CN104278355A - Washable light down feather composite fiber and preparation method thereof - Google Patents
Washable light down feather composite fiber and preparation method thereof Download PDFInfo
- Publication number
- CN104278355A CN104278355A CN201410454554.9A CN201410454554A CN104278355A CN 104278355 A CN104278355 A CN 104278355A CN 201410454554 A CN201410454554 A CN 201410454554A CN 104278355 A CN104278355 A CN 104278355A
- Authority
- CN
- China
- Prior art keywords
- parts
- butyl
- composite fiber
- add
- fiber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a washable light down feather composite fiber. The washable light down feather composite fiber is characterized by being prepared from the following raw materials in parts by weight: 12-14 parts of goose down, 15-20 parts of pig hair, 14-17 parts of camel hair, 6-8 parts of plumetis fibers, 10-12 parts of tencel fibers, 7-9 parts of cheviot fibers, 2.1-3.3 parts of sorbitol, 1.2-3.4 parts of glycerol monolaurate, 10-13 parts of grapevine, 1.2-3.1 parts of citric acid, 2-4 parts of phellodendron amurense, 1-3 parts of white atractylodes rhizome, 2-3 parts of the root bark of white mulberry, 0.3-0.5 part of magnesium chloride, 3-5 parts of oxidized castor oil, 100-120 parts of 1-butyl-3-methylimidazolium acetate, 110-130 parts of 1-butyl-3-methylimidazolium dibutyl phosphate, 1-3 parts of assistants and an appropriate amount of water. According to the washable light down feather composite fiber, the pig hairs and the camel hairs are added, and therefore, the feather utilization rate is increased and the cost is reduced; and the phellodendron amurense, the white atractylodes rhizome, the root bark of white mulberry and other Chinese herbal medicines are added, so that the washable light down feather composite fiber has the advantages of health keeping, sterilization, excellent breathability, washing durability and the like.
Description
Technical field
The present invention relates to nonwoven material technical field, be specifically related to a kind of laundry-resistant lightweight eider down composite fibre and preparation method thereof.
Background technology
Eider down is the long belly goose, duck, becomes the fine hair of a reed catkins shape, slabbing be feather.Because eider down is a kind of animal protein fiber, higher than cotton (vegetative fiber element) heat insulating ability, and ten million leg-of-mutton tiny pore that eider down nodular fibrous gathers, can the convergent-divergent with temperature Change, produce temperature adjustment function, Absorbable rod human body distributes the hot gas of flowing, the invasion of isolated cool ambient air, because eider down has the superperformance that the softly warming of this uniqueness and moisture absorption disperse, determine the health care that eider down is good, eiderdown quilt be widely used in clothes, wadded a quilt with cotton, the fields such as filler of weaving.
Natural down is used to there is many defects in prior art: one, because eider down content in feather is little, usually only to account for 20-25%, thus make the use cost of eider down too high; Two, eider down makes moist because of the humidity of environment, preserves the improper raw mite that easily goes mouldy; Three, intensity is poor, can make eider down pulverizing, conglomeration, reduce warmth retention property, affect attractive in appearance more than washed; Four, the frequent static electrification of eider down in prior art, brings inconvenience; Five, existing eider down does not have the characteristics such as fire-retardant, antibacterial, water-fastness, there is the hidden danger such as safety, so develop a kind of existing environmental protection, health care, the warmth retention property being conducive to again the health of people is strong, high strength, fire-retardant, antibacterial, laundry-resistant eider down composite fibre can solve the deficiencies in the prior art smoothly.
Summary of the invention
Object of the present invention is just to provide a kind of laundry-resistant lightweight eider down composite fibre and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of laundry-resistant lightweight eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: goose down 12-14, pig hair 15-20, camel hair 14-17, plumetis fiber 6-8, tencel fiber 10-12, cheviot fiber 7-9, sorbierite 2.1-3.3, lauric monoglyceride 1.2-3.4, grapevine 10-13, citric acid 1.2-3.1, golden cypress 2-4, bighead atractylodes rhizome 1-3, root bark of white mulberry 2-3, magnesium chloride 0.3-0.5, blown castor oil 3-5, 1-butyl-3-N-Methylimidazoleacetic salt 100-120, 1-butyl-3-methylimidazole dibutylphosphoric acid ester 110-130, auxiliary agent 1-3, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: polymer dispersion powder 1-2, even bubble silicone oil 3-4, Benzotriazole Ultraviolet Stabilizer 0.03-0.05, polyvinylpyrrolidone 0.2-0.4, trihydroxy ethylamine oleate soap 1.2-3.4, kuh-seng 1-3, erythrina bark 2-4, camphor 0.1-0.3, water 100, its preparation method is by kuh-seng, erythrina bark, camphor boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add other residual componentss be heated to 45-55 DEG C of agitation grinding 20-30 minute, to obtain final product.
The preparation method of described a kind of laundry-resistant lightweight eider down composite fibre, is characterized in that comprising the following steps:
(1) by golden cypress, the bighead atractylodes rhizome, the root bark of white mulberry, grapevine boiling 5-7 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to totally adding lauric monoglyceride, citric acid grinding 10-15 minute;
(2) goose down, pig hair, camel hair, tencel fiber are sprayed vaporific blown castor oil after washing, degreasing, ultra-fine grinding;
(3) take 1-butyl-3-N-Methylimidazoleacetic salt, 1-butyl-3-methylimidazole dibutylphosphoric acid ester drops in reactor and stirs and evenly mixs, add plumetis fiber, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: eider down composite fibre of the present invention adds pig hair, camel hair, improve the utilization rate of feather, reduce cost, also add the Chinese herbal medicines such as golden cypress, the bighead atractylodes rhizome, the root bark of white mulberry simultaneously, there is the advantages such as health-care sterilization, gas permeability be good, water-fastness.
Detailed description of the invention
Described one laundry-resistant lightweight eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: goose down 13, pig hair 17, camel hair 15, plumetis fiber 7, tencel fiber 11, cheviot fiber 7, sorbierite 2.8, lauric monoglyceride 1.7, grapevine 12, citric acid 1.9, golden cypress 2, the bighead atractylodes rhizome 1, the root bark of white mulberry 3, magnesium chloride 0.3, blown castor oil 3,1-butyl-3-N-Methylimidazoleacetic salt 100,1-butyl-3-methylimidazole dibutylphosphoric acid ester 130, auxiliary agent 1, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: polymer dispersion powder 1, even bubble silicone oil 3, Benzotriazole Ultraviolet Stabilizer 0.04, polyvinylpyrrolidone 0.2, trihydroxy ethylamine oleate soap 1.7, kuh-seng 1, erythrina bark 2, camphor 0.1, water 100, its preparation method is by kuh-seng, erythrina bark, camphor boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add other residual componentss be heated to 45-55 DEG C of agitation grinding 20-30 minute, to obtain final product.
Preparation method comprises the following steps:
(1) by golden cypress, the bighead atractylodes rhizome, the root bark of white mulberry, grapevine boiling 5-7 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to totally adding lauric monoglyceride, citric acid grinding 10-15 minute;
(2) goose down, pig hair, camel hair, tencel fiber are sprayed vaporific blown castor oil after washing, degreasing, ultra-fine grinding;
(3) take 1-butyl-3-N-Methylimidazoleacetic salt, 1-butyl-3-methylimidazole dibutylphosphoric acid ester drops in reactor and stirs and evenly mixs, add plumetis fiber step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The technical parameter index of the eider down composite fibre using the present invention to produce is as follows:
(1) light weight, warming, environmental protection;
(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99.7%;
(3) water-fastness, flame retardant effect is excellent.
Claims (2)
1. a laundry-resistant lightweight eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: goose down 12-14, pig hair 15-20, camel hair 14-17, plumetis fiber 6-8, tencel fiber 10-12, cheviot fiber 7-9, sorbierite 2.1-3.3, lauric monoglyceride 1.2-3.4, grapevine 10-13, citric acid 1.2-3.1, golden cypress 2-4, bighead atractylodes rhizome 1-3, root bark of white mulberry 2-3, magnesium chloride 0.3-0.5, blown castor oil 3-5, 1-butyl-3-N-Methylimidazoleacetic salt 100-120, 1-butyl-3-methylimidazole dibutylphosphoric acid ester 110-130, auxiliary agent 1-3, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: polymer dispersion powder 1-2, even bubble silicone oil 3-4, Benzotriazole Ultraviolet Stabilizer 0.03-0.05, polyvinylpyrrolidone 0.2-0.4, trihydroxy ethylamine oleate soap 1.2-3.4, kuh-seng 1-3, erythrina bark 2-4, camphor 0.1-0.3, water 100, its preparation method is by kuh-seng, erythrina bark, camphor boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add other residual componentss be heated to 45-55 DEG C of agitation grinding 20-30 minute, to obtain final product.
2. the preparation method of a kind of laundry-resistant lightweight eider down composite fibre according to claim 1, is characterized in that comprising the following steps:
(1) by golden cypress, the bighead atractylodes rhizome, the root bark of white mulberry, grapevine boiling 5-7 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to totally adding lauric monoglyceride, citric acid grinding 10-15 minute;
(2) goose down, pig hair, camel hair, tencel fiber are sprayed vaporific blown castor oil after washing, degreasing, ultra-fine grinding;
(3) take 1-butyl-3-N-Methylimidazoleacetic salt, 1-butyl-3-methylimidazole dibutylphosphoric acid ester drops in reactor and stirs and evenly mixs, add plumetis fiber, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410454554.9A CN104278355A (en) | 2014-09-09 | 2014-09-09 | Washable light down feather composite fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410454554.9A CN104278355A (en) | 2014-09-09 | 2014-09-09 | Washable light down feather composite fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104278355A true CN104278355A (en) | 2015-01-14 |
Family
ID=52253682
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410454554.9A Pending CN104278355A (en) | 2014-09-09 | 2014-09-09 | Washable light down feather composite fiber and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104278355A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104831409A (en) * | 2015-03-30 | 2015-08-12 | 安徽省三森纺织有限公司 | Washable down feather composite fiber added with titanium dioxide and producing method thereof |
| CN104831413A (en) * | 2015-03-30 | 2015-08-12 | 安徽省三森纺织有限公司 | Camellia nitidissima down feather composite fiber and producing method thereof |
| CN105926074A (en) * | 2016-04-28 | 2016-09-07 | 安徽华强羽绒有限公司 | Warming light eider down composite fiber and manufacturing method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030051112A (en) * | 2001-12-18 | 2003-06-25 | 최명부 | The Manufacture Metal to Shide Cotten |
| CN101536852A (en) * | 2009-04-23 | 2009-09-23 | 江苏丝乡丝绸股份有限公司 | Method for producing cocoon fiber quilt for dermatitis prevention |
| CN101736428A (en) * | 2009-12-23 | 2010-06-16 | 山东海龙股份有限公司 | Method for preparing Chinese medicinal cellulose fiber by solvent method |
| CN103055534A (en) * | 2012-12-20 | 2013-04-24 | 华南理工大学 | Method of extracting of essential oil in Chinese medicinal herb and cellulose comprehensive utilization |
| CN103276604A (en) * | 2013-05-10 | 2013-09-04 | 安徽一隆羽绒有限公司 | Wash-durable feather floss and feather fiber combined feather cotton and preparation method thereof |
| CN103710775A (en) * | 2013-12-18 | 2014-04-09 | 中国科学院过程工程研究所 | Preparation method of ionic liquid keratin spinning solutions |
-
2014
- 2014-09-09 CN CN201410454554.9A patent/CN104278355A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030051112A (en) * | 2001-12-18 | 2003-06-25 | 최명부 | The Manufacture Metal to Shide Cotten |
| CN101536852A (en) * | 2009-04-23 | 2009-09-23 | 江苏丝乡丝绸股份有限公司 | Method for producing cocoon fiber quilt for dermatitis prevention |
| CN101736428A (en) * | 2009-12-23 | 2010-06-16 | 山东海龙股份有限公司 | Method for preparing Chinese medicinal cellulose fiber by solvent method |
| CN103055534A (en) * | 2012-12-20 | 2013-04-24 | 华南理工大学 | Method of extracting of essential oil in Chinese medicinal herb and cellulose comprehensive utilization |
| CN103276604A (en) * | 2013-05-10 | 2013-09-04 | 安徽一隆羽绒有限公司 | Wash-durable feather floss and feather fiber combined feather cotton and preparation method thereof |
| CN103710775A (en) * | 2013-12-18 | 2014-04-09 | 中国科学院过程工程研究所 | Preparation method of ionic liquid keratin spinning solutions |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104831409A (en) * | 2015-03-30 | 2015-08-12 | 安徽省三森纺织有限公司 | Washable down feather composite fiber added with titanium dioxide and producing method thereof |
| CN104831413A (en) * | 2015-03-30 | 2015-08-12 | 安徽省三森纺织有限公司 | Camellia nitidissima down feather composite fiber and producing method thereof |
| CN105926074A (en) * | 2016-04-28 | 2016-09-07 | 安徽华强羽绒有限公司 | Warming light eider down composite fiber and manufacturing method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104264276A (en) | Mildew-proof down feather composite fiber and preparation method thereof | |
| CN104762691A (en) | Antimicrobial deodorizing down composite fiber and manufacturing method thereof | |
| CN104762692A (en) | Moisture-absorbing thermal-insulation down composite fiber and manufacturing method thereof | |
| CN104264277A (en) | Mothproof down feather composite fiber and preparation method thereof | |
| CN104195665B (en) | Eider down composite fibre that a kind of waste and old down fiber/acrylic staple fibre is compound and preparation method thereof | |
| CN104195664A (en) | Down feather composite fiber modified by polypropylene fiber and preparation method of down feather composite fiber | |
| CN104264275A (en) | Waterproof down feather composite fiber and preparation method thereof | |
| CN104233509A (en) | Down feather composite fibers with anion polyester staple fibers and production method thereof | |
| CN104233505A (en) | Antibacterial and mothproof silk composite fibers and manufacturing method thereof | |
| CN104213247A (en) | Water-washable silk composite fiber and preparation method thereof | |
| CN104294399A (en) | Down feather composite fibers with jasmine fragrance and preparation method thereof | |
| CN104278355A (en) | Washable light down feather composite fiber and preparation method thereof | |
| CN104762693A (en) | Regenerated down composite fiber and manufacturing method thereof | |
| CN104762694A (en) | Bactericidal mildewproof down composite fibers and manufacturing method thereof | |
| CN104831407A (en) | Compound warm down feather composite fiber and producing method thereof | |
| CN104213248A (en) | Moisture-absorbing air-permeable silk composite fiber and preparation method thereof | |
| CN104213245A (en) | Long-acting slow-release fragrant silk composite fiber and preparation method thereof | |
| CN104831411A (en) | Multifunctional mothproof down feather composite fiber and producing method thereof | |
| CN104213246A (en) | Silk composite fiber with anticancer function and preparation method thereof | |
| CN104233508A (en) | Puffed silk composite fibers with high elasticity and manufacturing method thereof | |
| CN104790063A (en) | Odor-removing down feather composite fiber and preparation method thereof | |
| CN104452266B (en) | A kind of antibacterial modified method of towel | |
| CN104357933A (en) | Ultraviolet-proof cotton fiber and preparation method thereof | |
| CN104233506A (en) | Silk composite fibers applicable to allergic constitution and manufacturing method thereof | |
| CN105862163A (en) | Cotton straw/bamboo fiber compounded down feather composite fibers and manufacturing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150114 |