CN104213247A - Water-washable silk composite fiber and preparation method thereof - Google Patents
Water-washable silk composite fiber and preparation method thereof Download PDFInfo
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Abstract
Disclosed water-washable silk composite fiber is characterized by being prepared from the following raw materials in parts by weight: 18-22 parts of silk, 11-13 parts of wool, 4-7 parts of cuprammonium rayon, 6-8 parts of polyester fiber, 8-10 parts of newdal fiber, 10-12 parts of bast fiber, 0.6-1.1 parts of nanometer TiO2, 6-9 parts of aloe viscose fiber, 0.7-0.9 parts of hydroxypropyl methyl cellulose, 0.8-1.4 parts of polypropylenglycol diglycidyl ether, 100-110 parts of 1-butyl-3-methylimidazolium dibutyl phosphate, 110-120 parts of 1-ethyl-3-methylimidazolium diethylphosphate, 1-3 parts of radix aucklandiae, 2-4 parts of cortex moutan, 3-5 parts of an auxiliary agent, and proper amount of water. By adding cuprammonium rayon and nanometer TiO2, the silk composite fiber has performances of resisting ultraviolet, resisting static electricity, resisting water washing and the like; and additionally by adding aloe viscose fiber, the Chinese herbal medicines and other compositions, the prepared silk composite fiber has the characteristics of resisting bacteria, diminishing inflammation, light and soft texture, excellent air permeability, high strength and high elasticity, and thus the silk composite fiber is repeatedly cleanable and keeps comfortableness, and is not flat or sunk after being used for a long time.
Description
Technical field
The present invention relates to nonwoven material technical field, be specifically related to a kind of silk composite fibre of washing and preparation method thereof.
Background technology
Silk is matured silkworm concretionary continuous fiber of secreted silk liquid while cocooing, also claiming natural silk, is the lightest the thinnest the most soft natural fabric of occurring in nature, mainly animal protein, consists of, be rich in 18 kinds of necessary amino acid of human body, can promote Skin Cell vigor, anti-vascular sclerosis, long-term use can anti-skin senescence, some skin disease is had to special antipruritic effect, to arthritis, scapulohumeral periarthritis, asthma has certain health-care function.Have " human body the second skin ", " fiber queen's " good reputation.Because silk light weight is and elongated, fabric sheen is good, comfortable and easy to wear, and feel is smooth plentiful, poor heat conductivity, and moisture absorption is ventilative, has determined the health care that silk is good, is widely used in industry, beauty treatment and medicine and other fields.
In prior art, use natural silk to have many defects: one, use cost is too high; Two, because of the humidity of environment, make moist, preserve the improper raw mite that easily goes mouldy; Three, intensity is poor, and conglomeration reduces warmth retention property, affects attractive in appearance; Four, frequent static electrification, makes troubles to people etc.So develop a kind of existing environmental protection, health care, the healthy warmth retention property that is conducive to again people is strong, high strength, fire-retardant, antibacterial, laundry-resistant silk composite fibre can solve the deficiencies in the prior art smoothly.
Summary of the invention
Object of the present invention is just to provide a kind of silk composite fibre of washing and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A silk composite fibre of washing, is characterized in that, by the raw material of following weight portion, is made: silk 18-22, wool 11-13, copper ammonia fibre 4-7, polyster fibre 6-8, Newdal Fiber 8-10, flax fibre 10-12, nano-TiO
20.6-1.1, aloe viscose 6-9, hydroxypropyl methylcellulose 0.7-0.9, polypropylene glycol diglycidyl ether 0.8-1.4,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110,1-ethyl-3-methylimidazole diethyl phosphate 110-120, costus root 1-3, root bark of tree peony 2-4, auxiliary agent 3-5, suitable quantity of water.
Described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling makes the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.
The preparation method of described a kind of silk composite fibre of washing, is characterized in that comprising the following steps:
(1) by costus root, root bark of tree peony boiling 4-6 hour, filter, in filtrate, drop into silk, wool, polyster fibre immersion 10-13 hour, evenly spray into polypropylene glycol diglycidyl ether after pulling oven dry, degreasing, ultra-fine grinding out;
(2) toward adding water in hydroxypropyl methylcellulose, be stirred to dissolving, add Newdal Fiber, aloe viscose, nano-TiO
2ultrasonic wave is pulverized and is ground 20-30 minute together;
(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;
(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.
The present invention has following beneficial effect: the present invention adds copper ammonia fibre, nano-TiO
2there is uvioresistant, the function such as antistatic, water-fastness, add in addition the compositions such as aloe viscose, Chinese herbal medicine, the silk composite fibre making has anti-inflammation, quality is light and soft, gas permeability is good, intensity is high, elasticity is high characteristic, therefore the present invention can clean and keep its comfortableness repeatedly, also use for a long time not flat collapsing.
The specific embodiment
Described a kind of silk composite fibre of washing, is characterized in that, by the raw material of following weight portion, is made: silk 19 wools 12, copper ammonia fibre 5, polyster fibre 6, Newdal Fiber 10, flax fibre 11, nano-TiO
20.8, aloe viscose 9, hydroxypropyl methylcellulose 0.7, polypropylene glycol diglycidyl ether 1.2,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100,1-ethyl-3-methylimidazole diethyl phosphate 110, costus root 1, the root bark of tree peony 2, auxiliary agent 4, suitable quantity of water.
Described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.6, fatty diglycollic amide 0.7, polyvinylpyrrolidone 0.2, trihydroxy ethylamine oleate soap 1.6, acrylate and vinyl acetate emulsion 1.2, nano-calcium carbonate 2, bamboo fibre 1, SIMMONDSIA CHINENSIS SEED OIL 2, the root of purple-flowered peucedanum 4, dried orange peel 5, cordate houttuynia 3.1, its preparation method is that the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling are made to the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre to soak 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.
Preparation method comprises the following steps:
(1) by costus root, root bark of tree peony boiling 4-6 hour, filter, in filtrate, drop into silk, wool, polyster fibre immersion 10-13 hour, evenly spray into polypropylene glycol diglycidyl ether after pulling oven dry, degreasing, ultra-fine grinding out;
(2) toward adding water in hydroxypropyl methylcellulose, be stirred to dissolving, add Newdal Fiber, aloe viscose, nano-TiO
2ultrasonic wave is pulverized and is ground 20-30 minute together;
(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;
(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.
The technical parameter index of the silk composite fibre that use the present invention produces is as follows:
(1) light weight, warming, gas permeability is good, water-fastness;
(2) finished product is all greater than 99.6% to the bacteriostasis rate of Escherichia coli, staphylococcus aureus, Candida albicans;
(3) thermal conductivity factor 0.053(m ℃).
Claims (2)
1. the silk composite fibre that can wash, is characterized in that, by the raw material of following weight portion, is made: silk 18-22, wool 11-13, copper ammonia fibre 4-7, polyster fibre 6-8, Newdal Fiber 8-10, flax fibre 10-12, nano-TiO
20.6-1.1, aloe viscose 6-9, hydroxypropyl methylcellulose 0.7-0.9, polypropylene glycol diglycidyl ether 0.8-1.4,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110,1-ethyl-3-methylimidazole diethyl phosphate 110-120, costus root 1-3, root bark of tree peony 2-4, auxiliary agent 3-5, suitable quantity of water, described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling makes the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.
2. the preparation method of a kind of silk composite fibre of washing according to claim 1, is characterized in that comprising the following steps:
(1) by costus root, root bark of tree peony boiling 4-6 hour, filter, in filtrate, drop into silk, wool, polyster fibre immersion 10-13 hour, evenly spray into polypropylene glycol diglycidyl ether after pulling oven dry, degreasing, ultra-fine grinding out;
(2) toward adding water in hydroxypropyl methylcellulose, be stirred to dissolving, add Newdal Fiber, aloe viscose, nano-TiO
2ultrasonic wave is pulverized and is ground 20-30 minute together;
(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;
(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104862803A (en) * | 2015-06-09 | 2015-08-26 | 苏州市轩德纺织科技有限公司 | Antibiosis acarus killing textile material and preparation method |
| CN104911733A (en) * | 2015-05-20 | 2015-09-16 | 铜陵宏正网络科技有限公司 | Spandex fiber-containing dry cleaning-resistant flame-retardant cashmere composite fiber and manufacturing method thereof |
| CN104975407A (en) * | 2015-06-17 | 2015-10-14 | 江苏德利恒棉业有限公司 | Newdal and silk fiber denim and production process thereof |
| CN105088768A (en) * | 2015-08-31 | 2015-11-25 | 安徽天威羊绒制品有限公司 | Hydrophobic modified antimicrobial cashmere fiber and manufacturing method of hydrophobic modified antimicrobial cashmere fiber |
| CN105088769A (en) * | 2015-08-31 | 2015-11-25 | 安徽天威羊绒制品有限公司 | Ultra-fine denier nylon 6 short fiber blended self-cleaning cashmere fiber and manufacture method of self-cleaning cashmere fiber |
| CN105113233A (en) * | 2015-08-31 | 2015-12-02 | 安徽天威羊绒制品有限公司 | Breathable moisture-adsorption cashmere fiber added with modified aloe viscose fiber and preparation method thereof |
| CN105155261A (en) * | 2015-08-31 | 2015-12-16 | 安徽天威羊绒制品有限公司 | Light-resistance and antistatic cashmere fiber and production method thereof |
| CN105239173A (en) * | 2015-08-31 | 2016-01-13 | 安徽天威羊绒制品有限公司 | Heat endurance high abrasion resistance warm keeping cashmere fiber and manufacturing method thereof |
| CN106388016A (en) * | 2016-12-26 | 2017-02-15 | 常熟市德欧纺织品有限公司 | Antibacterial combed cotton fabric |
| CN106435982A (en) * | 2016-12-26 | 2017-02-22 | 常熟市德欧纺织品有限公司 | Antibacterial nano viscose fabric |
| CN106490734A (en) * | 2016-12-26 | 2017-03-15 | 常熟市德欧纺织品有限公司 | A kind of waterproof nano viscose fabric |
| CN106510044A (en) * | 2016-12-26 | 2017-03-22 | 常熟市德欧纺织品有限公司 | Waterproof conductive fiber fabric |
| CN106510062A (en) * | 2016-12-26 | 2017-03-22 | 常熟市德欧纺织品有限公司 | Color-changing conductive fiber fabric |
| CN110339484A (en) * | 2019-05-21 | 2019-10-18 | 青岛市肿瘤医院 | A kind of tumour Far-infrared thermotherapy device |
| CN110565208A (en) * | 2018-06-06 | 2019-12-13 | 安徽瑞华棉业发展股份有限公司 | Child bed sheet fabric and preparation method thereof |
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Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104911733A (en) * | 2015-05-20 | 2015-09-16 | 铜陵宏正网络科技有限公司 | Spandex fiber-containing dry cleaning-resistant flame-retardant cashmere composite fiber and manufacturing method thereof |
| CN104862803A (en) * | 2015-06-09 | 2015-08-26 | 苏州市轩德纺织科技有限公司 | Antibiosis acarus killing textile material and preparation method |
| CN104975407A (en) * | 2015-06-17 | 2015-10-14 | 江苏德利恒棉业有限公司 | Newdal and silk fiber denim and production process thereof |
| CN105088768A (en) * | 2015-08-31 | 2015-11-25 | 安徽天威羊绒制品有限公司 | Hydrophobic modified antimicrobial cashmere fiber and manufacturing method of hydrophobic modified antimicrobial cashmere fiber |
| CN105088769A (en) * | 2015-08-31 | 2015-11-25 | 安徽天威羊绒制品有限公司 | Ultra-fine denier nylon 6 short fiber blended self-cleaning cashmere fiber and manufacture method of self-cleaning cashmere fiber |
| CN105113233A (en) * | 2015-08-31 | 2015-12-02 | 安徽天威羊绒制品有限公司 | Breathable moisture-adsorption cashmere fiber added with modified aloe viscose fiber and preparation method thereof |
| CN105155261A (en) * | 2015-08-31 | 2015-12-16 | 安徽天威羊绒制品有限公司 | Light-resistance and antistatic cashmere fiber and production method thereof |
| CN105239173A (en) * | 2015-08-31 | 2016-01-13 | 安徽天威羊绒制品有限公司 | Heat endurance high abrasion resistance warm keeping cashmere fiber and manufacturing method thereof |
| CN106388016A (en) * | 2016-12-26 | 2017-02-15 | 常熟市德欧纺织品有限公司 | Antibacterial combed cotton fabric |
| CN106435982A (en) * | 2016-12-26 | 2017-02-22 | 常熟市德欧纺织品有限公司 | Antibacterial nano viscose fabric |
| CN106490734A (en) * | 2016-12-26 | 2017-03-15 | 常熟市德欧纺织品有限公司 | A kind of waterproof nano viscose fabric |
| CN106510044A (en) * | 2016-12-26 | 2017-03-22 | 常熟市德欧纺织品有限公司 | Waterproof conductive fiber fabric |
| CN106510062A (en) * | 2016-12-26 | 2017-03-22 | 常熟市德欧纺织品有限公司 | Color-changing conductive fiber fabric |
| CN110565208A (en) * | 2018-06-06 | 2019-12-13 | 安徽瑞华棉业发展股份有限公司 | Child bed sheet fabric and preparation method thereof |
| CN110339484A (en) * | 2019-05-21 | 2019-10-18 | 青岛市肿瘤医院 | A kind of tumour Far-infrared thermotherapy device |
| CN110339484B (en) * | 2019-05-21 | 2021-04-30 | 青岛市肿瘤医院 | Far infrared thermotherapy device for tumour |
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