CN104831411A - Multifunctional mothproof down feather composite fiber and producing method thereof - Google Patents

Abstract

The invention discloses multifunctional mothproof down feather composite fiber characterized by comprising the following raw materials by weight: 12-14 parts of down feather, 19-23 parts of chicken feather, 15-18 parts of pig hair, 13-15 parts of lamb wool, 7-10 parts of combed cotton fiber, 6-9 parts of melton fiber, 0.4-0.7 parts of sodium polyacrylate, 0.04-0.08 parts of hyaluronic acid, 13-16 parts of paper pulp, 1.1-2.3 parts of carbon black, 2-3 parts of coptis, 1-3 parts of amomum cardamomum, 2-4 parts of clove, 0.6-1.1 parts o nano-aluminium oxide, 4-6 parts of epoxy butyl oleate, 100-120 parts of 1-butyl-3-methyl imidazole dimethyl phosphate, 110-125 parts of 1-butyl-3-methyl imidazole acetate, 2-4 parts of additives and proper amount of water. The multifunctional mothproof down feather composite fiber is added with a variety of active ingredients, wide in source of raw materials, green and environmentally-friendly, and the prepared multifunctional mothproof down feather composite fiber is warm-keeping, mothproof, simple to make, economical and practical.

Description

A kind of Multifunctional mothproof shell eider down composite fibre and preparation method thereof

Technical field

The present invention relates to nonwoven material technical field, be specifically related to a kind of Multifunctional mothproof shell eider down composite fibre and preparation method thereof.

Background technology

Eider down is the long belly goose, duck, becomes the fine hair of a reed catkins shape, slabbing be feather.Because eider down is a kind of animal protein fiber, higher than cotton (vegetative fiber element) heat insulating ability, and ten million leg-of-mutton tiny pore that eider down nodular fibrous gathers, can the convergent-divergent with temperature Change, produce temperature adjustment function, Absorbable rod human body distributes the hot gas of flowing, the invasion of isolated cool ambient air, because eider down has the superperformance that the softly warming of this uniqueness and moisture absorption disperse, determine the health care that eider down is good, eiderdown quilt be widely used in clothes, wadded a quilt with cotton, the fields such as filler of weaving.

Natural down is used to there is many defects in prior art: one, because eider down content in feather is little, usually only to account for 20-25%, thus make the use cost of eider down too high; Two, eider down makes moist because of the humidity of environment, preserves the improper raw mite that easily goes mouldy; Three, intensity is poor, can make eider down pulverizing, conglomeration, reduce warmth retention property, affect attractive in appearance more than washed; Four, the frequent static electrification of eider down in prior art, brings inconvenience; Five, existing eider down does not have the characteristics such as fire-retardant, antibacterial, water-fastness, there is the hidden danger such as safety, so develop a kind of existing environmental protection, health care, the warmth retention property being conducive to again the health of people is strong, high strength, fire-retardant, antibacterial, laundry-resistant eider down composite fibre can solve the deficiencies in the prior art smoothly.

Summary of the invention

Object of the present invention is just to provide a kind of Multifunctional mothproof shell eider down composite fibre and preparation method thereof, to overcome the deficiencies in the prior art.

The object of the present invention is achieved like this:

A kind of Multifunctional mothproof shell eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: duck's down 12-14, chicken feather 19-23, pig hair 15-18, little wool 13-15, combing cotton fibre 7-10, melton fiber 6-9, Sodium Polyacrylate 0.4-0.7, hyaluronic acid 0.04-0.08, paper pulp 13-16, carbon black 1.1-2.3, coptis 2-3, Amomum cardamomum 1-3, cloves 2-4, nano-aluminium oxide 0.6-1.1, epoxyoleic acid butyl ester 4-6, 1-butyl-3-methylimidazole dimethyl phosphate 100-120, 1-butyl-3-N-Methylimidazoleacetic salt 110-125, auxiliary agent 2-4, suitable quantity of water.

Described auxiliary agent is made up of following raw materials in part by weight: kaolin 2-3, menthol 0.2-0.4, rilanit special polyoxyethylene ether 3-5, dimethicone 2-4, carboxymethyl cellulose 1-2, imidazoline quaternary ammonium salt 0.4-0.7, tarragon 1-3, Asian puccoon 2-3, water 100, its preparation method is by tarragon, Asian puccoon boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, kaolin is added in filtrate, soak 10-12 hour, add other residual componentss again and add thermal agitation, grinding 20-30 minute, to obtain final product.

The preparation method of described a kind of Multifunctional mothproof shell eider down composite fibre, is characterized in that comprising the following steps:

(1) coptis, Amomum cardamomum, cloves boiling 1-2 hour is got, filter, filter residue, paper pulp are dried and pulverized, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to clean, add nano-aluminium oxide, pre-grind 2-3 hour;

(2) duck's down, chicken feather, pig hair, little wool are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray vaporific epoxyoleic acid butyl ester;

(3) take 1-butyl-3-methylimidazole dimethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add combing cotton fibre, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;

(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.

The present invention has following beneficial effect: the present invention adds plurality of active ingredients, the wide environmental protection of raw material sources, obtained eider down composite fibre not only warming but also Anti-moth-eating, makes simple, economical and practical.

Detailed description of the invention

Described a kind of Multifunctional mothproof shell eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: duck's down 13, chicken feather 19, pig hair 16, little wool 14, combing cotton fibre 8, melton fiber 6, Sodium Polyacrylate 0.4, hyaluronic acid 0.07, paper pulp 13, carbon black 1.7, the coptis 2, Amomum cardamomum 1, cloves 4, nano-aluminium oxide 0.6, epoxyoleic acid butyl ester 4,1-butyl-3-methylimidazole dimethyl phosphate 100,1-butyl-3-N-Methylimidazoleacetic salt 110, auxiliary agent 3, suitable quantity of water.

Described auxiliary agent is made up of following raw materials in part by weight: kaolin 2, menthol 0.2, rilanit special polyoxyethylene ether 5, dimethicone 4, carboxymethyl cellulose 1, imidazoline quaternary ammonium salt 0.4, tarragon 1, Asian puccoon 2, water 100, its preparation method is by tarragon, Asian puccoon boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, kaolin is added in filtrate, soak 10-12 hour, add other residual componentss again and add thermal agitation, grinding 20-30 minute, to obtain final product.

Preparation method comprises the following steps:

(1) coptis, Amomum cardamomum, cloves boiling 1-2 hour is got, filter, filter residue, paper pulp are dried and pulverized, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to clean, add nano-aluminium oxide, pre-grind 2-3 hour;

(2) duck's down, chicken feather, pig hair, little wool are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray vaporific epoxyoleic acid butyl ester;

(3) take 1-butyl-3-methylimidazole dimethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add combing cotton fibre, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;

(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.

The technical parameter index of the eider down composite fibre using the present invention to produce is as follows:

(1) light weight, warming, environmental protection;

(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99.6%;

(3) after 30 washings, antibiotic rate still reaches 96%.

Claims (2)

1. a Multifunctional mothproof shell eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: duck's down 12-14, chicken feather 19-23, pig hair 15-18, little wool 13-15, combing cotton fibre 7-10, melton fiber 6-9, Sodium Polyacrylate 0.4-0.7, hyaluronic acid 0.04-0.08, paper pulp 13-16, carbon black 1.1-2.3, coptis 2-3, Amomum cardamomum 1-3, cloves 2-4, nano-aluminium oxide 0.6-1.1, epoxyoleic acid butyl ester 4-6, 1-butyl-3-methylimidazole dimethyl phosphate 100-120, 1-butyl-3-N-Methylimidazoleacetic salt 110-125, auxiliary agent 2-4, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: kaolin 2-3, menthol 0.2-0.4, rilanit special polyoxyethylene ether 3-5, dimethicone 2-4, carboxymethyl cellulose 1-2, imidazoline quaternary ammonium salt 0.4-0.7, tarragon 1-3, Asian puccoon 2-3, water 100, its preparation method is by tarragon, Asian puccoon boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, kaolin is added in filtrate, soak 10-12 hour, add other residual componentss again and add thermal agitation, grinding 20-30 minute, to obtain final product.

2. the preparation method of a kind of Multifunctional mothproof shell eider down composite fibre according to claim 1, is characterized in that comprising the following steps:

(1) coptis, Amomum cardamomum, cloves boiling 1-2 hour is got, filter, filter residue, paper pulp are dried and pulverized, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to clean, add nano-aluminium oxide, pre-grind 2-3 hour;

(2) duck's down, chicken feather, pig hair, little wool are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray vaporific epoxyoleic acid butyl ester;

(3) take 1-butyl-3-methylimidazole dimethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add combing cotton fibre, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;

(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.