CN104213249A - Tea tree essential oil and polyvinyl chloride fiber combined silk composite fiber and preparation method thereof - Google Patents

Tea tree essential oil and polyvinyl chloride fiber combined silk composite fiber and preparation method thereof Download PDF

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Publication number
CN104213249A
CN104213249A CN201410405379.4A CN201410405379A CN104213249A CN 104213249 A CN104213249 A CN 104213249A CN 201410405379 A CN201410405379 A CN 201410405379A CN 104213249 A CN104213249 A CN 104213249A
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CN
China
Prior art keywords
parts
fiber
silk
tea tree
polyvinyl chloride
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Pending
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CN201410405379.4A
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Chinese (zh)
Inventor
徐造峰
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TONGCHENG SHUANGLONG SILK Co Ltd
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TONGCHENG SHUANGLONG SILK Co Ltd
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Priority to CN201410405379.4A priority Critical patent/CN104213249A/en
Publication of CN104213249A publication Critical patent/CN104213249A/en
Pending legal-status Critical Current

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Abstract

Disclosed tea tree essential oil and polyvinyl chloride fiber combined silk composite fiber is characterized by being prepared from the following raw materials in parts by weight: 17-23 parts of eria silk, 8-12 parts of long staple, 9-12 parts of spun silk, 7-10 parts of polyvinyl chloride fiber, 6-8 parts of fluorosilicone rubber fiber, 10-13 parts of cannabis sativa fiber, 1.2-2.5 parts of tea tree essential oil, 0.5-0.9 parts of polyoxyethylene hydrogenated castor oil, 0.3-0.6 parts of alum, 4-6 parts of paper pulp, 100-110 parts of 1-butyl-3-methylimidazolium dibutyl phosphate, 110-120 parts of 1-ethyl-3-methylimidazolium diethylphosphate, 2-4 parts of cassia seed, 1-3 parts of semen plantaginis, 2-5 parts of an auxiliary agent, and proper amount of water. The silk composite fiber is prepared by combining eria silk, cannabis sativa fiber, polyvinyl chloride fiber, tea tree essential oil and other effective compositions, the silk composite fiber has extremely good bacteria resistance and inhibiting property and superstrong adsorption capacity, has the effects of degrading peculiar smell and eliminating odor, makes up the disadvantages that natural silk easily generates bacteria and is bad in air permeability and easy to harden and the like. Additionally, the added tea tree essential oil has the efficacy of killing bacteria, diminishing inflammation, astringing pores, treating cold, cough, rhinitis, asthma and the like, and enabling a user to keep a cool head and recover vitality and resist depression. The prepared silk composite fiber is excellent in practicality and is favored by consumers.

Description

Silk composite fiber of a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound and preparation method thereof
 
Technical field
The present invention relates to nonwoven material technical field, be specifically related to silk composite fiber of a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound and preparation method thereof.
Background technology
Silk is matured silkworm secreted silk liquid concretionary continuous fiber when cocooing, also claim natural silk, be the lightest the thinnest the most soft natural fabric of occurring in nature, form primarily of animal protein, be rich in 18 kinds of necessary amino acid of human body, can promote Skin Cell vigor, anti-vascular sclerosis, Long-Time Service can anti-skin senescence, special antipruritic effect is had to some skin disease, to arthritis, scapulohumeral periarthritis, asthma has certain health-care function.Have the good reputation of " human body second skin ", " fiber queen ".Elongated due to silk light weight, fabric sheen is good, comfortable and easy to wear, and feel is smooth plentiful, poor heat conductivity, and moisture absorption is breathed freely, and determines the health care that silk is good, is widely used in industry, beauty treatment and medicine and other fields.
Natural silk is used to there is many defects in prior art: one, use cost is too high; Two, make moist because of the humidity of environment, preserve the improper raw mite that easily goes mouldy; Three, intensity is poor, conglomeration, reduces warmth retention property, affects attractive in appearance; Four, frequent static electrification, brings inconvenience etc.So develop a kind of existing environmental protection, health care, the warmth retention property being conducive to again the health of people is strong, high strength, fire-retardant, antibacterial, laundry-resistant silk composite fiber can solve the deficiencies in the prior art smoothly.
Summary of the invention
Object of the present invention is just to provide silk composite fiber of a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
The silk composite fiber of a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound, it is characterized in that, be made up of the raw material of following weight portion: ricinus silk 17-23, long wool hair 8-12, spun silk 9-12, polyvinyl chloride fibre fiber 7-10, fluorosioloxane rubber fiber 6-8, hemp 10-13, tea tree ethereal oil 1.2-2.5, rilanit special polyoxyethylene ether 0.5-0.9, alum 0.3-0.6, paper pulp 4-6,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110,1-ethyl-3-methylimidazole diethyl phosphate 110-120, cassia seed 2-4, plantain seed 1-3, auxiliary agent 2-5, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, nano-calcium carbonate is added in filtrate, bamboo fibre soaks 10-12 hour, add other residual componentss again and be heated to 55-65 DEG C of agitation grinding 20-30 minute, obtain.
The preparation method of the silk composite fiber of described a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound, is characterized in that comprising the following steps:
(1) by cassia seed, plantain seed, paper pulp boiling 1-2 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to totally adding alum grinding 20-30 minute;
(2) ricinus silk, long wool hair, spun silk, polyvinyl chloride fibre fiber are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray tea tree ethereal oil;
(3) take 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate drops in reactor and stirs and evenly mixs, add step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute again, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: the present invention by the active ingredients such as ricinus silk, hemp, polyvinyl chloride fibre fiber, tea tree ethereal oil in addition compound make, hemp is soft, good toughness, and there is good bacteria resistance and superpower absorption affinity, there is the effect of decomposing peculiar smell and smelly eliminating, make up the easy breed bacteria of natural silk, poor air permeability, easily the shortcoming such as to harden; Tea tree ethereal oil has the effect such as bactericidal antiphlogistic, convergence pore, treatment cold, cough, rhinitis, asthma, and clear the head, rejuvenate, anti-dejected, the silk composite fiber practicality utilizing the present invention to obtain is good, extremely consumers.
Detailed description of the invention
The silk composite fiber of described a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound, it is characterized in that, be made up of the raw material of following weight portion: ricinus silk 19, long wool hair 8, spun silk 9, polyvinyl chloride fibre fiber 8, fluorosioloxane rubber fiber 7, hemp 10, tea tree ethereal oil 1.8, rilanit special polyoxyethylene ether 0.6, alum 0.3, paper pulp 4,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100,1-ethyl-3-methylimidazole diethyl phosphate 110, cassia seed 2, plantain seed 3, auxiliary agent 4, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.6, fatty diglycollic amide 0.7, polyvinylpyrrolidone 0.2, trihydroxy ethylamine oleate soap 1.6, acrylate and vinyl acetate emulsion 1.2, nano-calcium carbonate 2, bamboo fibre 1, SIMMONDSIA CHINENSIS SEED OIL 2, the root of purple-flowered peucedanum 4, dried orange peel 5, cordate houttuynia 3.1, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add nano-calcium carbonate, bamboo fibre soaks 10-12 hour, add other residual componentss again and be heated to 55-65 DEG C of agitation grinding 20-30 minute, to obtain final product.
Preparation method comprises the following steps:
(1) by cassia seed, plantain seed, paper pulp boiling 1-2 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to totally adding alum grinding 20-30 minute;
(2) ricinus silk, long wool hair, spun silk, polyvinyl chloride fibre fiber are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray tea tree ethereal oil;
(3) take 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate drops in reactor and stirs and evenly mixs, add step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute again, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The technical parameter index of the silk composite fiber using the present invention to produce is as follows:
(1) light weight, warming, gas permeability is good, water-fastness, flame retardant effect is excellent;
(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99.4%;
(3) after 20 washings, antibiotic rate still reaches 95.8%;
(4) thermal conductivity factor 0.047(m DEG C).

Claims (2)

1. the silk composite fiber of tea tree ethereal oil/polyvinyl chloride fibre fiber compound, it is characterized in that, be made up of the raw material of following weight portion: ricinus silk 17-23, long wool hair 8-12, spun silk 9-12, polyvinyl chloride fibre fiber 7-10, fluorosioloxane rubber fiber 6-8, hemp 10-13, tea tree ethereal oil 1.2-2.5, rilanit special polyoxyethylene ether 0.5-0.9, alum 0.3-0.6, paper pulp 4-6,1-butyl-3-methylimidazole dibutylphosphoric acid ester 100-110,1-ethyl-3-methylimidazole diethyl phosphate 110-120, cassia seed 2-4, plantain seed 1-3, auxiliary agent 2-5, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: Seconary Alkane Sulphonate Sodium 0.4-0.7, fatty diglycollic amide 0.5-0.8, polyvinylpyrrolidone 0.1-0.3, trihydroxy ethylamine oleate soap 1.1-2.1, acrylate and vinyl acetate emulsion 0.8-1.3, nano-calcium carbonate 2-3, bamboo fibre 1-3, SIMMONDSIA CHINENSIS SEED OIL 2-4, root of purple-flowered peucedanum 3-4, dried orange peel 2-5, cordate houttuynia 1.2-3.2, its preparation method is by the root of purple-flowered peucedanum, dried orange peel, cordate houttuynia boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, nano-calcium carbonate is added in filtrate, bamboo fibre soaks 10-12 hour, add other residual componentss again and be heated to 55-65 DEG C of agitation grinding 20-30 minute, obtain.
2. the preparation method of the silk composite fiber of a kind of tea tree ethereal oil/polyvinyl chloride fibre fiber compound according to claim 1, is characterized in that comprising the following steps:
(1) by cassia seed, plantain seed, paper pulp boiling 1-2 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to totally adding alum grinding 20-30 minute;
(2) ricinus silk, long wool hair, spun silk, polyvinyl chloride fibre fiber are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray tea tree ethereal oil;
(3) take 1-butyl-3-methylimidazole dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate drops in reactor and stirs and evenly mixs, add step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute again, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
CN201410405379.4A 2014-08-18 2014-08-18 Tea tree essential oil and polyvinyl chloride fiber combined silk composite fiber and preparation method thereof Pending CN104213249A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106835316A (en) * 2017-04-01 2017-06-13 百事基材料(青岛)股份有限公司 A kind of cellulose fibre with itching-relieving action and preparation method thereof
CN107815773A (en) * 2017-09-30 2018-03-20 湖州东凯纺织有限公司 Anti-bacterial fibre cloth and preparation method thereof

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CN102586942A (en) * 2012-03-18 2012-07-18 山东省花生研究所 Method for preparing peanut protein composite fiber by using ionic liquid
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CN103710775A (en) * 2013-12-18 2014-04-09 中国科学院过程工程研究所 Preparation method of ionic liquid keratin spinning solutions
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CN102400238A (en) * 2011-09-01 2012-04-04 丁一 Element-negative-ion-releasing sterilizing mite-preventing electromagnetic-wave-preventing fire-retarding nano-grade fabric used in vehicles
CN102586942A (en) * 2012-03-18 2012-07-18 山东省花生研究所 Method for preparing peanut protein composite fiber by using ionic liquid
CN103668547A (en) * 2012-09-22 2014-03-26 青岛道合生物科技有限公司 Mixed-fiber antibacterial towel
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Cited By (2)

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Publication number Priority date Publication date Assignee Title
CN106835316A (en) * 2017-04-01 2017-06-13 百事基材料(青岛)股份有限公司 A kind of cellulose fibre with itching-relieving action and preparation method thereof
CN107815773A (en) * 2017-09-30 2018-03-20 湖州东凯纺织有限公司 Anti-bacterial fibre cloth and preparation method thereof

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