CN106758230A - A kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric and preparation method thereof - Google Patents

A kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric and preparation method thereof Download PDF

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Publication number
CN106758230A
CN106758230A CN201611202009.6A CN201611202009A CN106758230A CN 106758230 A CN106758230 A CN 106758230A CN 201611202009 A CN201611202009 A CN 201611202009A CN 106758230 A CN106758230 A CN 106758230A
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cashmere
shell fabric
composite shell
heat endurance
high abrasion
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倪进培
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/15—Proteins or derivatives thereof
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D06M2101/12—Keratin fibres or silk
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/35—Abrasion, pilling or fibrillation resistance
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/45—Shrinking resistance, anti-felting properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Microbiology (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric, it is made from the following raw materials in parts by weight：Inner Mongolia White cashmere 30 32, mulberry silk 21 22,3D conductive fibers 89, cotton rose stem follicarpium glue 9 11,40%（owf）Natural sericin solution 36 38, shitosan 68, paraffin 23, guar gum 46, lignocellulosic 78, medical stone powder 35, tea tree ethereal oil 0.1 0.3, the N-Methylimidazoleacetic salt 180 190, suitable quantity of water of 1 butyl 3, optimization of C/C composites of the present invention improves production technology, cashmere composite fibre is obtained through wet spinning technology, blended dressing liquid impregnation process improves cashmere antibacterial, antiultraviolet and anti-felting property again, and obtained Cashmere composite shell fabric has the strong wearability of wear-resisting, high thermal stability, spinnability.

Description

A kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric and its making Method
Technical field
The present invention relates to textile material technical field, more particularly to a kind of heat endurance high abrasion natural plants antibacterial cashmere Composite material and preparation method thereof.
Background technology
Cotton rose also known as Flos Hibisci Mutabilis, cotton rose, are Malvaceae machaka or dungarunga, and its flower, leaf can be used as medicine, with cool The effects such as blood hemostasis, clearing heat and detoxicating, alleviating pain and detumescence, and no side effectses.Recent studies indicate that, Huang is contained in cotton rose Ketone compounds, have inhibitory action to typhoid bacillus, staphylococcus aureus etc..At present, the application for cotton rose is main Its flower, Ye Zhong is concentrated on, the research for its stem skin and accompaniment is less.Research shows that certain plants stem skin is produced through degumming Pectin have more significant antibacterial and radiation proof the effects such as.For knitting fleece fabrics uv resistance energy and anti-microbial property compared with Poor characteristic, is further to lift knitting cashmere product added value,《The extraction of cotton rose stem follicarpium glue and its to knitting cashmere face The application of material》One literary grace acid-extraction, with sour dilution as extract solution, the technique such as research pH value, extraction time, solid-liquid ratio Cotton rose stem skin pectous extracting method is optimized, and it is whole for the function of knitting fleece fabrics to prepare good pectin Reason, as a result shows:Cotton rose stem skin using tartaric acid dilution as extract solution, in pH value 2, extraction time 90min, solid-liquid ratio 1 : under 30 process conditions, pectin yield up to 13.24%, after knitting fleece fabrics is arranged through cotton rose pectin, anti-microbial property and anti- Ultraviolet performance is significantly improved.
Because cashmere is compared with common fine wool, its surface has regular thin thin scale layer, when cashmere fiber is machine-washed Easily felting, the easy shrinking deformation influence taking of manufactured goods.And the antibiotic radiation proof performance in text only to cashmere changes Enter, in order to further improve the wearability of cashmere fiber, overcome its shortcoming, cashmere fiber needs to carry out feld proofing.Will Cotton rose stem follicarpium glue is very few to the report that the felt proofing of cashmere fiber is studied with natural sericin Combined Treatment.Except this it Outward, cashmere is compared to wool one is that yield is few but price is high is difficult volume production, so that develop substituting having for cashmere The NEW TYPE OF COMPOSITE cashmere fiber of the functions such as warmth retention property is high, low cost, felt proofing, antibiotic radiation proof.
The content of the invention
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of heat endurance high abrasion natural plants resist Bacterium Cashmere composite shell fabric and preparation method thereof.
The present invention is achieved by the following technical solutions：
A kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric, is made from the following raw materials in parts by weight：The Inner Mongol White goat wool 30-32, mulberry silk 21-22,3D conductive fiber 8-9, cotton rose stem follicarpium glue 9-11,40%（owf）Natural silk gum egg White solution 36-38, shitosan 6-8, paraffin 2-3, guar gum 4-6, lignocellulosic 7-8, medical stone powder 3-5, tea tree ethereal oil 0.1-0.3,1- butyl -3- N-Methylimidazoleacetic salt 180-190, suitable quantity of water.
A kind of preparation method of described heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric, including following step Suddenly：
（1）By medical stone powder in drying box 100-120 DEG C preheating and drying 1-2 hours, keeping temperature add paraffin, tea tree ethereal oil Stirring 10-15 minutes, is vacuum dried the medical stone powder that must be modified；
（2）Lignocellulosic is dried into ground 100 eye mesh screen, sprinkling mass concentration is stirred and evenly mixed for the hydrochloric acid solution of 4-8%, Magnetic agitation 2-3 hours in 60-80 DEG C of water bath with thermostatic control, washing to neutrality is vacuum dried, and adds guar gum, shitosan ultrasound to grind Mill 1-3 hours, dries to obtain modified wood fibre element；
（3）To extrude powdered after the cotton rose stem follicarpium glue air drying of extraction, add suitable quantity of water to be made into 7.5% pectin Solution, is stirred continuously to whole dissolvings in 85-95 DEG C of water bath with thermostatic control, adds 40%（owf）Natural sericin solution, step （1）Material ultrasonic disperse must mix dressing liquid in 30-40 minutes；
（4）Add Inner Mongolia White cashmere, mulberry silk, 3D conductive during 1- butyl -3- N-Methylimidazoleacetics salt is put into reactor Fiber grinds 20-40 minutes, is heated to 100-120 DEG C, adds step（2）Material stirring reacts 50-70 minutes, and spinning obtains cashmere Composite fibre；
（5）By step（4）Obtained cashmere composite fibre puts into step（3）In mixing dressing liquid, bath raio 1: 50 impregnates 30-40 Minute, take out, clean with distilled water flushing, room temperature is dried, discharging.
It is an advantage of the invention that：Optimization of C/C composites of the present invention improves production technology, and cashmere is obtained through wet spinning technology is combined Fiber, then blended dressing liquid impregnation process improves cashmere antibacterial, antiultraviolet and anti-felting property；The present invention is by lignocellulosic It is modified to be added in raw material, the cementation between fiber is played, addition mulberry silk, 3D conductive fibers reduce making for cashmere Consumption reduces cost, cashmere composite fibre obtained in spinning has the advantages that insulation, high adsorption capacity, is conducive to strengthening silk gum egg White adsorbance, improves the hydrophily of cashmere fiber, further reduces the direction friction effect of fiber surface, thus shrinkproof Obtain bigger improvement；There is the strong taking of wear-resisting, high thermal stability, spinnability using Cashmere composite shell fabric obtained in the present invention Energy.
Specific embodiment
A kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric, is made from the following raw materials in parts by weight：It is interior Mongolian white goat wool 30, mulberry silk 21,3D conductive fibers 8, cotton rose stem follicarpium glue 9,40%（owf）Natural sericin solution 36th, shitosan 6, paraffin 2, guar gum 4, lignocellulosic 7, medical stone powder 3, tea tree ethereal oil 0.1,1- butyl -3- methylimidazoles Acetate 180, suitable quantity of water.
A kind of preparation method of described heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric, including following step Suddenly：
（1）By medical stone powder in drying box 100-120 DEG C preheating and drying 1-2 hours, keeping temperature add paraffin, tea tree ethereal oil Stirring 10-15 minutes, is vacuum dried the medical stone powder that must be modified；
（2）Lignocellulosic is dried into ground 100 eye mesh screen, sprinkling mass concentration is stirred and evenly mixed for the hydrochloric acid solution of 4-8%, Magnetic agitation 2-3 hours in 60-80 DEG C of water bath with thermostatic control, washing to neutrality is vacuum dried, and adds guar gum, shitosan ultrasound to grind Mill 1-3 hours, dries to obtain modified wood fibre element；
（3）To extrude powdered after the cotton rose stem follicarpium glue air drying of extraction, add suitable quantity of water to be made into 7.5% pectin Solution, is stirred continuously to whole dissolvings in 85-95 DEG C of water bath with thermostatic control, adds 40%（owf）Natural sericin solution, step （1）Material ultrasonic disperse must mix dressing liquid in 30-40 minutes；
（4）Add Inner Mongolia White cashmere, mulberry silk, 3D conductive during 1- butyl -3- N-Methylimidazoleacetics salt is put into reactor Fiber grinds 20-40 minutes, is heated to 100-120 DEG C, adds step（2）Material stirring reacts 50-70 minutes, and spinning obtains cashmere Composite fibre；
（5）By step（4）Obtained cashmere composite fibre puts into step（3）In mixing dressing liquid, bath raio 1: 50 impregnates 30-40 Minute, take out, clean with distilled water flushing, room temperature is dried, discharging.
Uv transmittance using Cashmere composite shell fabric obtained in the present invention for wavelength less than 290nm goes to zero, UPF Value reaches 52, and the bacteriostasis rate to staphylococcus aureus can reach 95.271%.

Claims (2)

1. a kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric, it is characterised in that by the original of following weight portion Material is made：Inner Mongolia White cashmere 30-32, mulberry silk 21-22,3D conductive fiber 8-9, cotton rose stem follicarpium glue 9-11,40% （owf）Natural sericin solution 36-38, shitosan 6-8, paraffin 2-3, guar gum 4-6, lignocellulosic 7-8, medical stone powder 3-5, tea tree ethereal oil 0.1-0.3,1- butyl -3- N-Methylimidazoleacetic salt 180-190, suitable quantity of water.
2. the making side of a kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric according to claim 1 Method, it is characterised in that comprise the following steps：
（1）By medical stone powder in drying box 100-120 DEG C preheating and drying 1-2 hours, keeping temperature add paraffin, tea tree ethereal oil Stirring 10-15 minutes, is vacuum dried the medical stone powder that must be modified；
（2）Lignocellulosic is dried into ground 100 eye mesh screen, sprinkling mass concentration is stirred and evenly mixed for the hydrochloric acid solution of 4-8%, Magnetic agitation 2-3 hours in 60-80 DEG C of water bath with thermostatic control, washing to neutrality is vacuum dried, and adds guar gum, shitosan ultrasound to grind Mill 1-3 hours, dries to obtain modified wood fibre element；
（3）To extrude powdered after the cotton rose stem follicarpium glue air drying of extraction, add suitable quantity of water to be made into 7.5% pectin Solution, is stirred continuously to whole dissolvings in 85-95 DEG C of water bath with thermostatic control, adds 40%（owf）Natural sericin solution, step （1）Material ultrasonic disperse must mix dressing liquid in 30-40 minutes；
（4）Add Inner Mongolia White cashmere, mulberry silk, 3D conductive during 1- butyl -3- N-Methylimidazoleacetics salt is put into reactor Fiber grinds 20-40 minutes, is heated to 100-120 DEG C, adds step（2）Material stirring reacts 50-70 minutes, and spinning obtains cashmere Composite fibre；
（5）By step（4）Obtained cashmere composite fibre puts into step（3）In mixing dressing liquid, bath raio 1: 50 impregnates 30-40 Minute, take out, clean with distilled water flushing, room temperature is dried, discharging.
CN201611202009.6A 2016-12-23 2016-12-23 A kind of heat endurance high abrasion natural plants antibacterial Cashmere composite shell fabric and preparation method thereof Withdrawn CN106758230A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107620145A (en) * 2017-09-27 2018-01-23 海宁市成达经编有限公司 A kind of super abrasive antibacterial quilt cover fabric and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104783361A (en) * 2014-01-18 2015-07-22 如皋市三飞时装有限公司 Mould-proof cashmere overcoat shell fabric

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104783361A (en) * 2014-01-18 2015-07-22 如皋市三飞时装有限公司 Mould-proof cashmere overcoat shell fabric

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
赵菊梅等: ""木芙蓉茎皮果胶的提取及其对针织羊绒面料的应用"", 《毛纺科技》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107620145A (en) * 2017-09-27 2018-01-23 海宁市成达经编有限公司 A kind of super abrasive antibacterial quilt cover fabric and preparation method thereof

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Application publication date: 20170531