CN105970348A - Antibiotic and healthy composite down wadding and preparation method thereof - Google Patents

Antibiotic and healthy composite down wadding and preparation method thereof Download PDF

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Publication number
CN105970348A
CN105970348A CN201610450783.2A CN201610450783A CN105970348A CN 105970348 A CN105970348 A CN 105970348A CN 201610450783 A CN201610450783 A CN 201610450783A CN 105970348 A CN105970348 A CN 105970348A
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China
Prior art keywords
parts
oil
hour
antibiotic
chitin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610450783.2A
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Chinese (zh)
Inventor
张延新
郑玲
胡世安
高大云
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ANHUI LION GOOSE PRODUCT Co Ltd
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ANHUI LION GOOSE PRODUCT Co Ltd
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Priority to CN201610450783.2A priority Critical patent/CN105970348A/en
Publication of CN105970348A publication Critical patent/CN105970348A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D01F1/103—Agents inhibiting growth of microorganisms
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M19/00—Treatment of feathers

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses antibiotic and healthy composite down wadding and a preparation method thereof. The antibiotic and healthy composite down wadding is prepared from the following raw materials in parts by weight: 17-23 parts of white duck down, 5-8 parts of bamboo pulp fibers, 6-9 parts of polyester fibers, 4-7 parts of chitin, 0.3-0.7 part of tea saponin, 4.1-5.8 parts of a carbon nano-tube, 2-4 parts of vermiculite, 0.4-0.7 part of zinc nitrate, 3.2-4.6 parts of methyltrimethoxy silane, 16-20 parts of chlorinated 1-butyl-3-methylimidazolium, 0.05-0.1 part of pomegranate seed oil, 0.05-0.1 part of thyme oil, 0.02-0.04 part of garlic oil, 0.02-0.04 part of ginger oil, 0.02-0.04 part of sodium cocoyl glycinate and 0.1-0.2 part of isopropyl myristate. The composite down wadding is good in heat retention property, strength, flexibility and weather resistance, and moderate in compressibility, air permeability and moisture permeability, also has the efficacies of bacterium resistance, disinfection and ageing resistance and is good in processability and using performance.

Description

A kind of antibiotic health care eider down compound wadding material and preparation method thereof
Technical field
The invention belongs to Eider down processing technical field, be specifically related to a kind of antibiotic health care eider down compound wadding material and Preparation method.
Background technology
Along with the raising of people's living standard, daily textile be there has also been more demand, be greatly promoted Heat insulating material formed development.People have been not limited solely to warming psychological need to heat insulating material formed requirement, And the most attractive in appearance, comfortable, health care etc., and towards higher standard evolution.
Eider down, feather material source in birds, are have premium properties natural heat insulating material formed.Eider down has Gently, soft, fluffy, sucting wet air permeability is good, the advantage of high insulating effect, is usually used in clothing and bedding, is subject to Welcome to consumers in general.But down feather material is expensive, resource-constrained, processing characteristics is poor, and Down products is the most clumsy too fat to move, it is impossible to meet the needs that quality is frivolous.Exploitation novel heat-preserving material, is protecting Improve the wearability of down products on the premise of holding its original premium properties, make product to frivolous, attractive in appearance, Direction durable, multi-functional is developed, and the exploitation application for down products opens rational approach.
Summary of the invention
It is an object of the invention to provide a kind of antibiotic health care eider down compound wadding material and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of antibiotic health care eider down compound wadding material, is prepared by the raw materials in: white duck down 17-23 part, Bamboo pulp fiber 5-8 part, polyster fibre 6-9 part, chitin 4-7 part, tea saponin 0.3-0.7 part, carbon are received Mitron 4.1-5.8 part, Vermiculitum 2-4 part, zinc nitrate 0.4-0.7 part, MTMS 3.2-4.6 Part, chlorination-1-butyl-3-Methylimidazole. 16-20 part, granada seed oil 0.05-0.1 part, thyme oil 0.05-0.1 part, Oleum Bulbus Allii 0.02-0.04 part, oil of Rhizoma Zingiberis Recens 0.02-0.04 part, sodium cocoyl glycinate 0.02-0.04 part, isopropyl myristate 0.1-0.2 part.
As preferably, the compound wadding of described a kind of antibiotic health care eider down is expected, is prepared by the raw materials in: White duck down 20 parts, bamboo pulp fiber 6 parts, polyster fibre 7 parts, chitin 5 parts, tea saponin 0.5 part, CNT 5 parts, Vermiculitum 3 parts, zinc nitrate 0.5 part, MTMS 3.5 parts, chlorination-1- Butyl-3-Methylimidazole. 18 parts, granada seed oil 0.1 part, thyme oil 0.1 part, Oleum Bulbus Allii 0.04 part, Oil of Rhizoma Zingiberis Recens 0.04 part, sodium cocoyl glycinate 0.04 part, isopropyl myristate 0.2 part.
Described a kind of antibiotic health care eider down compound wadding material, its preparation method comprises the following steps:
(1) Vermiculitum is processed 1-2 hour in 700-800 DEG C of high-temperature calcination, be cooled to room temperature and crush, add Zinc nitrate aqueous solution soaks 5-8 hour, adds tea saponin extra-fine grinding 2-4 hour, is spray-dried；
(2) by granada seed oil, thyme oil, Oleum Bulbus Allii and oil of Rhizoma Zingiberis Recens mix homogeneously, then it is sprayed on vermiculite power Middle stirring at normal temperature 0.5-1h, obtains active powder；
(3) bamboo pulp fiber, polyster fibre being put in saline and soaked 5-8 hour, drying is pulverized, Add CNT, MTMS puts into 50-70 DEG C of stirred in water bath 30-50 minute, dries Dry；
(4) by chitin, chlorination-1-butyl-3-Methylimidazole. stirring and evenly mixing, step (2), (3) are added Material grinds 20-40 minute, is heated to 80-90 DEG C, keeps temperature to stir 1-3 hour；
(5) sodium cocoyl glycinate and isopropyl myristate are passed through spray after suitable quantity of water mixing and stirring Mist method is sprayed on duck's down, 60-80 DEG C of insulation 0.5-1h, puts into step (4) material after being pulverized by white duck down In, it is warming up to 110-120 DEG C, adds other residual components stirring reaction 50-70 minute, prepare spinning former Liquid；
(6) prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
Beneficial effects of the present invention: the eider down of the present invention is combined wadding and expects existing good warmth retention property, also has good Intensity, pliability and weatherability, compressibility, breathable moisture permeability are moderate, have antibacterial sterilization, anti-simultaneously Aging effect, processing characteristics and serviceability are good.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
A kind of antibiotic health care eider down compound wadding material, is prepared by the raw materials in: white duck down 17-23 part, Bamboo pulp fiber 5-8 part, polyster fibre 6-9 part, chitin 4-7 part, tea saponin 0.3-0.7 part, carbon are received Mitron 4.1-5.8 part, Vermiculitum 2-4 part, zinc nitrate 0.4-0.7 part, MTMS 3.2-4.6 Part, chlorination-1-butyl-3-Methylimidazole. 16-20 part, granada seed oil 0.05-0.1 part, thyme oil 0.05-0.1 part, Oleum Bulbus Allii 0.02-0.04 part, oil of Rhizoma Zingiberis Recens 0.02-0.04 part, sodium cocoyl glycinate 0.02-0.04 part, isopropyl myristate 0.1-0.2 part.
As preferably, the compound wadding of described a kind of antibiotic health care eider down is expected, is prepared by the raw materials in: White duck down 20 parts, bamboo pulp fiber 6 parts, polyster fibre 7 parts, chitin 5 parts, tea saponin 0.5 part, CNT 5 parts, Vermiculitum 3 parts, zinc nitrate 0.5 part, MTMS 3.5 parts, chlorination-1- Butyl-3-Methylimidazole. 18 parts, granada seed oil 0.1 part, thyme oil 0.1 part, Oleum Bulbus Allii 0.04 part, Oil of Rhizoma Zingiberis Recens 0.04 part, sodium cocoyl glycinate 0.04 part, isopropyl myristate 0.2 part.
Described a kind of antibiotic health care eider down compound wadding material, its preparation method comprises the following steps:
(1) Vermiculitum is processed 1-2 hour in 700-800 DEG C of high-temperature calcination, be cooled to room temperature and crush, add Zinc nitrate aqueous solution soaks 5-8 hour, adds tea saponin extra-fine grinding 2-4 hour, is spray-dried；
(2) by granada seed oil, thyme oil, Oleum Bulbus Allii and oil of Rhizoma Zingiberis Recens mix homogeneously, then it is sprayed on vermiculite power Middle stirring at normal temperature 0.5-1h, obtains active powder；
(3) bamboo pulp fiber, polyster fibre being put in saline and soaked 5-8 hour, drying is pulverized, Add CNT, MTMS puts into 50-70 DEG C of stirred in water bath 30-50 minute, dries Dry；
(4) by chitin, chlorination-1-butyl-3-Methylimidazole. stirring and evenly mixing, step (2), (3) are added Material grinds 20-40 minute, is heated to 80-90 DEG C, keeps temperature to stir 1-3 hour；
(5) sodium cocoyl glycinate and isopropyl myristate are passed through spray after suitable quantity of water mixing and stirring Mist method is sprayed on duck's down, 60-80 DEG C of insulation 0.5-1h, puts into step (4) material after being pulverized by white duck down In, it is warming up to 110-120 DEG C, adds other residual components stirring reaction 50-70 minute, prepare spinning former Liquid；
(6) prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
Embodiment 1
Following raw materials according is weighed: white duck down 20, bamboo pulp fiber 6, polyster fibre 7, first according to weight Shell element 5, tea saponin 0.5, CNT 5.0, Vermiculitum 3, zinc nitrate 0.5, first Base trimethoxy silane 3.5, chlorination-1-butyl-3-Methylimidazole. 18, granada seed oil 0.1, hundred In Oleum sesami 0.1, Oleum Bulbus Allii 0.04, oil of Rhizoma Zingiberis Recens 0.04, sodium cocoyl glycinate 0.04, meat Isopropyl myristate 0.2.
(1) Vermiculitum is processed 2 hours in 800 DEG C of high-temperature calcinations, be cooled to room temperature and crush, add zinc nitrate Aqueous solution soaking 8 hours, adds tea saponin extra-fine grinding 2 hours, is spray-dried；
(2) by granada seed oil, thyme oil, Oleum Bulbus Allii and oil of Rhizoma Zingiberis Recens mix homogeneously, then it is sprayed on vermiculite power Middle stirring at normal temperature 1h, obtains active powder；
(3) bamboo pulp fiber, polyster fibre being put in saline and soaked 8 hours, drying is pulverized, and adds Enter CNT, MTMS puts into 70 DEG C of stirred in water bath 50 minutes, dries；
(4) by chitin, chlorination-1-butyl-3-Methylimidazole. stirring and evenly mixing, step (2), (3) are added Material grinds 40 minutes, is heated to 80 DEG C, keeps temperature to stir 3 hours；
(5) sodium cocoyl glycinate and isopropyl myristate are passed through spray after suitable quantity of water mixing and stirring Mist method is sprayed on duck's down, 60 DEG C of insulation 1h, puts in step (4) material, heat up after being pulverized by white duck down To 110 DEG C, add other residual components stirring reaction 50 minutes, prepare spinning solution；
(6) prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
Above content is only to present configuration example and explanation, the technology people of affiliated the art Described specific embodiment is made various amendment or supplements or use similar mode to substitute, only by member Will without departing from invention structure or surmount scope defined in the claims, all should belong to the present invention's Protection domain.

Claims (3)

1. an antibiotic health care eider down compound wadding material, it is characterised in that be prepared by the raw materials in: White duck down 17-23 part, bamboo pulp fiber 5-8 part, polyster fibre 6-9 part, chitin 4-7 part, tea saponin 0.3-0.7 part, CNT 4.1-5.8 part, Vermiculitum 2-4 part, zinc nitrate 0.4-0.7 part, methyl three Methoxy silane 3.2-4.6 part, chlorination-1-butyl-3-Methylimidazole. 16-20 part, granada seed oil 0.05-0.1 Part, thyme oil 0.05-0.1 part, Oleum Bulbus Allii 0.02-0.04 part, oil of Rhizoma Zingiberis Recens 0.02-0.04 part, cocos nucifera oil Acyl Glycine sodium 0.02-0.04 part, isopropyl myristate 0.1-0.2 part.
A kind of antibiotic health care eider down the most according to claim 1 compound wadding material, it is characterised in that under by The raw material of row weight portion is made: white duck down 20 parts, bamboo pulp fiber 6 parts, polyster fibre 7 parts, chitin 5 Part, tea saponin 0.5 part, CNT 5 parts, Vermiculitum 3 parts, zinc nitrate 0.5 part, methyl trimethoxy epoxide 3.5 parts of silane, chlorination-1-butyl-3-Methylimidazole. 18 parts, granada seed oil 0.1 part, thyme oil 0.1 Part, Oleum Bulbus Allii 0.04 part, oil of Rhizoma Zingiberis Recens 0.04 part, sodium cocoyl glycinate 0.04 part, myristic acid isopropyl Ester 0.2 part.
A kind of antibiotic health care eider down the most according to claim 1 compound wadding material, it is characterised in that its system Preparation Method comprises the following steps:
(1) Vermiculitum is processed 1-2 hour in 700-800 DEG C of high-temperature calcination, be cooled to room temperature and crush, add Zinc nitrate aqueous solution soaks 5-8 hour, adds tea saponin extra-fine grinding 2-4 hour, is spray-dried；
(2) by granada seed oil, thyme oil, Oleum Bulbus Allii and oil of Rhizoma Zingiberis Recens mix homogeneously, then it is sprayed on vermiculite power Middle stirring at normal temperature 0.5-1h, obtains active powder；
(3) bamboo pulp fiber, polyster fibre being put in saline and soaked 5-8 hour, drying is pulverized, Add CNT, MTMS puts into 50-70 DEG C of stirred in water bath 30-50 minute, dries Dry；
(4) by chitin, chlorination-1-butyl-3-Methylimidazole. stirring and evenly mixing, step (2), (3) are added Material grinds 20-40 minute, is heated to 80-90 DEG C, keeps temperature to stir 1-3 hour；
(5) sodium cocoyl glycinate and isopropyl myristate are passed through spray after suitable quantity of water mixing and stirring Mist method is sprayed on duck's down, 60-80 DEG C of insulation 0.5-1h, puts into step (4) material after being pulverized by white duck down In, it is warming up to 110-120 DEG C, adds other residual components stirring reaction 50-70 minute, prepare spinning former Liquid；
(6) prepared spinning solution carried out spinning, winding, boundling, stretching and get final product.
CN201610450783.2A 2016-06-17 2016-06-17 Antibiotic and healthy composite down wadding and preparation method thereof Pending CN105970348A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107934901A (en) * 2017-11-16 2018-04-20 合隆企业（深圳）有限公司 A kind of rapid-curing cutback natural feather packing material and preparation method thereof
CN109763197A (en) * 2019-02-14 2019-05-17 杭州新尚科技咨询有限公司 A kind of preparation method of environment-friendly type light color uvioresistant polyester fabric
CN109763196A (en) * 2019-02-14 2019-05-17 杭州新尚科技咨询有限公司 A kind of preparation method of the uvioresistant polyester fabric suitable for outdoor work

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Publication number Priority date Publication date Assignee Title
CN104762693A (en) * 2015-03-27 2015-07-08 安徽省含山县富强羽绒制品有限公司 Regenerated down composite fiber and manufacturing method thereof
CN104928787A (en) * 2015-06-02 2015-09-23 安徽省含山县富强羽绒制品有限公司 Ecological bacteriostatic down feather fiber with functions of moisture absorption and air permeability, and production method thereof
CN104947223A (en) * 2015-06-02 2015-09-30 安徽省含山县富强羽绒制品有限公司 Low-damage green ecological bacteriostatic down fiber and making method thereof
CN105088533A (en) * 2015-07-31 2015-11-25 安徽天鹅科技实业（集团）有限公司 Antibacterial health down composite flocculant material and preparation method
CN105239201A (en) * 2015-08-15 2016-01-13 陆思烨 Toothbrush hair having anti-bacterial and health-caring function and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104762693A (en) * 2015-03-27 2015-07-08 安徽省含山县富强羽绒制品有限公司 Regenerated down composite fiber and manufacturing method thereof
CN104928787A (en) * 2015-06-02 2015-09-23 安徽省含山县富强羽绒制品有限公司 Ecological bacteriostatic down feather fiber with functions of moisture absorption and air permeability, and production method thereof
CN104947223A (en) * 2015-06-02 2015-09-30 安徽省含山县富强羽绒制品有限公司 Low-damage green ecological bacteriostatic down fiber and making method thereof
CN105088533A (en) * 2015-07-31 2015-11-25 安徽天鹅科技实业（集团）有限公司 Antibacterial health down composite flocculant material and preparation method
CN105239201A (en) * 2015-08-15 2016-01-13 陆思烨 Toothbrush hair having anti-bacterial and health-caring function and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107934901A (en) * 2017-11-16 2018-04-20 合隆企业（深圳）有限公司 A kind of rapid-curing cutback natural feather packing material and preparation method thereof
CN107934901B (en) * 2017-11-16 2019-12-31 合隆企业（深圳）有限公司 Quick-drying down filling material and preparation method thereof
CN109763197A (en) * 2019-02-14 2019-05-17 杭州新尚科技咨询有限公司 A kind of preparation method of environment-friendly type light color uvioresistant polyester fabric
CN109763196A (en) * 2019-02-14 2019-05-17 杭州新尚科技咨询有限公司 A kind of preparation method of the uvioresistant polyester fabric suitable for outdoor work
CN109763196B (en) * 2019-02-14 2021-10-01 杭州新尚科技咨询有限公司 Preparation method of anti-ultraviolet polyester fabric suitable for outdoor operation

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