocynum fibre.
Summary of the invention
The object of the present invention is to provide a kind of degumming effect good, can improve the degumming tech of the apocynum fibre of flax fibre row yielding.
Process:
1, poach: harvesting is grown in the wild venetum bar in Xinjiang Weili border of the county during annual March in November to the coming year, spread out natural drying and made it air-dry in 3 days, by spreading out waste of flax: the weight ratio of water=1:5, input is equipped with in the cement pit of water steam heating tube at the bottom of pond.Pool inner water is warming up to 60-70 °, makes to spread out waste of flax and be incubated 3-4 hours in pond, pull out and put ground, treat that it drops to outdoor temperature naturally, numb skin under peel manually;
2, come unstuck: by bluish dogbane skin: water=1: 8 weight ratio, packs bluish dogbane skin 300kg, clear water 2400kg in the cylinder of the loose fine degumming machine of bluish dogbane, as follows operation:
A: water is warming up to 40-45 degree, then opens the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 15 minutes, drain flushing water in cylinder, put into external purification pond, treat after self-purification that used next time;
B: to the sulfuric acid 5kg that puts into clear water 2400kg, concentration 98% in cylinder, water is warming up to 30-40 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, to numb skin rinse 35 minutes, also cry pickling, drain flushing liquor in cylinder, put into external purification pond, after self-purification, treat that used next time;
C: put into clear water 2400kg in cylinder, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 25 minutes, drain flushing water in cylinder, put into external purification pond, treat after self-purification that used next time;
D: put into caustic soda (NaOH) 15kg of clear water 2400kg, concentration 96%, the soda ash (Na of concentration 96% in cylinder
2cO
3) 18kg, water is warming up to 90-100 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, at this temperature, to numb skin kiering 120 minutes, drain flushing liquor in cylinder, put into external purification pond, after self-purification, treat that used next time;
E: put into clear water 2400kg in cylinder, water is warming up to 50-60 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 50 minutes, drain flushing water in cylinder, put into external purification pond, after self-purification, treat that used next time;
F: to the SI-101 softener 10kg that puts into clear water 2400kg, concentration 50% in cylinder, water is warming up to 35-40 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed and within 50 minutes, makes it soft, drain flushing liquor in cylinder, put into external purification pond, after self-purification, treat to use next time, take out apocynum fibre;
3, copy fiber crops: the apocynum fibre 30kg after coming unstuck is placed on circular flax stamping device, by 12 on this machine wooden fiber crops hammers that strike, the apocynum fibre on disk is beaten 5 times, be that flax stamping device disk rotates 5 circles, during this, uninterruptedly rinse apocynum fibre with the automatic flushing machine on this machine, the pectin on it is all removed;
4, dehydration: the apocynum fibre of copying is dropped into the dehydration of the loose hair of cage Water Extraction Machinery;
5, dry: the apocynum fibre that took off water is dropped into loose fibre dryer, under temperature 100-105 degree, dry 0.5-1 hour, obtain keen-witted and capable apocynum fibre.
6, health: keen-witted and capable apocynum fibre is added to wet process, and the keen-witted and capable apocynum fibre lay of every 1000kg ground, spreads water 200 kg with humidification pump, make its moisture reach 20%, then insert temperature 30-35 degree, in the warehouse of relative humidity 60-65%, stack health 6-7 days;
7, shredding: the good apocynum fibre of health is dropped into multi-functional garnett, utilize 3 circular air draught dust cages on machine to remove impurity and breaking bar;
8, divide comb: apocynum fibre good shredding being dropped into carding machine, comb suede, is that short flannel divides comb to fall by doubling and the fiber below length 16mm;
9, packing: a point apocynum fibre packaging and warehousing of having combed, stand-by.
In national textile fabrics quality surveillance, spin Co., Ltd of mark Beijing inspection authentication center in the heart in the fabric to apocynum fibre, apocynum fibre and cotton blending gained, nine detections of product of making respectively on October 12nd, 1 2013 on September 15th, 2010, result is as following table:
September 15 2010 date of issuance
Report is made numbering (№) BA10005826-1
Sample title: bluish dogbane fabric
Sample message: white/green woven fabric 50% apocynum fibre 50% cotton
Test item is as follows:
Gas permeability 268mm/s
Poisture-penetrability 7.88 × 10
3g/ (m2.d)
Examining report 2
September 15 2010 date of issuance
Report is made numbering (№) BA10005826-2
Sample title: apocynum fibre
Sample message: essential color fiber 100% apocynum fibre
Test item is as follows:
Candida albicans (ATCC10231) bacteriostasis rate 97%
Escherichia coli (8099) bacteriostasis rate 95%
Klebsiella pneumoniae (ATCC4352) bacteriostasis rate 97%
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate 99%
Far infrared normal emittance 80%
Examining report 3
June 7 2011 date of issuance
Report is made numbering (№) BA11001261
Sample title: bluish dogbane fabric
Sample message: white woven fabric 30% apocynum fibre 70% cotton
Test item is as follows:
Gas permeability 471mm/s
Poisture-penetrability 11110 g/ (m2.d)
Far infrared normal emittance 80%
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate 60%
Klebsiella pneumoniae (ATCC4352) bacteriostasis rate 93%
Candida albicans (ATCC10231) bacteriostasis rate 97%
Escherichia coli (8099) bacteriostasis rate 89%
Examining report 4
August 15 2011 date of issuance
Report is made numbering (№) BA11003396S
Sample title: apocynum fibre
Sample message: white fiber 60% apocynum fibre 40% cotton
Test item is as follows:
Candida albicans (ATCC10231) bacteriostasis rate 75%
Escherichia coli (8099) bacteriostasis rate 99%
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate 99%
Klebsiella pneumoniae (ATCC4352) bacteriostasis rate 63%
Far infrared normal emittance 76%
Examining report 5
September 8 2011 date of issuance
Report is made numbering (№) BA11004217
Sample title: apocynum fibre
Sample message: color 60% apocynum fibre 40% cotton of white fiber
Test item is as follows:
Escherichia coli (8099) bacteriostasis rate 94%
Examining report 6
December 25 2012 date of issuance
Report is made numbering (№) BA12002583
Sample title: apocynum fibre
Sample message: colour of camel's hair apocynum fibre apocynum fibre 100 %
Test item is as follows:
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate > 99%
Examining report 7
August 15 2013 date of issuance
Report is made numbering (№) BA13001696-1
Sample title: apocynum fibre
Sample message: white fiber
Test item is as follows:
Far infrared normal emittance 79%
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate 93%
Examining report 8
August 15 2013 date of issuance
Report is made numbering (№) BA13001696-2
Sample title: bluish dogbane fabric
Sample message: ecru woven fabric
Test item is as follows:
Far infrared normal emittance 88%
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate 98%
Examining report 9
October 12 2013 date of issuance
Report is made numbering (№) BA13002200
Sample title: bluish dogbane underwear
Sample message: white knitted fabric
Test item is as follows:
Golden yellow staphylococcus (ATCC6538) bacteriostasis rate > 99%
Adopt above-mentioned technique, make apocynum fibre degumming effect good, flax fibre row yielding is high, 2-2.5 tons of bluish dogbane skins can be produced 1 ton of flax fibre, can produce 40 English with cotton blending and prop up above high-count yarn, its fabric can make home textile product various in style, underpants, socks, quilt, summer sleeping mat, pillow etc., has natural bacteriostatic, the unique function of transmitting to the useful far infrared of human body.
Detailed description of the invention:
Process:
1, poach: harvesting is grown in the wild venetum bar in Xinjiang Weili border of the county during annual March in November to the coming year, spread out natural drying and made it air-dry in 3 days, by spreading out waste of flax: the weight ratio of water=1:5, input is equipped with in the cement pit of water steam heating tube at the bottom of pond.Pool inner water is warming up to 60-70 °, makes to spread out waste of flax and be incubated 3-4 hours under this water temperature, pull out and put ground, treat that it drops to outdoor temperature naturally, numb skin under peel manually;
2, come unstuck: by bluish dogbane skin: water=1: 8 weight ratio, packs bluish dogbane skin 300kg, clear water 2400kg in the cylinder of the loose fine degumming machine of WSC-300 type bluish dogbane, as follows operation:
A: water is warming up to 40-45 degree, then opens the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 15 minutes, drain flushing water in cylinder, put into purification water pool, treat next reuse after self-purification;
B: to the sulfuric acid 5kg that puts into clear water 2400kg, concentration 98% in cylinder, water is warming up to 30-40 degree, then opens the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 35 minutes, drain flushing liquor in cylinder, put into purification water pool, after self-purification, treat next reuse;
C: put into clear water 2400kg in cylinder, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 25 minutes, drain flushing water in cylinder, put into purification water pool, treat next reuse after self-purification;
D: put into caustic soda (NaOH) 15kg of clear water 2400kg, concentration 96%, the soda ash (Na of concentration 96% in cylinder
2cO
3) 18kg, water is warming up to 90-100 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 120 minutes, drain flushing liquor in cylinder, put into purification water pool, after self-purification, treat next reuse;
E: put into clear water 2400kg in cylinder, water is warming up to 50-60 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 50 minutes, drain flushing water in cylinder, put into purification water pool, treat next reuse after self-purification;
F: to putting into clear water 2400kg in cylinder, Laiyang City Sheng Bang Chemical Co., Ltd. produces the SI-101 softener 10kg of concentration 50%, water is warming up to 35-40 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 50 minutes, drain flushing liquor in cylinder, put into purification water pool, after self-purification, treat next reuse, take out apocynum fibre;
3, copy fiber crops: on the apocynum fibre coming unstuck, also leave small part pectin, apocynum fibre 30kg after coming unstuck is placed in to De Shanlixin textile machinery factory of Changde City to be produced on the circular flax stamping device of CZ041 type, by 12 on this machine wooden fiber crops hammers that strike, the apocynum fibre on disk is beaten 5 times, be that flax stamping device disk rotates 5 circles, during this, uninterruptedly rinse apocynum fibre with the subsidiary automatic flushing machine of this machine, the pectin on it is all removed;
4, dehydration: the apocynum fibre of copying is dropped into machinery plant of Qian Zhou Datong District, Wuxi and produce the dehydration of the loose hair of XGZ-300 type cage Water Extraction Machinery;
5, dry: the apocynum fibre that took off water is dropped into Wuxi Wan Bang machinery plant and produce BO61 type loose fibre dryer, under temperature 100 degree, dry 0.5-1 hour, obtain keen-witted and capable apocynum fibre.
6, health: while reaching 10-16% because of the moisture of apocynum fibre, the brute force of its fiber is best, for the shredding comb suede of next step, make not easy fracture of fiber, keen-witted and capable apocynum fibre is added to wet process, the keen-witted and capable apocynum fibre lay of every 1000kg ground, spreads water 200 kg with humidification pump, makes its moisture reach 20%.Then insert temperature 30-35 degree, in the warehouse of humidity 60-65%, stack health 6-7 days;
7, shredding: apocynum fibre is from coming unstuck to health, in fiber, also contain partial impurities and breaking bar, apocynum fibre good health is dropped into Jiangyin Heng Yuan Harmann Berstorff, Maschinenbau GmbH and produce the multi-functional garnett of HYFU866 type, utilize 3 circular air draught dust cages on machine to remove impurity and breaking bar;
8, divide comb: the apocynum fibre that shredding is good, also having part doubling, fiber below length 16mm is short flannel, apocynum fibre good shredding is dropped into Qingdao Zhong Fu Harmann Berstorff, Maschinenbau GmbH and produce A186G type carding machine, comb suede, divide comb to fall doubling and the short flannel below length 16mm;
9, packing: the apocynum fibre packaging and warehousing of having combed, stand-by.
Claims (1)
1. a degumming tech for apocynum fibre, is characterized by: process is as follows:
1. poach: harvesting is grown in the wild venetum bar in Xinjiang Weili border of the county during annual March in November to the coming year, spread out natural drying and made it air-dry in 3 days, by spreading out waste of flax: the weight ratio of water=1:5, at the bottom of dropping into pond, be equipped with in the cement pit of water steam heating tube, pool inner water is warming up to 60-70 °, makes to spread out waste of flax and be incubated 3-4 hours in pond, pull out and put ground, treat that it drops to outdoor temperature naturally, numb skin under peel manually;
2. come unstuck: by bluish dogbane skin: water=1: 8 weight ratio, packs bluish dogbane skin 300kg, clear water 2400kg in the cylinder of the loose fine degumming machine of bluish dogbane, as follows operation:
A: water is warming up to 40-45 degree, then opens the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 15 minutes, drain flushing water in cylinder, put into external purification pond, treat after self-purification that used next time;
B: to the sulfuric acid 5kg that puts into clear water 2400kg, concentration 98% in cylinder, water is warming up to 30-40 degree, then opens the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 35 minutes, drain flushing liquor in cylinder, put into external purification pond, after self-purification, treat that used next time;
C: put into clear water 2400kg in cylinder, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 25 minutes, drain flushing water in cylinder, put into external purification pond, treat after self-purification that used next time;
D: put into caustic soda (NaOH) 15kg of clear water 2400kg, concentration 96%, the soda ash (Na of concentration 96% in cylinder
2cO
3) 18kg, water is warming up to 90-100 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 120 minutes, drain flushing liquor in cylinder, put into external purification pond, after self-purification, treat that used next time;
E: put into clear water 2400kg in cylinder, water is warming up to 50-60 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 50 minutes, drain flushing water in cylinder, put into external purification pond, after self-purification, treat that used next time;
F: to the SI-101 softener 10kg that puts into clear water 2400kg, concentration 50% in cylinder, water is warming up to 35-40 degree, then open the water circulating pump that this machine carries, water circulation in cylinder is flowed, numb skin is rinsed 50 minutes, drain flushing liquor in cylinder, put into external purification pond, after self-purification, treat to use next time, take out apocynum fibre;
3. copy fiber crops: the apocynum fibre 30kg coming unstuck is placed on circular flax stamping device, by 12 on this machine wooden fiber crops hammers that strike, the apocynum fibre on disk is beaten 5 times, be that flax stamping device disk rotates 5 circles, during this, uninterruptedly rinse apocynum fibre with the subsidiary automatic flushing machine of this machine, the pectin on it is all removed;
4. dehydration: the apocynum fibre of copying is dropped into the dehydration of the loose hair of cage Water Extraction Machinery;
5. dry: the apocynum fibre that took off water is dropped into loose fibre dryer, under temperature 100 degree, dry 0.5-1 hour, obtain keen-witted and capable bluish dogbane;
6. health: keen-witted and capable apocynum fibre is added to wet process, and the keen-witted and capable apocynum fibre lay of every 1000kg ground, spreads water 200 kg with humidification pump, make its moisture reach 20%, then insert temperature 30-35 degree, in the warehouse of relative humidity 60-65%, stack health 6-7 days;
7. shredding: the good apocynum fibre of health is dropped into multi-functional garnett, utilize 3 circular air draught dust cages on machine to remove impurity and breaking bar;
8. divide comb: apocynum fibre good shredding being dropped into carding machine, comb suede, is that short flannel divides comb to fall by doubling and the fiber below length 16mm;
9. packing: a point apocynum fibre packaging and warehousing of having combed, stand-by.
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| CN105316776A (en) * | 2014-07-11 | 2016-02-10 | 天津工业大学 | Fine treatment process of fibrilia |
| CN105970137A (en) * | 2016-05-30 | 2016-09-28 | 南京工程学院 | Large roller repairing layer and preparation method thereof |
| CN106757615A (en) * | 2017-01-18 | 2017-05-31 | 江南大学 | A kind of production method of cotton/blended yarn of apocynum |
| CN107095534A (en) * | 2017-04-07 | 2017-08-29 | 王达宏 | The preparation method of health care's pillow |
| CN107119334A (en) * | 2017-06-28 | 2017-09-01 | 梁国柱 | A kind of apocynum fibre degumming method of comprehensive utilization |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105316776A (en) * | 2014-07-11 | 2016-02-10 | 天津工业大学 | Fine treatment process of fibrilia |
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| CN105970137B (en) * | 2016-05-30 | 2018-06-15 | 南京工程学院 | A kind of large-scale roller repair layer and preparation method thereof |
| CN106757615A (en) * | 2017-01-18 | 2017-05-31 | 江南大学 | A kind of production method of cotton/blended yarn of apocynum |
| CN106757615B (en) * | 2017-01-18 | 2018-10-26 | 江南大学 | A kind of production method of cotton/blended yarn of apocynum |
| CN107095534A (en) * | 2017-04-07 | 2017-08-29 | 王达宏 | The preparation method of health care's pillow |
| CN107119334A (en) * | 2017-06-28 | 2017-09-01 | 梁国柱 | A kind of apocynum fibre degumming method of comprehensive utilization |
| CN107119334B (en) * | 2017-06-28 | 2019-02-19 | 梁国柱 | A kind of apocynum fibre degumming method of comprehensive utilization |
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| Publication number | Publication date |
|---|---|
| CN104018232B (en) | 2018-08-07 |
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