CN105002613A - Antistatic cashmere composite fiber containing stainless steel fiber and manufacturing method thereof - Google Patents
Antistatic cashmere composite fiber containing stainless steel fiber and manufacturing method thereof Download PDFInfo
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- CN105002613A CN105002613A CN201510255478.3A CN201510255478A CN105002613A CN 105002613 A CN105002613 A CN 105002613A CN 201510255478 A CN201510255478 A CN 201510255478A CN 105002613 A CN105002613 A CN 105002613A
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Abstract
The invention discloses antistatic cashmere composite fiber containing stainless steel fiber. The antistatic cashmere composite fiber is prepared by raw materials comprising, by weight, 30-35 parts of berber Fleece, 10-13 parts of rabbit hair, 6-9 parts of soybean protein fiber, 7-10 parts of nanometer bamboo-carbon fiber, 11-14 parts of stainless steel fiber, 5-8 parts of aloe fiber, 4-7 parts of polyethylene glycol distearate, 0.02-0.04 parts of lemon oil, 1.3-2.5 parts of polytetrahydrofuran glycol, 3-5 parts of ethanol amine, 0.6-1.1 parts of nano-TiO2, 2-4 parts of artificial zeolite powder, 1-3 parts of cimicifugae foetidae, 3-4 parts of Mangnolia officinalis, 4-6 parts of pineapple leaves, 110-120 parts of 1-ethyl-3-methylimidazolium acetate, 100-110 parts of 1-allyl-3-methylimidazolium chloride, 20-24 parts of addition agent and appropriate amount of water. The antistatic cashmere composite fiber prepared by the invention has special functions of being anti-static, anti-microbial, mothproof, wear resistant, and anti-radiation and the like.
Description
Technical field
The present invention relates to nonwoven material technical field, be specifically related to a kind of anti-static cashmere composite fibre containing stainless steel fibre and preparation method thereof.
Background technology
Cashmere is that growth is at goat appearance cortex, cover the high-grade natural fabric thin and bending one by one at goat coarse wool root, wherein containing a lot of air, and form air layer, the invasion and attack of external cold air can be defendd, retain body temperature can not lower, there is the title of " fiber jewel ", " fiber queen ".Because output is rare, the more important thing is its excellent quality and characteristic, have light, soft, sliding, glutinous feature, is that all textile raw materials that the current mankind can utilize are all incomparable, and be thus otherwise known as " soft gold ".
Goat cashmere mainly originates in China, owing to limiting by kind, goat is greater than sheep for the consumption of grassland and vegetation, and input-output ratio is relatively on the low side, thus cause the cultivation quantity of goat to decline to some extent, in addition due to the change of rearing conditions and to goat improvement, the fineness of goat cashmere is thicker year by year; Along with the raising of people's living standard, to the demand of cashmere product at quality and quantity and functionally expand just gradually, increasing wool textile enterprises joins cashmere and produces, and makes this just rare goat cashmere resource costly, and this brings very large managerial risk also to many enterprises; Cashmere fiber itself is a kind of native protein, and its manufactured goods certainly exist many defects, is such as subject to damage by worms, easily balling-up, easily to play electrostatic, not wear-resisting, not radiation proof, intensity low etc.If the composite fibre of cashmere fibres and other fiber blends can be prepared, just when reducing costs, the new product not being worse than pure cashmere fiber textile quality can be obtained.
Summary of the invention
Object of the present invention is just to provide a kind of anti-static cashmere composite fibre containing stainless steel fibre and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of anti-static cashmere composite fibre containing stainless steel fibre, it is characterized in that, be made up of the raw material of following weight portion: lamb suede 30-35, rabbit hair 10-13, soybean fiber 6-9, nanometer bamboo carbon fiber 7-10, stainless steel fibre 11-14, aloe fibre 5-8, polyethylene glycol stearate diester 4-7, lemon oil 0.02-0.04, PTMG 1.3-2.5, monoethanolamine 3-5, nano titanium oxide 0.6-1.1, artificial zeolite powder 2-4, rattletop 1-3, bark of official magnolia 3-4, pineapple leaves 4-6, 1-ethyl-3-methylimidazole acetate 110-120, 1-allyl-3-methylimidazole villaumite 100-110, auxiliary agent 20-24, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: methyl acrylate 30-35, butyl methacrylate 40-45, haloflex 15-20, methacrylic acid 10-15, 1,2-PD 13-18, polypropylene glycol diglycidyl ether 20-30, hydroxypropyl methylcellulose 1-3, Silane coupling agent KH550 0.4-0.8, triethanolamine 3-6, tributyl phosphate 12-15, glyceryl monooleate 14-18, sodium metasilicate 0.2-0.5, microcrystalline wax 7-9, N hydroxymethyl acrylamide 4-7, deionized water 100-200, its preparation method is by methacrylic acid, 1,2-PD, polypropylene glycol diglycidyl ether puts into reactor mixing and stirring, is warming up to 140-155 DEG C, adds Silane coupling agent KH550 and keeps thermotonus 3-5 hour, be cooled to 85-100 DEG C, add methyl acrylate, butyl methacrylate, haloflex, pours nitrogen, keeps temperature to heat while stirring, adds tributyl phosphate, glyceryl monooleate, N hydroxymethyl acrylamide insulation reaction 2-3 hour, then add other leftover materials and be cooled to stirring at room temperature grinding 1-2 hour and get final product.
The preparation method of described a kind of anti-static cashmere composite fibre containing stainless steel fibre, is characterized in that comprising the following steps:
(1) by rattletop, the bark of official magnolia, pineapple leaves boiling 4-6 hour, filter, polyethylene glycol stearate diester, lemon oil, auxiliary agent stirring 30-40 minute is added in filtrate, drop into lamb suede, the rabbit hair, soybean fiber, nanometer bamboo carbon fiber, stainless steel fibre immersion 10-13 hour, pull oven dry, degreasing, ultra-fine grinding out;
(2) add water artificial zeolite powder grinding pulping, adds nano titanium oxide and stir and evenly mix and put into Ultrasonic machining groove, concussion 6-12 hour, dries grinding 2-4 hour;
(3) take 1-ethyl-3-methylimidazole acetate, 1-allyl-3-methylimidazole villaumite drops in reactor and stirs and evenly mixs, add aloe fibre, step (1), (2) product grinding 30-50 minute, be heated to 100-120 DEG C, add other residual components agitation grinding 50-70 minute, obtained spinning solution, through spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: the present invention adopts multicomponent fibre and cashmere blending technology, the cashmere composite fibre obtained can make up the defect of simple cashmere fiber, make cashmere product more frivolous, because stainless steel fibre has conduction, anti electromagnetic wave, antistatic, abrasion-resistant, high temperature resistant, the effects such as cut resistant, with the addition of nano titanium oxide and other active ingredient simultaneously, the cashmere composite fibre after blending is made to have antistatic, antibacterial Anti-moth-eating, wear-resisting, the specific functions such as radiation proof, that can improve goods wears performance, improve added value and the class of fleece fabrics.
Detailed description of the invention
Described a kind of anti-static cashmere composite fibre containing stainless steel fibre, it is characterized in that, be made up of the raw material of following weight portion: lamb suede 32, the rabbit hair 12, soybean fiber 9, nanometer bamboo carbon fiber 7, stainless steel fibre 11, aloe fibre 5, polyethylene glycol stearate diester 5, lemon oil 0.02, PTMG 1.7, monoethanolamine 5, nano titanium oxide 0.7, artificial zeolite powder 4, rattletop 1, the bark of official magnolia 3, pineapple leaves 5,1-ethyl-3-methylimidazole acetate 115,1-allyl-3-methylimidazole villaumite 107, auxiliary agent 22, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: methyl acrylate 32, butyl methacrylate 43, haloflex 17, methacrylic acid 12, 1,2-PD 15, polypropylene glycol diglycidyl ether 26, hydroxypropyl methylcellulose 1, Silane coupling agent KH550 0.7, triethanolamine 3, tributyl phosphate 14, glyceryl monooleate 16, sodium metasilicate 0.3, microcrystalline wax 8, N hydroxymethyl acrylamide 6, deionized water 180, its preparation method is by methacrylic acid, 1,2-PD, polypropylene glycol diglycidyl ether puts into reactor mixing and stirring, is warming up to 140-155 DEG C, adds Silane coupling agent KH550 and keeps thermotonus 3-5 hour, be cooled to 85-100 DEG C, add methyl acrylate, butyl methacrylate, haloflex, pours nitrogen, keeps temperature to heat while stirring, adds tributyl phosphate, glyceryl monooleate, N hydroxymethyl acrylamide insulation reaction 2-3 hour, then add other leftover materials and be cooled to stirring at room temperature grinding 1-2 hour and get final product.
Preparation method comprises the following steps:
(1) by rattletop, the bark of official magnolia, pineapple leaves boiling 4-6 hour, filter, polyethylene glycol stearate diester, lemon oil, auxiliary agent stirring 30-40 minute is added in filtrate, drop into lamb suede, the rabbit hair, soybean fiber, nanometer bamboo carbon fiber, stainless steel fibre immersion 10-13 hour, pull oven dry, degreasing, ultra-fine grinding out;
(2) add water artificial zeolite powder grinding pulping, adds nano titanium oxide and stir and evenly mix and put into Ultrasonic machining groove, concussion 6-12 hour, dries grinding 2-4 hour;
(3) take 1-ethyl-3-methylimidazole acetate, 1-allyl-3-methylimidazole villaumite drops in reactor and stirs and evenly mixs, add aloe fibre, step (1), (2) product grinding 30-50 minute, be heated to 100-120 DEG C, add other residual components agitation grinding 50-70 minute, obtained spinning solution, through spinning, winding, boundling, stretching and get final product.
The technical parameter index of the cashmere composite fibre using the present invention to produce is as follows:
(1) feel cunning is glutinous, drapability good, moisture absorption is ventilative, warming, environmental protection;
(2) detect according to national standard, its Anti-moth-eating index reaches 1A level, mothproof qualified;
(3) after 30 washings, antibiotic rate still reaches 96%;
(4) antistatic behaviour of this cashmere composite fibre under the condition of washing 30 times is measured according to the method for national standard GB/T 12703.4-2010 and GBT12703.5-2010 good.
Claims (2)
1. the anti-static cashmere composite fibre containing stainless steel fibre, it is characterized in that, be made up of the raw material of following weight portion: lamb suede 30-35, rabbit hair 10-13, soybean fiber 6-9, nanometer bamboo carbon fiber 7-10, stainless steel fibre 11-14, aloe fibre 5-8, polyethylene glycol stearate diester 4-7, lemon oil 0.02-0.04, PTMG 1.3-2.5, monoethanolamine 3-5, nano titanium oxide 0.6-1.1, artificial zeolite powder 2-4, rattletop 1-3, bark of official magnolia 3-4, pineapple leaves 4-6, 1-ethyl-3-methylimidazole acetate 110-120, 1-allyl-3-methylimidazole villaumite 100-110, auxiliary agent 20-24, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: methyl acrylate 30-35, butyl methacrylate 40-45, haloflex 15-20, methacrylic acid 10-15, 1,2-PD 13-18, polypropylene glycol diglycidyl ether 20-30, hydroxypropyl methylcellulose 1-3, Silane coupling agent KH550 0.4-0.8, triethanolamine 3-6, tributyl phosphate 12-15, glyceryl monooleate 14-18, sodium metasilicate 0.2-0.5, microcrystalline wax 7-9, N hydroxymethyl acrylamide 4-7, deionized water 100-200, its preparation method is by methacrylic acid, 1,2-PD, polypropylene glycol diglycidyl ether puts into reactor mixing and stirring, is warming up to 140-155 DEG C, adds Silane coupling agent KH550 and keeps thermotonus 3-5 hour, be cooled to 85-100 DEG C, add methyl acrylate, butyl methacrylate, haloflex, pours nitrogen, keeps temperature to heat while stirring, adds tributyl phosphate, glyceryl monooleate, N hydroxymethyl acrylamide insulation reaction 2-3 hour, then add other leftover materials and be cooled to stirring at room temperature grinding 1-2 hour and get final product.
2. the preparation method of a kind of anti-static cashmere composite fibre containing stainless steel fibre according to claim 1, is characterized in that comprising the following steps:
(1) by rattletop, the bark of official magnolia, pineapple leaves boiling 4-6 hour, filter, polyethylene glycol stearate diester, lemon oil, auxiliary agent stirring 30-40 minute is added in filtrate, drop into lamb suede, the rabbit hair, soybean fiber, nanometer bamboo carbon fiber, stainless steel fibre immersion 10-13 hour, pull oven dry, degreasing, ultra-fine grinding out;
(2) add water artificial zeolite powder grinding pulping, adds nano titanium oxide and stir and evenly mix and put into Ultrasonic machining groove, concussion 6-12 hour, dries grinding 2-4 hour;
(3) take 1-ethyl-3-methylimidazole acetate, 1-allyl-3-methylimidazole villaumite drops in reactor and stirs and evenly mixs, add aloe fibre, step (1), (2) product grinding 30-50 minute, be heated to 100-120 DEG C, add other residual components agitation grinding 50-70 minute, obtained spinning solution, through spinning, winding, boundling, stretching and get final product.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106757442A (en) * | 2016-12-13 | 2017-05-31 | 安徽天威羊绒制品有限公司 | A kind of oil-stain-preventing collagen Cashmere composite shell fabric and preparation method thereof |
| WO2019006941A1 (en) * | 2017-07-07 | 2019-01-10 | 苏州市晨彩纺织研发有限公司 | Antistatic textile fabric and preparation method therefor |
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| CN104264277A (en) * | 2014-09-09 | 2015-01-07 | 安徽省含山县富强羽绒制品有限公司 | Mothproof down feather composite fiber and preparation method thereof |
| CN104278359A (en) * | 2014-10-14 | 2015-01-14 | 安徽天鹅科技实业（集团）有限公司 | Cotton fibers with antibacterial and insect-resisting effects and production method of cotton fibers |
| CN104357948A (en) * | 2014-10-15 | 2015-02-18 | 安徽颍元农业科技股份有限公司 | Cotton fiber modified by dead sea black mud and preparation method of cotton fiber |
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Patent Citations (4)
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| US20100176210A1 (en) * | 2009-01-09 | 2010-07-15 | Porex Corporation | Hydrophilic Porous Wicks for Vaporizable Materials |
| CN104264277A (en) * | 2014-09-09 | 2015-01-07 | 安徽省含山县富强羽绒制品有限公司 | Mothproof down feather composite fiber and preparation method thereof |
| CN104278359A (en) * | 2014-10-14 | 2015-01-14 | 安徽天鹅科技实业（集团）有限公司 | Cotton fibers with antibacterial and insect-resisting effects and production method of cotton fibers |
| CN104357948A (en) * | 2014-10-15 | 2015-02-18 | 安徽颍元农业科技股份有限公司 | Cotton fiber modified by dead sea black mud and preparation method of cotton fiber |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106757442A (en) * | 2016-12-13 | 2017-05-31 | 安徽天威羊绒制品有限公司 | A kind of oil-stain-preventing collagen Cashmere composite shell fabric and preparation method thereof |
| WO2019006941A1 (en) * | 2017-07-07 | 2019-01-10 | 苏州市晨彩纺织研发有限公司 | Antistatic textile fabric and preparation method therefor |
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Application publication date: 20151028 |