CN104213244A - Warm-keeping air-permeable silk composite fiber and preparation method thereof - Google Patents

Abstract

Disclosed warm-keeping air-permeable silk composite fiber is characterized by being prepared from the following raw materials in parts by weight: 15-20 parts of mulberry silk, 11-13 parts of rex rabbit hair, 5-7 parts of polypropylene fiber, 7-9 parts of soybean protein fiber, 6-8 parts of space cotton, 9-11 parts of silk floss, 4-7 parts of coffee carbon fiber, 0.2-0.4 parts of hemin, 1.2-3.2 parts of palm oil, 0.4-0.7 parts of alumina silicate, 100-110 parts of 1-butyl-3-methylimidazolium dibutyl phosphate, 105-110 parts of 1-ethyl-3-methylimidazolium diethylphosphate, 1-3 parts of spica prunellae, 2-4 parts of folium artemisiae argyi, 3-6 parts of an auxiliary agent, and proper amount of water. Coffee carbon fiber is subjected to modification processing and then is added into raw materials, and the prepared silk composite fiber has the effects of storing heat, keeping warm, making air through, retaining moisture, emitting negative ions, resisting ultraviolet and the like. A negative-oxygen-ion silk quilt prepared from the silk composite fiber is capable of adjusting the body state of a user in sleep to an optimum state, enabling the user to rapidly enter a deep sleep state, improving the self immunity of the user and realizing the efficacy of prolonging life span.

Description

Silk composite fibre of a kind of heat-insulation breathable and preparation method thereof

 

Technical field

The present invention relates to nonwoven material technical field, be specifically related to silk composite fibre of a kind of heat-insulation breathable and preparation method thereof.

Background technology

Silk is matured silkworm concretionary continuous fiber of secreted silk liquid while cocooing, also claiming natural silk, is the lightest the thinnest the most soft natural fabric of occurring in nature, mainly animal protein, consists of, be rich in 18 kinds of necessary amino acid of human body, can promote Skin Cell vigor, anti-vascular sclerosis, long-term use can anti-skin senescence, some skin disease is had to special antipruritic effect, to arthritis, scapulohumeral periarthritis, asthma has certain health-care function.Have " human body the second skin ", " fiber queen's " good reputation.Because silk light weight is and elongated, fabric sheen is good, comfortable and easy to wear, and feel is smooth plentiful, poor heat conductivity, and moisture absorption is ventilative, has determined the health care that silk is good, is widely used in industry, beauty treatment and medicine and other fields.

In prior art, use natural silk to have many defects: one, use cost is too high; Two, because of the humidity of environment, make moist, preserve the improper raw mite that easily goes mouldy; Three, intensity is poor, and conglomeration reduces warmth retention property, affects attractive in appearance; Four, frequent static electrification, makes troubles to people etc.So develop a kind of existing environmental protection, health care, the healthy warmth retention property that is conducive to again people is strong, high strength, fire-retardant, antibacterial, laundry-resistant silk composite fibre can solve the deficiencies in the prior art smoothly.

Summary of the invention

Object of the present invention is just to provide silk composite fibre of a kind of heat-insulation breathable and preparation method thereof, to overcome the deficiencies in the prior art.

The object of the present invention is achieved like this:

A kind of silk composite fibre of heat-insulation breathable, it is characterized in that, by the raw material of following weight portion, made: mulberry silk 15-20, otter rabbit hair 11-13, polypropylene fibre 5-7, soybean fiber 7-9, space wadding 6-8, silk floss 9-11, coffee carbon fiber 4-7, PORPHYRIN IRON 0.2-0.4, palm oil 1.2-3.2, alumina silicate 0.4-0.7,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110,1-ethyl-3-methylimidazole diethyl phosphate 105-110, selfheal 1-3, Chen Ai 2-4, auxiliary agent 3-6, suitable quantity of water.

Described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling makes the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.

The preparation method of the silk composite fibre of described a kind of heat-insulation breathable, is characterized in that comprising the following steps:

(1) by PORPHYRIN IRON boiling 4-6 hour, filter, toward dropping into mulberry silk, the otter rabbit hair, polypropylene fibre in filtrate, soak 10-13 hour, add PORPHYRIN IRON grinding 15-30 minute after pulling oven dry, degreasing, ultra-fine grinding out, finally evenly spray into again palm oil;

(2) get alumina silicate and put into calcining furnace high-temperature process 30-40 minute, cooling space wadding, silk floss, the coffee carbon fiber ultrasonic wave pulverizing grinding 10-15 minute together that adds;

(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;

(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.

The present invention has following beneficial effect: the present invention will join in raw material after coffee carbon fiber modification, the silk composite fibre making has heat accumulation thermal, ventilative moisture absorption, disperses the effects such as anion and uvioresistant, the negative oxygen ion cocoon silk quilt that utilizes silk composite fibre of the present invention to make, can allow user's condition oneself in sleep be adjusted to optimum state, enter very soon deep sleep state, improve autoimmunity, reach the effect of promoting longevity.

The specific embodiment

The silk composite fibre of described a kind of heat-insulation breathable, it is characterized in that, by the raw material of following weight portion, made: mulberry silk 17, the otter rabbit hair 12, polypropylene fibre 6, soybean fiber 8, space wadding 7, silk floss 9, coffee carbon fiber 4, PORPHYRIN IRON 0.3, palm oil 2.2, alumina silicate 0.6,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100,1-ethyl-3-methylimidazole diethyl phosphate 105, selfheal 1, Chen Ai 2, auxiliary agent 3, suitable quantity of water.

Described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.6, fatty diglycollic amide 0.7, polyvinylpyrrolidone 0.2, trihydroxy ethylamine oleate soap 1.6, acrylate and vinyl acetate emulsion 1.2, nano-calcium carbonate 2, bamboo fibre 1, SIMMONDSIA CHINENSIS SEED OIL 2, the root of purple-flowered peucedanum 4, dried orange peel 5, cordate houttuynia 3.1, its preparation method is that the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling are made to the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre to soak 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.

Preparation method comprises the following steps:

(1) by PORPHYRIN IRON boiling 4-6 hour, filter, toward dropping into mulberry silk, the otter rabbit hair, polypropylene fibre in filtrate, soak 10-13 hour, add PORPHYRIN IRON grinding 15-30 minute after pulling oven dry, degreasing, ultra-fine grinding out, finally evenly spray into again palm oil;

(2) get alumina silicate and put into calcining furnace high-temperature process 30-40 minute, cooling space wadding, silk floss, the coffee carbon fiber ultrasonic wave pulverizing grinding 10-15 minute together that adds;

(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;

(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.

The technical parameter index of the silk composite fibre that use the present invention produces is as follows:

(1) light weight, warming, gas permeability is good;

(2) finished product is all greater than 99.7% to the bacteriostasis rate of Escherichia coli, staphylococcus aureus, Candida albicans;

(3) after 10 washings, antibiotic rate still reaches 97%;

(4) thermal conductivity factor 0.049(m ℃).

Claims (2)

1. the silk composite fibre of a heat-insulation breathable, it is characterized in that, by the raw material of following weight portion, made: mulberry silk 15-20, otter rabbit hair 11-13, polypropylene fibre 5-7, soybean fiber 7-9, space wadding 6-8, silk floss 9-11, coffee carbon fiber 4-7, PORPHYRIN IRON 0.2-0.4, palm oil 1.2-3.2, alumina silicate 0.4-0.7,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110,1-ethyl-3-methylimidazole diethyl phosphate 105-110, selfheal 1-3, Chen Ai 2-4, auxiliary agent 3-6, suitable quantity of water, described auxiliary agent is made by following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling makes the concentrated liquid of tradition Chinese medicine for 3-5 hour, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add again other residual componentss to be heated to 55-65 ℃ of agitation grinding 20-30 minute, obtain.

2. the preparation method of the silk composite fibre of a kind of heat-insulation breathable according to claim 1, is characterized in that comprising the following steps:

(1) by PORPHYRIN IRON boiling 4-6 hour, filter, toward dropping into mulberry silk, the otter rabbit hair, polypropylene fibre in filtrate, soak 10-13 hour, add PORPHYRIN IRON grinding 15-30 minute after pulling oven dry, degreasing, ultra-fine grinding out, finally evenly spray into again palm oil;

(2) get alumina silicate and put into calcining furnace high-temperature process 30-40 minute, cooling space wadding, silk floss, the coffee carbon fiber ultrasonic wave pulverizing grinding 10-15 minute together that adds;

(3) take in 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate input reactor and stir and evenly mix, add step (1), (2) product to grind 20-40 minute, be heated to 100-120 ℃, add again other residual components stirring reaction 50-70 minute, make spinning solution;

(4) finally the spinning solution making is carried out to spinning, coiling, boundling, stretching and get final product.