CN104018232B - The degumming tech of apocynum fibre - Google Patents

The degumming tech of apocynum fibre Download PDF

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CN104018232B
CN104018232B CN201410301221.2A CN201410301221A CN104018232B CN 104018232 B CN104018232 B CN 104018232B CN 201410301221 A CN201410301221 A CN 201410301221A CN 104018232 B CN104018232 B CN 104018232B
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water
cylinder
apocynum fibre
machine
purification
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CN104018232A (en
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温新惠
王存恩
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Xinjiang Youma liangpin Biotechnology Co., Ltd
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XINJIANG HONGHE FABRIC DECORATION CO Ltd
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Abstract

The degumming tech of the apocynum fibre of the present invention belongs to field of textiles, wild venetum bar through boiling, degumming, copy fiber crops, dehydration, drying, health, shredding, divide comb, packing step, obtain apocynum fibre.This technique so that apocynum fibre degumming effect is good, flaxen fiber row yielding is high, 1 ton of flaxen fiber can be produced by spreading out hemp skin for 2-2.5 tons, it can be with the blended high-count yarn for producing 40 English branch or more of cotton, home textile product, underpants, socks, quilt, summer sleeping mat, pillow etc. various in style can be made in its fabric, the unique function with natural bacteriostatic, the transmitting far infrared beneficial to human body.

Description

The degumming tech of apocynum fibre
Technical field
The degumming tech of the apocynum fibre of the present invention belongs to field of textiles.
Background technology
Very widely used today cotton products such as cotton-wadded quilt, in the environment of southern winter cool, damp, due to easy to moisture absorption easily Lead to the moisture absorption, grow bacterium, grows mildew, there is peculiar smell.Bluish dogbane(Apocynum venetum linn)It is that Xinjiang of China is spreaded out The distinctive wild plant of desert area is moored, is referred to as " king of fiber ", 1975-the 1979 of the publication of Beijing Science Press 1986 In " traditional Chinese medicine research " literature summary page 530-531, Liu Shoushan, which writes articles, to be pointed out:Bluish dogbane is unique one kind can emit life naturally The fibre plant of object wave, the softness with cotton, the gloss of silk, numb is smooth.Apocynum fibre is planted in the wild fiber having found It is best in quality in object, it is the superior raw material of weaving, papermaking, apocynum fibre is blended with cotton, the advantages of both can having both, at For ideal family's woven material.Bluish dogbane cold nature, bitter but sweet flavor, energy heat-clearing and fire-reducing, suppressing hyperactive liver for calming endogenous wind cure mainly headache, dizziness, insomnia etc. Disease, sesame slices flavones containing bluish dogbane have cardiac effect, and manufactured dogbane tea, bluish dogbane tablet and bluish dogbane cigarette etc. can treat The diseases such as hypertension.
Currently, general obtain bluish dogbane using spreading out hemp skin and be put into the method for kiering in cuboid pond made of iron plate Fiber, there are the following problems:
1. the kiering time is long, because pool inner water does not recycle, jute fiber degumming degree is irregular, and degumming effect is bad;
2. because being unable to pickling, washing in iron pond, it is necessary to pull apocynum fibre out and put into the artificial pickling of cement pit, water again It washes, not only increases processing cost, but also increase labor intensity;
3. without combing suede, obtained flaxen fiber row yielding is not high, and 1 ton of shredding can just be made through boiling 3.6 tons of hemp skins of numb shredding Flaxen fiber, row yielding only 28%.Flaxen fiber number is low, following in 2500 public branch.Flaxen fiber and cotton scribbled, proportion Only up to 35:65,21 English can only be spun and prop up yarn below.The above high-count yarn is propped up due to spinning 40 English, it is desirable that apocynum fibre number Reach 4000 public branch or more, therefore the method that tradition obtains apocynum fibre cannot achieve this purpose.
Invention content
It is good that the purpose of the present invention is to provide a kind of degumming effects, and the de- of the apocynum fibre of flaxen fiber row yielding can be improved Adhesive process.
Process:
1, boiling:Harvesting is grown in the wild venetum bar in Xinjiang Weili border of the county during March in annual November to the coming year, It is spread out natural drying and is allowed to air-dried in 3 days, by spreading out waste of flax:Water=1:5 weight ratio, input bottom of pond are equipped with vapor and follow In the cement pit of ring heating tube.Pool inner water is warming up to 60-70 DEG C, makes to spread out waste of flax and keeps the temperature 3-4 hours in pond, pulls pendulum out Ground is put, waits for that it naturally rings to outdoor temperature, hemp skin under peel manually;
2, degumming:By spreading out hemp skin:Water=1:8 weight ratio will spread out hemp skin 300kg, clear water 2400kg is packed into sieve Cloth fiber crops dissipate in the cylinder of fine degumming machine, operate as follows:
A:Water is warming up to 40-45 DEG C, the included water circulating pump of the machine is then turned on, so that water in cylinder is circulated, to fiber crops Skin rinses 15 minutes, drains flushing water in cylinder, is put into external purification pond, next use is waited for after self-purification;
B:Be put into cylinder clear water 2400kg, concentration 98% sulfuric acid 5kg, water is warming up to 30-40 DEG C, is then turned on this The included water circulating pump of machine, makes water in cylinder circulate, and is rinsed 35 minutes to hemp skin, also cries pickling, drained flushing liquor in cylinder, put Enter in external purification pond, next use is waited for after self-purification;
C:It is put into clear water 2400kg into cylinder, is then turned on the included water circulating pump of the machine, water in cylinder is made to circulate, Hemp skin is rinsed 25 minutes, flushing water in cylinder is drained, is put into external purification pond, next use is waited for after self-purification;
D:Be put into cylinder clear water 2400kg, concentration 96% caustic soda(NaOH)The soda ash of 15kg, concentration 96%(Na2CO3) Water is warming up to 90-100 DEG C by 18kg, is then turned on the included water circulating pump of the machine, so that water in cylinder is circulated, in this temperature Under to hemp skin kiering 120 minutes, drain flushing liquor in cylinder, be put into external purification pond, next use is waited for after self-purification;
E:It is put into clear water 2400kg into cylinder, water is warming up to 50-60 DEG C, is then turned on the included water circulating pump of the machine, So that water in cylinder is circulated, hemp skin is rinsed 50 minutes, flushing water in cylinder is drained, is put into external purification pond, self-purification After wait for next use;
F:Be put into cylinder clear water 2400kg, concentration 50% 101 softening agent 10kg of SI-, water is warming up to 35-40 DEG C, It is then turned on the included water circulating pump of the machine, water in cylinder is made to circulate, hemp skin is rinsed and is allowed within 50 minutes soft, is drained in cylinder Flushing liquor, is put into external purification pond, and next use is waited for after self-purification, takes out apocynum fibre;
3, fiber crops are copied:Apocynum fibre 30kg after degumming is placed on round flax stamping device, it is wooden by 12 on the machine It strikes fiber crops hammer and the apocynum fibre on disk is beaten 5 times, i.e., flax stamping device disk rotational 5 encloses, uninterruptedly on the machine during this Automatic flushing machine rinses apocynum fibre, and pectin thereon is all removed;
4, it is dehydrated:The apocynum fibre input cage copied is dissipated hair dewaterer dehydration;
5, it dries:Dehydrated apocynum fibre is put into loose fibre dryer, is dried at 100-105 DEG C of temperature 0.5-1 hour, obtain keen-witted and capable apocynum fibre.
6, health:Humidification process is carried out to keen-witted and capable apocynum fibre, per 1000kg, keen-witted and capable apocynum fibre lays ground, 200 kg of water is spread with humidification pump, so that its water content is reached 20%, is then placed in 30-35 DEG C of temperature, the storehouse of relative humidity 60-65% In library, health 6-7 days is stacked;
7, shredding:The good apocynum fibre of health is put into multi-functional hard waste machine, utilizes 3 round air draught dust cages on machine Remove impurity and breaking bar;
8, divide comb:The good apocynum fibre of shredding is put into carding machine, carries out comb suede, simultaneously silk and length 16mm is below Fiber, that is, short flannel point comb falls;
9, it is packaged:Point apocynum fibre a combed packaging and warehousing, for use.
Examine Co., Ltd of authentication center in September 15 in 2010 through national textile fabrics quality surveillance center Beijing Zhong Fangbiao Day on October 12nd, 1 the fabric to apocynum fibre, apocynum fibre and the blended gained of cotton, product obtained respectively Nine detections, as a result such as following table:
2010 dates of issuance September 15 days
Report makes number(№)BA10005826-1
Sample ID:Spread out flax fabric
Sample message:In vain/50% apocynum fibre of green woven fabric, 50% cotton
Detection project is as follows:
Gas permeability 268mm/s
Penetrability 7.88 × 103 g/(m2.d)
Examining report 2
2010 dates of issuance September 15 days
Report makes number(№)BA10005826-2
Sample ID:Apocynum fibre
Sample message:100% apocynum fibre of essential color fiber
Detection project is as follows:
Candida albicans(ATCC10231)Bacteriostasis rate 97%
Escherichia coli(8099)Bacteriostasis rate 95%
Klebsiella pneumoniae(ATCC4352)Bacteriostasis rate 97%
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate 99%
Far infrared normal emittance 80%
Examining report 3
June 7 2011 date of issuance
Report makes number(№)BA11001261
Sample ID:Spread out flax fabric
Sample message:30% apocynum fibre of white woven object, 70% cotton
Detection project is as follows:
Gas permeability 471mm/s
11110 g/ of penetrability (m2.d)
Far infrared normal emittance 80%
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate 60%
Klebsiella pneumoniae(ATCC4352)Bacteriostasis rate 93%
Candida albicans(ATCC10231)Bacteriostasis rate 97%
Escherichia coli(8099)Bacteriostasis rate 89%
Examining report 4
2011 dates of issuance August 15 days
Report makes number(№)BA11003396S
Sample ID:Apocynum fibre
Sample message:60% apocynum fibre of white fiber, 40% cotton
Detection project is as follows:
Candida albicans(ATCC10231)Bacteriostasis rate 75%
Escherichia coli(8099)Bacteriostasis rate 99%
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate 99%
Klebsiella pneumoniae(ATCC4352)Bacteriostasis rate 63%
Far infrared normal emittance 76%
Examining report 5
2011 dates of issuance September 8 days
Report makes number(№)BA11004217
Sample ID:Apocynum fibre
Sample message:White fiber coloured silk 60% apocynum fibre, 40% cotton
Detection project is as follows:
Escherichia coli(8099)Bacteriostasis rate 94%
Examining report 6
December 25 2012 date of issuance
Report makes number(№)BA12002583
Sample ID:Apocynum fibre
Sample message:100 % of colour of camel's hair apocynum fibre apocynum fibre
Detection project is as follows:
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate > 99%
Examining report 7
2013 dates of issuance August 15 days
Report makes number(№)BA13001696-1
Sample ID:Apocynum fibre
Sample message:White fiber
Detection project is as follows:
Far infrared normal emittance 79%
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate 93%
Examining report 8
2013 dates of issuance August 15 days
Report makes number(№)BA13001696-2
Sample ID:Spread out flax fabric
Sample message:Ecru woven fabric
Detection project is as follows:
Far infrared normal emittance 88%
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate 98%
Examining report 9
October 12 2013 date of issuance
Report makes number(№)BA13002200
Sample ID:Bluish dogbane underwear
Sample message:White knitted fabric
Detection project is as follows:
Golden yellow staphylococcus(ATCC6538)Bacteriostasis rate > 99%
Using above-mentioned technique so that apocynum fibre degumming effect is good, and flaxen fiber row yielding is high, 2-2.5 tons of bluish dogbanes Skin can produce 1 ton of flaxen fiber, can be with the blended high-count yarn for producing 40 English branch or more of cotton, and it is numerous that kind can be made in fabric More home textile product, underpants, socks, quilt, summer sleeping mat, pillow etc., with natural bacteriostatic, the transmitting far infrared beneficial to human body Unique function.
Specific implementation mode:
Process:
1, boiling:Harvesting is grown in the wild venetum in Xinjiang Weili border of the county during March in annual November to the coming year Bar is spread out natural drying and is allowed to air-dried in 3 days, by spreading out waste of flax:Water=1:5 weight ratio, input bottom of pond are equipped with water steaming In the cement pit of gas circulating-heating pipe.Pool inner water is warming up to 60-70 DEG C, making to spread out waste of flax, that 3-4 are kept the temperature under this water temperature is small When, it pulls out and puts ground, wait for that it naturally rings to outdoor temperature, hemp skin under peel manually;
2, degumming:By spreading out hemp skin:Water=1:8 weight ratio will spread out hemp skin 300kg, clear water 2400kg is packed into 300 type bluish dogbanes of WSC-dissipate in the cylinder of fine degumming machine, operate as follows:
A:Water is warming up to 40-45 DEG C, the included water circulating pump of the machine is then turned on, water in cylinder is made to circulate, it is right Hemp skin is rinsed 15 minutes, is drained flushing water in cylinder, is put into purification water pool, next reuse is waited for after self-purification;
B:Be put into cylinder clear water 2400kg, concentration 98% sulfuric acid 5kg, water is warming up to 30-40 DEG C, is then turned on The included water circulating pump of the machine, makes water in cylinder circulate, and is rinsed 35 minutes to hemp skin, drains flushing liquor in cylinder, be put into purification Next reuse is waited in pond, after self-purification;
C:It is put into clear water 2400kg into cylinder, is then turned on the included water circulating pump of the machine, water in cylinder is made to circulate, Hemp skin is rinsed 25 minutes, flushing water in cylinder is drained, is put into purification water pool, next reuse is waited for after self-purification;
D:Be put into cylinder clear water 2400kg, concentration 96% caustic soda(NaOH)The soda ash of 15kg, concentration 96%(Na2CO3) Water is warming up to 90-100 DEG C by 18kg, is then turned on the included water circulating pump of the machine, water in cylinder is made to circulate, rushed to hemp skin It washes 120 minutes, drains flushing liquor in cylinder, be put into purification water pool, next reuse is waited for after self-purification;
E:It is put into clear water 2400kg into cylinder, water is warming up to 50-60 DEG C, is then turned on the included water circulating pump of the machine, So that water in cylinder is circulated, hemp skin is rinsed 50 minutes, flushing water in cylinder is drained, is put into purification water pool, waited for after self-purification Next reuse;
F:It is soft that clear water 2400kg, the SI -101 of Laiyang City Sheng Bang Chemical Co., Ltd.s production concentration 50% are put into cylinder Water is warming up to 35-40 DEG C by agent 10kg, is then turned on the included water circulating pump of the machine, so that water in cylinder is circulated, to hemp skin It rinses 50 minutes, drains flushing liquor in cylinder, be put into purification water pool, next reuse is waited for after self-purification, take out apocynum fibre;
3, fiber crops are copied:Also there are small part pectin on the apocynum fibre of degumming, the apocynum fibre 30kg after degumming It is placed on De Shanlixin textile machinery factories of Changde City production CZ041 type circle flax stamping devices, numb hammer is struck by 12 on the machine are wooden Apocynum fibre on disk is beaten 5 times, i.e., flax stamping device disk rotational 5 encloses, uninterruptedly with subsidiary automatic of the machine during this Water feeder rinses apocynum fibre, and pectin thereon is all removed;
4, it is dehydrated:Apocynum fibre input machinery plant of Wuxi Datong District the Qian Zhou production XGZ-300 type cages copied are dissipated hair Dewaterer is dehydrated;
5, it dries:Dehydrated apocynum fibre input Wuxi Wan Bang machinery plants are produced into BO61 type loose fibre dryers, The lower drying 0.5-1 hour of 100 degree of temperature, obtains keen-witted and capable apocynum fibre.
6, health:Because apocynum fibre water content up to 10-16% when, the strength of fiber is best, for next step Shredding comb suede, keep fiber not easy to break, humidification process carried out to keen-witted and capable apocynum fibre, per 1000kg keen-witted and capable apocynum fibres Ground is laid, 200 kg of water is spread with humidification pump, its water content is made to reach 20%.Then 30-35 DEG C of temperature, humidity 60-are placed in In 65% warehouse, health 6-7 days is stacked;
7, shredding:Apocynum fibre also contains partial impurities and breaking bar from degumming to health in fiber, health is good Apocynum fibre puts into Jiangyin Heng Yuan Harmann Berstorff, Maschinenbau GmbH production multi-functional hard waste machine of HYFU866 types, is inhaled using 3 on machine are round Travel fatigue cage removes impurity and breaking bar;
8, divide comb:The good apocynum fibre of shredding, also part and silk, length 16mm fiber, that is, short flannels below, will open The good apocynum fibre input Qingdao Zhong Fu Harmann Berstorff, Maschinenbau GmbH of pine produces A186G type carding machines, comb suede is carried out, by simultaneously silk and length 16mm short flannels below point comb falls;
9, it is packaged:The apocynum fibre packaging and warehousing combed, for use.

Claims (1)

1. a kind of degumming tech of apocynum fibre, it is characterized in that:Process is as follows:
1. boiling:Harvesting is grown in the wild venetum bar in Xinjiang Weili border of the county during March in annual November to the coming year, by it It spreads natural drying out and is allowed to air-dried in 3 days, by spreading out waste of flax:Water=1:5 weight ratio, input bottom of pond are equipped with water steam and add In the cement pit of heat pipe, pool inner water is warming up to 60-70 DEG C, makes to spread out waste of flax and keeps the temperature 3-4 hours in pond, pulls out and puts ground Face waits for that it naturally rings to outdoor temperature, hemp skin under peel manually;
2. degumming:By spreading out hemp skin:Water=1:8 weight ratio will spread out hemp skin 300kg, clear water 2400kg is packed into bluish dogbane and dissipates In the cylinder of fine degumming machine, operate as follows:
A:Water is warming up to 40-45 DEG C, the included water circulating pump of the machine is then turned on, water in cylinder is made to circulate, hemp skin is rushed It washes 15 minutes, drains flushing water in cylinder, be put into external purification pond, next use is waited for after self-purification;
B:Be put into cylinder clear water 2400kg, concentration 98% sulfuric acid 5kg, water is warming up to 30-40 DEG C, be then turned on the machine from The water circulating pump of band makes water in cylinder circulate, and is rinsed 35 minutes to hemp skin, drains flushing liquor in cylinder, be put into external purification water Next use is waited in pond, after self-purification;
C:It is put into clear water 2400kg into cylinder, is then turned on the included water circulating pump of the machine, so that water in cylinder is circulated, to hemp skin It rinses 25 minutes, drains flushing water in cylinder, be put into external purification pond, next use is waited for after self-purification;
D:Be put into cylinder clear water 2400kg, concentration 96% caustic soda(NaOH)The soda ash of 15kg, concentration 96%(Na2CO3)18kg, Water is warming up to 90-100 DEG C, the included water circulating pump of the machine is then turned on, water in cylinder is made to circulate, 120 are rinsed to hemp skin Minute, flushing liquor in cylinder is drained, is put into external purification pond, next use is waited for after self-purification;
E:It is put into clear water 2400kg into cylinder, water is warming up to 50-60 DEG C, is then turned on the included water circulating pump of the machine, makes cylinder Interior water circulates, and is rinsed 50 minutes to hemp skin, drains flushing water in cylinder, be put into external purification pond, waited for after self-purification Next time uses;
F:Be put into cylinder clear water 2400kg, concentration 50% 101 softening agent 10kg of SI-, water is warming up to 35-40 DEG C, then The included water circulating pump of the machine is opened, water in cylinder is made to circulate, hemp skin is rinsed 50 minutes, flushing liquor in cylinder is drained, is put into Next use is waited in external purification pond, after self-purification, takes out apocynum fibre;
3. copying fiber crops:The apocynum fibre 30kg of degumming is placed on round flax stamping device, fiber crops are struck by 12 on the machine are wooden Apocynum fibre on disk is beaten 5 times by hammer, i.e., flax stamping device disk rotational 5 encloses, and subsidiary oneself of the machine is uninterruptedly used during this Dynamic water feeder rinses apocynum fibre, and pectin thereon is all removed;
4. being dehydrated:The apocynum fibre input cage copied is dissipated hair dewaterer dehydration;
5. drying:Dehydrated apocynum fibre is put into loose fibre dryer, dries 0.5-1 hours, obtains at 100 DEG C of temperature To keen-witted and capable bluish dogbane;
6. health:Humidification process is carried out to keen-witted and capable apocynum fibre, keen-witted and capable apocynum fibre lays ground per 1000kg, with humidification Pump spreads water 200kg, its water content is made to reach 20%, then 30-35 DEG C of temperature of merging, in the warehouse of relative humidity 60-65%, stacks Health 6-7 days;
7. shredding:The good apocynum fibre of health is put into multi-functional hard waste machine, is removed using 3 round air draught dust cages on machine Impurity and breaking bar;
8. dividing comb:The good apocynum fibre of shredding is put into carding machine, carries out comb suede, by simultaneously silk and length 16mm fibers below That is short flannel point comb falls;
9. being packaged:Point apocynum fibre a combed packaging and warehousing, for use.
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CN106757615B (en) * 2017-01-18 2018-10-26 江南大学 A kind of production method of cotton/blended yarn of apocynum
CN107095534A (en) * 2017-04-07 2017-08-29 王达宏 The preparation method of health care's pillow
CN107119334B (en) * 2017-06-28 2019-02-19 梁国柱 A kind of apocynum fibre degumming method of comprehensive utilization

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