CN106811971A - A kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance and preparation method thereof - Google Patents

A kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance and preparation method thereof Download PDF

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Publication number
CN106811971A
CN106811971A CN201611202001.XA CN201611202001A CN106811971A CN 106811971 A CN106811971 A CN 106811971A CN 201611202001 A CN201611202001 A CN 201611202001A CN 106811971 A CN106811971 A CN 106811971A
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cashmere
shell fabric
composite shell
fatigue resistance
minutes
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倪进培
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/15—Proteins or derivatives thereof
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D06M2101/12—Keratin fibres or silk
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/45—Shrinking resistance, anti-felting properties
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Microbiology (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance, it is made from the following raw materials in parts by weight：Cashmere 25 28, expanded goose feather powder 20 22, apocynum fibre 8 10, cotton rose stem follicarpium glue 10 12,40%（owf）Natural sericin solution 30 35, amido silicon oil 35, nano active powdered carbon 24, ten difluoro heptyl propyl trimethoxy silicanes 13, butyl acrylate 57, soybean residue 68, the N-Methylimidazoleacetic salt 170 190 of 1 butyl 3, suitable quantity of water, optimization of C/C composites of the present invention improves production technology, cashmere composite fibre is obtained through wet spinning technology, blended dressing liquid impregnation process improves cashmere antibacterial again, antiultraviolet and anti-felting property, obtained Cashmere composite shell fabric is soft abundant, gloss is naturally soft, with antibacterial, ultraviolet radiation preventing and antifatigue healthcare function.

Description

A kind of natural plants antibacterial Cashmere composite shell fabric and its making with fatigue resistance Method
Technical field
The present invention relates to textile material technical field, more particularly to a kind of natural plants antibacterial cashmere with fatigue resistance Composite material and preparation method thereof.
Background technology
Cotton rose also known as Flos Hibisci Mutabilis, cotton rose, are Malvaceae machaka or dungarunga, and its flower, leaf can be used as medicine, with cool The effects such as blood hemostasis, clearing heat and detoxicating, alleviating pain and detumescence, and no side effectses.Recent studies indicate that, Huang is contained in cotton rose Ketone compounds, have inhibitory action to typhoid bacillus, staphylococcus aureus etc..At present, the application for cotton rose is main Its flower, Ye Zhong is concentrated on, the research for its stem skin and accompaniment is less.Research shows that certain plants stem skin is produced through degumming Pectin have more significant antibacterial and radiation proof the effects such as.For knitting fleece fabrics uv resistance energy and anti-microbial property compared with Poor characteristic, is further to lift knitting cashmere product added value,《The extraction of cotton rose stem follicarpium glue and its to knitting cashmere face The application of material》One literary grace acid-extraction, with sour dilution as extract solution, the technique such as research pH value, extraction time, solid-liquid ratio Cotton rose stem skin pectous extracting method is optimized, and it is whole for the function of knitting fleece fabrics to prepare good pectin Reason, as a result shows:Cotton rose stem skin using tartaric acid dilution as extract solution, in pH value 2, extraction time 90min, solid-liquid ratio 1 : under 30 process conditions, pectin yield up to 13.24%, after knitting fleece fabrics is arranged through cotton rose pectin, anti-microbial property and anti- Ultraviolet performance is significantly improved.
Because cashmere is compared with common fine wool, its surface has regular thin thin scale layer, when cashmere fiber is machine-washed Easily felting, the easy shrinking deformation influence taking of manufactured goods.And the antibiotic radiation proof performance in text only to cashmere changes Enter, in order to further improve the wearability of cashmere fiber, overcome its shortcoming, cashmere fiber needs to carry out feld proofing.Will Cotton rose stem follicarpium glue is very few to the report that the felt proofing of cashmere fiber is studied with natural sericin Combined Treatment.Except this it Outward, cashmere is compared to wool one is that yield is few but price is high is difficult volume production, so that develop substituting having for cashmere The NEW TYPE OF COMPOSITE cashmere fiber of the functions such as warmth retention property is high, low cost, felt proofing, antibiotic radiation proof.
The content of the invention
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of natural plants with fatigue resistance resist Bacterium Cashmere composite shell fabric and preparation method thereof.
The present invention is achieved by the following technical solutions：
A kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance, is made from the following raw materials in parts by weight：Cashmere 25-28, expanded goose feather powder 20-22, apocynum fibre 8-10, cotton rose stem follicarpium glue 10-12,40%（owf）Natural sericin Solution 30-35, amido silicon oil 3-5, nano active powdered carbon 2-4, ten difluoro heptyl propyl trimethoxy silicane 1-3, acrylic acid fourth Ester 5-7, soybean residue 6-8,1- butyl -3- N-Methylimidazoleacetic salt 170-190, suitable quantity of water.
A kind of preparation method of described natural plants antibacterial Cashmere composite shell fabric with fatigue resistance, including following step Suddenly：
（1）By nano active powdered carbon in drying box 100-120 DEG C preheating and drying 1-2 hours, keeping temperature added for ten difluoro heptan Base propyl trimethoxy silicane is stirred 10-15 minutes, is vacuum dried to obtain modified Nano activated carbon powder；
（2）Soybean residue is dried into ground 100 eye mesh screen, sprinkling mass concentration is stirred and evenly mixed for the hydrochloric acid solution of 4-8%, in 60- Magnetic agitation 2-3 hours in 80 DEG C of waters bath with thermostatic control, washing to neutrality is vacuum dried, and adds butyl acrylate ultrasonic grinding 1-3 small When, dry the soybean residue superfines that must be modified；
（3）To extrude powdered after the cotton rose stem follicarpium glue air drying of extraction, add suitable quantity of water to be made into 7.5% pectin Solution, is stirred continuously to whole dissolvings in 85-95 DEG C of water bath with thermostatic control, adds 40%（owf）Natural sericin solution, step （1）Material ultrasonic disperse must mix dressing liquid in 30-40 minutes；
（4）Cashmere, expanded goose feather powder, apocynum fibre are added during 1- butyl -3- N-Methylimidazoleacetics salt is put into reactor Grinding 20-40 minutes, is heated to 100-120 DEG C, adds step（2）Material stirring reacts 50-70 minutes, and spinning obtains cashmere and is combined Fiber；
（5）By step（4）Obtained cashmere composite fibre puts into step（3）In mixing dressing liquid, bath raio 1: 50 impregnates 30-40 Minute, take out, clean with distilled water flushing, room temperature is dried, discharging.
It is an advantage of the invention that：Optimization of C/C composites of the present invention improves production technology, and cashmere is obtained through wet spinning technology is combined Fiber, then blended dressing liquid impregnation process improves cashmere antibacterial, antiultraviolet and anti-felting property；Be modified for soybean residue by the present invention After be added in raw material, play the cementation between fiber, add expanded goose feather powder, apocynum fibre, reduce making for cashmere Consumption reduces cost, cashmere composite fibre obtained in spinning has the advantages that insulation, high adsorption capacity, is conducive to strengthening silk gum egg White adsorbance, improves the hydrophily of cashmere fiber, further reduces the direction friction effect of fiber surface, thus shrinkproof Obtain bigger improvement；It is naturally soft using the soft abundant, gloss of Cashmere composite shell fabric obtained in the present invention, with antibacterial, Ultraviolet radiation preventing and antifatigue healthcare function.
Specific embodiment
A kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance, is made from the following raw materials in parts by weight：Mountain Cashmere 25, expanded goose feather powder 20, apocynum fibre 8, cotton rose stem follicarpium glue 10,40%（owf）Natural sericin solution 30, Amido silicon oil 3, nano active powdered carbon 2, ten difluoro heptyl propyl trimethoxy silicanes 1, butyl acrylate 5, soybean residue 6,1- fourths Base -3- N-Methylimidazoleacetics salt 170, suitable quantity of water.
A kind of preparation method of described natural plants antibacterial Cashmere composite shell fabric with fatigue resistance, including following step Suddenly：
（1）By nano active powdered carbon in drying box 100-120 DEG C preheating and drying 1-2 hours, keeping temperature added for ten difluoro heptan Base propyl trimethoxy silicane is stirred 10-15 minutes, is vacuum dried to obtain modified Nano activated carbon powder；
（2）Soybean residue is dried into ground 100 eye mesh screen, sprinkling mass concentration is stirred and evenly mixed for the hydrochloric acid solution of 4-8%, in 60- Magnetic agitation 2-3 hours in 80 DEG C of waters bath with thermostatic control, washing to neutrality is vacuum dried, and adds butyl acrylate ultrasonic grinding 1-3 small When, dry the soybean residue superfines that must be modified；
（3）To extrude powdered after the cotton rose stem follicarpium glue air drying of extraction, add suitable quantity of water to be made into 7.5% pectin Solution, is stirred continuously to whole dissolvings in 85-95 DEG C of water bath with thermostatic control, adds 40%（owf）Natural sericin solution, step （1）Material ultrasonic disperse must mix dressing liquid in 30-40 minutes；
（4）Cashmere, expanded goose feather powder, apocynum fibre are added during 1- butyl -3- N-Methylimidazoleacetics salt is put into reactor Grinding 20-40 minutes, is heated to 100-120 DEG C, adds step（2）Material stirring reacts 50-70 minutes, and spinning obtains cashmere and is combined Fiber；
（5）By step（4）Obtained cashmere composite fibre puts into step（3）In mixing dressing liquid, bath raio 1: 50 impregnates 30-40 Minute, take out, clean with distilled water flushing, room temperature is dried, discharging.
Uv transmittance using Cashmere composite shell fabric obtained in the present invention for wavelength less than 290nm goes to zero, UPF Value reaches 53, and the bacteriostasis rate to staphylococcus aureus can reach 95.571%.

Claims (2)

1. a kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance, it is characterised in that by the original of following weight portion Material is made：Cashmere 25-28, expanded goose feather powder 20-22, apocynum fibre 8-10, cotton rose stem follicarpium glue 10-12,40% （owf）Natural sericin solution 30-35, amido silicon oil 3-5, nano active powdered carbon 2-4, ten difluoro heptyl propyl trimethoxies Silane 1-3, butyl acrylate 5-7, soybean residue 6-8,1- butyl -3- N-Methylimidazoleacetic salt 170-190, suitable quantity of water.
2. the making side of a kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance according to claim 1 Method, it is characterised in that comprise the following steps：
（1）By nano active powdered carbon in drying box 100-120 DEG C preheating and drying 1-2 hours, keeping temperature added for ten difluoro heptan Base propyl trimethoxy silicane is stirred 10-15 minutes, is vacuum dried to obtain modified Nano activated carbon powder；
（2）Soybean residue is dried into ground 100 eye mesh screen, sprinkling mass concentration is stirred and evenly mixed for the hydrochloric acid solution of 4-8%, in 60- Magnetic agitation 2-3 hours in 80 DEG C of waters bath with thermostatic control, washing to neutrality is vacuum dried, and adds butyl acrylate ultrasonic grinding 1-3 small When, dry the soybean residue superfines that must be modified；
（3）To extrude powdered after the cotton rose stem follicarpium glue air drying of extraction, add suitable quantity of water to be made into 7.5% pectin Solution, is stirred continuously to whole dissolvings in 85-95 DEG C of water bath with thermostatic control, adds 40%（owf）Natural sericin solution, step （1）Material ultrasonic disperse must mix dressing liquid in 30-40 minutes；
（4）Cashmere, expanded goose feather powder, apocynum fibre are added during 1- butyl -3- N-Methylimidazoleacetics salt is put into reactor Grinding 20-40 minutes, is heated to 100-120 DEG C, adds step（2）Material stirring reacts 50-70 minutes, and spinning obtains cashmere and is combined Fiber；
（5）By step（4）Obtained cashmere composite fibre puts into step（3）In mixing dressing liquid, bath raio 1: 50 impregnates 30-40 Minute, take out, clean with distilled water flushing, room temperature is dried, discharging.
CN201611202001.XA 2016-12-23 2016-12-23 A kind of natural plants antibacterial Cashmere composite shell fabric with fatigue resistance and preparation method thereof Withdrawn CN106811971A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109097990A (en) * 2018-08-27 2018-12-28 江苏阳光股份有限公司 A kind of pectin antibacterial finishing process of fleece fabrics
CN112458595A (en) * 2020-11-17 2021-03-09 张喜梅 Antibacterial health-care and anti-ultraviolet environment-friendly composite fabric and production device thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1664194A (en) * 2005-03-17 2005-09-07 刘磊 Chicken feather down fibre yarn and method for making same

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1664194A (en) * 2005-03-17 2005-09-07 刘磊 Chicken feather down fibre yarn and method for making same

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王雪燕 等: "《蛋白质化学及其应用》", 31 January 2016, 中国纺织出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109097990A (en) * 2018-08-27 2018-12-28 江苏阳光股份有限公司 A kind of pectin antibacterial finishing process of fleece fabrics
CN112458595A (en) * 2020-11-17 2021-03-09 张喜梅 Antibacterial health-care and anti-ultraviolet environment-friendly composite fabric and production device thereof

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Application publication date: 20170609