CN104213248A - Moisture-absorbing air-permeable silk composite fiber and preparation method thereof - Google Patents

Abstract

Disclosed moisture-absorbing air-permeable silk composite fiber is characterized by being prepared from the following raw materials in parts by weight: 16-19 parts of silk, 13-15 parts of camel hair, 7-9 parts of coral fleece, 10-12 parts of ramie fiber, 8-11 parts of PTT short fiber, 5-7 parts of soybean fiber, 2.3-4.7 parts of milk protein fiber, 0.4-0.8 parts of tea polyphenol, 1.2-3.2 parts of plastic starch, 0.3-0.6 parts of sodium pyrophosphate, 1.2-2.4 parts of cocounut oil essence, 100-110 parts of 1-butyl-3-methylimidazolium dibutyl phosphate, 110-120 parts of 1-ethyl-3-methylimidazolium diethylphosphate, 1-2 parts of frankincense, 0.5-0.9 parts of sediment of human urine, 0.6-0.8 part of flos lonicerae, 2-4 parts of an auxiliary agent, and proper amount of water. By adding ramie fiber, the silk composite fiber has functions of resisting bacteria, inhibiting bacteria, eliminating and adsorbing odor, absorbing moisture and breathing, and the like, and by adding tea polyphenol, the improved silk composite fiber also has effects of resisting radiation, being smooth and light, keeping warm and resisting static electricity.

Description

Silk composite fibre that a kind of moisture absorption is ventilative and preparation method thereof

 

Technical field

The present invention relates to nonwoven material technical field, be specifically related to ventilative silk composite fibre of a kind of moisture absorption and preparation method thereof.

Background technology

Silk is matured silkworm concretionary continuous fiber of secreted silk liquid while cocooing, also claiming natural silk, is the lightest the thinnest the most soft natural fabric of occurring in nature, mainly animal protein, consists of, be rich in 18 kinds of necessary amino acid of human body, can promote Skin Cell vigor, anti-vascular sclerosis, long-term use can anti-skin senescence, some skin disease is had to special antipruritic effect, to arthritis, scapulohumeral periarthritis, asthma has certain health-care function.Have " human body the second skin ", " fiber queen's " good reputation.Because silk light weight is and elongated, fabric sheen is good, comfortable and easy to wear, and feel is smooth plentiful, poor heat conductivity, and moisture absorption is ventilative, has determined the health care that silk is good, is widely used in industry, beauty treatment and medicine and other fields.

In prior art, use natural silk to have many defects: one, use cost is too high; Two, because of the humidity of environment, make moist, preserve the improper raw mite that easily goes mouldy; Three, intensity is poor, and conglomeration reduces warmth retention property, affects attractive in appearance; Four, frequent static electrification, makes troubles to people etc.So develop a kind of existing environmental protection, health care, the healthy warmth retention property that is conducive to again people is strong, high strength, fire-retardant, antibacterial, laundry-resistant silk composite fibre can solve the deficiencies in the prior art smoothly.

Summary of the invention

Object of the present invention is just to provide ventilative silk composite fibre of a kind of moisture absorption and preparation method thereof, to overcome the deficiencies in the prior art.

The object of the present invention is achieved like this:

The silk composite fibre that a kind of moisture absorption is ventilative, it is characterized in that, raw material by following weight portion is made: silk 16-19, camel hair 13-15, coral suede 7-9, ramee 10-12, PTT staple fibre 8-11, fibre and soya 5-7, milk protein fiber 2.3-4.7, Tea Polyphenols 0.4-0.8, plasticity starch 1.2-3.2, sodium pyrophosphate 0.3-0.6, cocounut oil elite 1.2-2.4, 1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110, 1-ethyl-3-methylimidazole diethyl phosphate 110-120, frankincense 1-2, calamitas urinae hominis 0.5-0.9, honeysuckle 0.6-0.8, auxiliary agent 2-4, suitable quantity of water.

Described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling makes the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.

The preparation method of the silk composite fibre that described a kind of moisture absorption is ventilative, is characterized in that comprising the following steps:

(1) by frankincense, calamitas urinae hominis, honeysuckle boiling 4-6 hour, filter, in filtrate, drop into silk, camel hair, milk protein fiber immersion 10-13 hour, evenly spray into cocounut oil elite after pulling oven dry, degreasing, ultra-fine grinding out;

(2) in Tea Polyphenols, add hot water to be stirred to dissolving, add coral suede, ramee, PTT staple fibre, plasticity starch, sodium pyrophosphate ultrasonic wave to process 30-40 minute;

(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;

(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.

The present invention has following beneficial effect: the present invention adds ramee, have the functions such as antibacterial bacteriostatic, deodorizing absorption, moisture absorption are ventilative, the silk composite fibre adding after Tea Polyphenols is improved also has radioresistance, smooth, soft, warming and anlistatig effect.

The specific embodiment

The silk composite fibre that described a kind of moisture absorption is ventilative, it is characterized in that, by the raw material of following weight portion, made: silk 17, camel hair 14, coral suede 9, ramee 10, PTT staple fibre 11, fibre and soya 5, milk protein fiber 4.5, Tea Polyphenols 0.4, plasticity starch 2.2, sodium pyrophosphate 0.5, cocounut oil elite 1.6,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100,1-ethyl-3-methylimidazole diethyl phosphate 120, frankincense 1, calamitas urinae hominis 0.6, honeysuckle 0.8, auxiliary agent 4, suitable quantity of water.

Described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.6, fatty diglycollic amide 0.7, polyvinylpyrrolidone 0.2, trihydroxy ethylamine oleate soap 1.6, acrylate and vinyl acetate emulsion 1.2, nano-calcium carbonate 2, bamboo fibre 1, SIMMONDSIA CHINENSIS SEED OIL 2, the root of purple-flowered peucedanum 4, dried orange peel 5, cordate houttuynia 3.1, its preparation method is that the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling are made to the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre to soak 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.

Preparation method comprises the following steps:

(1) by frankincense, calamitas urinae hominis, honeysuckle boiling 4-6 hour, filter, in filtrate, drop into silk, camel hair, milk protein fiber immersion 10-13 hour, evenly spray into cocounut oil elite after pulling oven dry, degreasing, ultra-fine grinding out;

(2) in Tea Polyphenols, add hot water to be stirred to dissolving, add coral suede, ramee, PTT staple fibre, plasticity starch, sodium pyrophosphate ultrasonic wave to process 30-40 minute;

(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;

(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.

The technical parameter index of the silk composite fibre that use the present invention produces is as follows:

(1) light weight, warming, gas permeability is good;

(2) finished product is all greater than 99.5% to the bacteriostasis rate of Escherichia coli, staphylococcus aureus, Candida albicans;

(3) after 20 washings, antibiotic rate still reaches 96%;

(4) thermal conductivity factor 0.048(m ℃).

Claims (2)

1. the silk composite fibre that moisture absorption is ventilative, it is characterized in that, raw material by following weight portion is made: silk 16-19, camel hair 13-15, coral suede 7-9, ramee 10-12, PTT staple fibre 8-11, fibre and soya 5-7, milk protein fiber 2.3-4.7, Tea Polyphenols 0.4-0.8, plasticity starch 1.2-3.2, sodium pyrophosphate 0.3-0.6, cocounut oil elite 1.2-2.4, 1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110, 1-ethyl-3-methylimidazole diethyl phosphate 110-120, frankincense 1-2, calamitas urinae hominis 0.5-0.9, honeysuckle 0.6-0.8, auxiliary agent 2-4, suitable quantity of water, described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling makes the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.

2. the preparation method of the ventilative silk composite fibre of a kind of moisture absorption according to claim 1, is characterized in that comprising the following steps:

(1) by frankincense, calamitas urinae hominis, honeysuckle boiling 4-6 hour, filter, in filtrate, drop into silk, camel hair, milk protein fiber immersion 10-13 hour, evenly spray into cocounut oil elite after pulling oven dry, degreasing, ultra-fine grinding out;

(2) in Tea Polyphenols, add hot water to be stirred to dissolving, add coral suede, ramee, PTT staple fibre, plasticity starch, sodium pyrophosphate ultrasonic wave to process 30-40 minute;

(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;

(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.