CN105926074A - Warming light eider down composite fiber and manufacturing method thereof - Google Patents
Warming light eider down composite fiber and manufacturing method thereof Download PDFInfo
- Publication number
- CN105926074A CN105926074A CN201610274170.8A CN201610274170A CN105926074A CN 105926074 A CN105926074 A CN 105926074A CN 201610274170 A CN201610274170 A CN 201610274170A CN 105926074 A CN105926074 A CN 105926074A
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- China
- Prior art keywords
- eider down
- hour
- powder
- warming
- down composite
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H1/00—Macromolecular products derived from proteins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/06—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyolefin as constituent
Abstract
The invention discloses a warming light eider down composite fiber. Soybean protein powder is modified and then is added into raw materials so that the warming light eider down composite fiber contains soybean protein fiber components and has fiber bonding effects. Attapulgite, polypropylene fibers and Japanese banana leaves are modified and then are added into the raw materials so that the warming light eider down composite fiber is natural and environmentally friendly and has a low cost. The warming light eider down composite fiber has the advantages of light weight, warming, antibiosis, mildew inhibition and washing resistance. A down jacket prepared from the warming light eider down composite fibers does not produce agglomeration and eider down leakage is effectively reduced.
Description
Technical field
The present invention relates to nonwoven material technical field, be specifically related to eider down composite fibre of a kind of warming lightweight and preparation method thereof.
Background technology
Eider down is the long abdominal part in geese and ducks, becomes the fine hair of Flos Phragmitis piece shape, slabbing be feather.Owing to eider down is a kind of animal protein fiber, higher than Cotton Gossypii (vegetative fiber element) heat insulating ability, and the tiny pore of ten million triangle that gathers on eider down nodular fibrous, can the convergent-divergent with temperature Change, produce temperature adjustment function, absorbable human body distributes the steam of flowing, the invasion of isolation cool ambient air, owing to eider down has the superperformance that the most warming of this uniqueness dissipates with moisture absorption, determine the health care that eider down is good, eiderdown quilt be widely used in clothing, wadded a quilt with cotton, the fields such as filler of weaving.
Prior art use natural down there is many defects: one, owing to eider down content in feather is little, the most only to account for 20-25%, so that the use cost of eider down is too high；Two, eider down makes moist because of the humidity of environment, preserves the improper raw demodicid mite that easily goes mouldy；Three, intensity is poor, washed many eider down can be made to pulverize, conglomeration, reduces warmth retention property, affects attractive in appearance；Four, the frequent static electrification of eider down in prior art, brings inconvenience；Five, existing eider down does not has the characteristics such as fire-retardant, antibacterial, water-fastness, there is the hidden danger such as safety, so the warmth retention property developing the health of a kind of existing environmental protection, health care, the most beneficially people is strong, high intensity, eider down composite fibre fire-retardant, antibacterial, laundry-resistant can solve the deficiencies in the prior art smoothly.
Summary of the invention
It is an object of the invention to provide eider down composite fibre of a kind of warming lightweight and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of eider down composite fibre of warming lightweight, it is characterized in that, be prepared by the raw materials in: duck's down superfine powder 16-19, expanded ox hair powder 20-24, nanometer drake feather powder 20-25, polypropylene fiber 13-16, glycerol 3-5, attapulgite 4-6, Folium Musae 17-20, Pericarpium Citri Reticulatae 1-3, Rhizoma Pinelliae 2-4, sulfur 0.01-0.03, titanium dioxide 0.1-0.2,1-butyl-3-Methylimidazole. dibutylphosphoric acid ester 110-130,1-ethyl-3-methylimidazole diethyl phosphate 120-140, modified soy-bean protein powder 2-4, suitable quantity of water；Described modified soy-bean protein powder its preparation method is: by ground for the soybean protein powder of 100 weight portions 100 eye mesh screens; spray concentration is the hydrochloric acid solution stirring and evenly mixing of 1-2mol/L; continuous magnetic agitation 2-3 hour in 60-80 DEG C of water bath with thermostatic control; washing is to neutral vacuum drying; add ethylenediaminetetraacetic acid dianhydride ultrasonic disperse 1-3 hour in 55-75 DEG C of water-bath of 8-10 weight portion, dry to obtain acylation modification soybean protein powder.
The preparation method of the eider down composite fibre of described a kind of warming lightweight, it is characterised in that comprise the following steps:
(1) by Pericarpium Citri Reticulatae, Rhizoma Pinelliae boiling 1-2 hour, add Folium Musae to soak 8-10 hour, filter, take filtering residue and dry pulverizing, the 10% sulphuric acid heated and stirred adding 20 times of quality of filter residue powder in mass ratio is reacted 1-2 hour, and the sodium hydroxide heated and stirred adding 2 times of quality of filter residue powder is reacted 1-2 hour, filters, wash to totally with clear water, dry and spray vaporific glycerol；
(2) attapulgite is put in retort and calcine 2-3 hour at 540-650 DEG C, take out, add titanium dioxide and be ground to 200-300 mesh, the most uniformly spray to polypropylene fiber surface；
(3) weigh 1-butyl-3-Methylimidazole. dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate puts into stirring and evenly mixing in reactor, addition sulfur, step (1), (2) product grind 20-40 minute, it is heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, prepare spinning solution；
(4) finally prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: the present invention adds in raw material by modified for soybean protein powder, both big bean or pea azelon composition had been contained, play again the cementation between fiber, join in raw material by modified to attapulgite, polypropylene fiber, Folium Musae etc., natural environmental protection, low cost, and the eider down composite fibre prepared to have light weight warming, antibacterial fungistatic, the advantage such as water-fastness, the down jackets using this product to make do not have the group's of beating phenomenon, and effectively reduce and bore floss phenomenon.
Detailed description of the invention
The eider down composite fibre of described a kind of warming lightweight, it is characterized in that, be prepared by the raw materials in: duck's down superfine powder 17, expanded ox hair powder 23, nanometer drake feather powder 21, polypropylene fiber 13, glycerol 3, attapulgite 6, Folium Musae 17, Pericarpium Citri Reticulatae 1, the Rhizoma Pinelliae 4, sulfur 0.01, titanium dioxide 0.2,1-butyl-3-Methylimidazole. dibutylphosphoric acid ester 110,1-ethyl-3-methylimidazole diethyl phosphate 120, modified soy-bean protein powder 4, suitable quantity of water；Described modified soy-bean protein powder its preparation method is: by ground for the soybean protein powder of 100 weight portions 100 eye mesh screens; spray concentration is the hydrochloric acid solution stirring and evenly mixing of 1-2mol/L; continuous magnetic agitation 2-3 hour in 60-80 DEG C of water bath with thermostatic control; washing is to neutral vacuum drying; add ethylenediaminetetraacetic acid dianhydride ultrasonic disperse 1-3 hour in 55-75 DEG C of water-bath of 8-10 weight portion, dry to obtain acylation modification soybean protein powder.
Manufacture method comprises the following steps:
(1) by Pericarpium Citri Reticulatae, Rhizoma Pinelliae boiling 1-2 hour, add Folium Musae to soak 8-10 hour, filter, take filtering residue and dry pulverizing, the 10% sulphuric acid heated and stirred adding 20 times of quality of filter residue powder in mass ratio is reacted 1-2 hour, and the sodium hydroxide heated and stirred adding 2 times of quality of filter residue powder is reacted 1-2 hour, filters, wash to totally with clear water, dry and spray vaporific glycerol；
(2) attapulgite is put in retort and calcine 2-3 hour at 540-650 DEG C, take out, add titanium dioxide and be ground to 200-300 mesh, the most uniformly spray to polypropylene fiber surface；
(3) weigh 1-butyl-3-Methylimidazole. dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate puts into stirring and evenly mixing in reactor, addition sulfur, step (1), (2) product grind 20-40 minute, it is heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, prepare spinning solution；
(4) finally prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
The technical parameter index using the eider down composite fibre of present invention production is as follows:
(1) light weight, warming, environmental protection；
(2) finished product is all higher than 99% to escherichia coli, staphylococcus aureus, the bacteriostasis rate of Candida albicans；
(3) after 20 times are washed, antibiotic rate still reaches 96%.
Claims (2)
1. the eider down composite fibre of a warming lightweight, it is characterized in that, be prepared by the raw materials in: duck's down superfine powder 16-19, expanded ox hair powder 20-24, nanometer drake feather powder 20-25, polypropylene fiber 13-16, glycerol 3-5, attapulgite 4-6, Folium Musae 17-20, Pericarpium Citri Reticulatae 1-3, Rhizoma Pinelliae 2-4, sulfur 0.01-0.03, titanium dioxide 0.1-0.2,1-butyl-3-Methylimidazole. dibutylphosphoric acid ester 110-130,1-ethyl-3-methylimidazole diethyl phosphate 120-140, modified soy-bean protein powder 2-4, suitable quantity of water；Described modified soy-bean protein powder its preparation method is: by ground for the soybean protein powder of 100 weight portions 100 eye mesh screens; spray concentration is the hydrochloric acid solution stirring and evenly mixing of 1-2mol/L; continuous magnetic agitation 2-3 hour in 60-80 DEG C of water bath with thermostatic control; washing is to neutral vacuum drying; add ethylenediaminetetraacetic acid dianhydride ultrasonic disperse 1-3 hour in 55-75 DEG C of water-bath of 8-10 weight portion, dry to obtain acylation modification soybean protein powder.
The manufacture method of the eider down composite fibre of a kind of warming lightweight the most according to claim 1, it is characterised in that comprise the following steps:
(1) by Pericarpium Citri Reticulatae, Rhizoma Pinelliae boiling 1-2 hour, add Folium Musae to soak 8-10 hour, filter, take filtering residue and dry pulverizing, the 10% sulphuric acid heated and stirred adding 20 times of quality of filter residue powder in mass ratio is reacted 1-2 hour, and the sodium hydroxide heated and stirred adding 2 times of quality of filter residue powder is reacted 1-2 hour, filters, wash to totally with clear water, dry and spray vaporific glycerol；
(2) attapulgite is put in retort and calcine 2-3 hour at 540-650 DEG C, take out, add titanium dioxide and be ground to 200-300 mesh, the most uniformly spray to polypropylene fiber surface；
(3) weigh 1-butyl-3-Methylimidazole. dibutylphosphoric acid ester, 1-ethyl-3-methylimidazole diethyl phosphate puts into stirring and evenly mixing in reactor, addition sulfur, step (1), (2) product grind 20-40 minute, it is heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, prepare spinning solution；
(4) finally prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610274170.8A CN105926074A (en) | 2016-04-28 | 2016-04-28 | Warming light eider down composite fiber and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610274170.8A CN105926074A (en) | 2016-04-28 | 2016-04-28 | Warming light eider down composite fiber and manufacturing method thereof |
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| CN105926074A true CN105926074A (en) | 2016-09-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610274170.8A Pending CN105926074A (en) | 2016-04-28 | 2016-04-28 | Warming light eider down composite fiber and manufacturing method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111453690A (en) * | 2020-04-26 | 2020-07-28 | 安徽华英新塘羽绒有限公司 | Waterproof velvet and preparation method thereof |
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| CN104195664A (en) * | 2014-08-30 | 2014-12-10 | 安徽一隆羽绒有限公司 | Down feather composite fiber modified by polypropylene fiber and preparation method of down feather composite fiber |
| CN104278355A (en) * | 2014-09-09 | 2015-01-14 | 安徽省含山县富强羽绒制品有限公司 | Washable light down feather composite fiber and preparation method thereof |
| CN105088404A (en) * | 2015-07-31 | 2015-11-25 | 安徽天鹅家纺股份有限公司 | Washable wrinkle-proof compound silk floss material |
| CN105088396A (en) * | 2015-07-31 | 2015-11-25 | 安徽天鹅家纺股份有限公司 | Soft and comfortable novel compound polypropylene fiber fabric |
-
2016
- 2016-04-28 CN CN201610274170.8A patent/CN105926074A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104195664A (en) * | 2014-08-30 | 2014-12-10 | 安徽一隆羽绒有限公司 | Down feather composite fiber modified by polypropylene fiber and preparation method of down feather composite fiber |
| CN104278355A (en) * | 2014-09-09 | 2015-01-14 | 安徽省含山县富强羽绒制品有限公司 | Washable light down feather composite fiber and preparation method thereof |
| CN105088404A (en) * | 2015-07-31 | 2015-11-25 | 安徽天鹅家纺股份有限公司 | Washable wrinkle-proof compound silk floss material |
| CN105088396A (en) * | 2015-07-31 | 2015-11-25 | 安徽天鹅家纺股份有限公司 | Soft and comfortable novel compound polypropylene fiber fabric |
Non-Patent Citations (1)
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| 刘琼等: "新型pH敏感的大豆蛋白水凝胶的研制", 《西北工业大学学报》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111453690A (en) * | 2020-04-26 | 2020-07-28 | 安徽华英新塘羽绒有限公司 | Waterproof velvet and preparation method thereof |
| CN111453690B (en) * | 2020-04-26 | 2021-10-26 | 安徽华英新塘羽绒有限公司 | Waterproof velvet and preparation method thereof |
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Application publication date: 20160907 |