CN105113123A - Ageing-resistant down feather composite wadding and preparation method thereof - Google Patents
Ageing-resistant down feather composite wadding and preparation method thereof Download PDFInfo
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- CN105113123A CN105113123A CN201510500754.8A CN201510500754A CN105113123A CN 105113123 A CN105113123 A CN 105113123A CN 201510500754 A CN201510500754 A CN 201510500754A CN 105113123 A CN105113123 A CN 105113123A
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Abstract
The invention discloses ageing-resistant down feather composite wadding. The ageing-resistant down feather composite wadding is prepared from the following raw materials in parts by weight: 10-20 parts of duck's down, 100-150 parts of a viscose fiber stock solution, 1-2 parts of coix seeds, 1-2 parts of polygonum multiflorum, 1-2 parts of gynostemma pentaphyllum, 0.5-1 part of rhodiola, 1-2 parts of epoxidized soybean oil, 0.02-0.04 part of castor oil polyoxyethylene ether, 0.01-0.02 part of vitamin C phosphate magnesium and 1-2 part of nano montmorillonite. The ageing-resistant down feather composite wadding disclosed by the invention has good heat retention property, good strength, toughness and wear resistance, moderate compression property and air and moisture permeability, good ageing resistance, strong durability and good processing and using performance.
Description
Technical field
The present invention relates to heat insulating material formed field, be specifically related to a kind of ageing-resistant eider down compound wadding material and preparation method thereof.
Background technology
Along with the raising of people's living standard, more demand be there has also been to daily textiles, greatly facilitate heat insulating material formed development.People are not only confined to warming psychological need to heat insulating material formed requirement, and attractive in appearance, comfortable, health care etc. in addition, and towards higher standard evolution.
Eider down, feather material source, in bird, are have premium properties natural heat insulating material formed.Eider down has gently, soft, fluffy, sucting wet air permeability is good, the advantage of high insulating effect, is usually used in clothes and bedding, is subject to the welcome of consumers in general.But down feather material is expensive, resource-constrained, processing characteristics is poor, and down products is comparatively clumsy too fat to move, cannot meet the needs that quality is frivolous.Development of new is heat insulating material formed, and under the prerequisite keeping its original premium properties, improve the wearability of down products, make product to frivolous, attractive in appearance, durable, multi-functional future development, the Application and Development for down products opens rational approach.
Summary of the invention
The object of this invention is to provide a kind of ageing-resistant eider down compound wadding material, thermal property and mechanical property good, frivolous softness, comfortable durable.
The present invention is achieved by the following technical solutions:
An ageing-resistant eider down compound wadding material, it is obtained by the raw material of following weight parts:
Duck's down 10-20, viscose stoste 100-150, coix seed 1-2, fleece-flower root 1-2, gynostemma pentaphylla 1-2, rhodiola root 0.5-1, epoxidized soybean oil 1-2, castor oil polyoxyethylene ether 0.02-0.04, L-Ascorbic Acid L-O-Phosphate 0.01-0.02, nano imvite 1-2;
Wherein, viscose stoste is obtained by the raw material of following weight parts: viscose glue 100-120, Silicone acrylic emulsion 3-5, pure acrylate elastic emulsion 4-8, nano aluminium oxide 0.1-0.2, Tween-80 0.1-0.2; The preparation method of described viscose stoste be add after first Tween-80 and nano aluminium oxide being mixed in viscose glue and in 20-25 DEG C, 1000-1500r/min stirs 10-15min, add all the other raw materials again and stir 10-15min under similarity condition, to obtain final product.
Wherein, viscose glue forms alkali cellulose by native cellulose through alkalization, then generate cellulose xanthate ester with carbon disulfide effect, and be dissolved in the viscous solution obtained in sig water, solid content is 10-15%.
Viscose glue after wet spinning and a series for the treatment of process viscose.
A preparation method for ageing-resistant eider down compound wadding material, comprises the following steps:
(1) coix seed, the fleece-flower root, gynostemma pentaphylla and rhodiola root are added heating in suitable quantity of water and boil 4-6h, cooled and filtered, removing filter residue also concentrates rear and nano imvite mixing and stirring, completely dry under 70-80 DEG C of condition, obtains active powder after grinding is even;
(2) add in viscose stoste by the active powder in (1), dispersed with stirring even final vacuum deaeration removing gas, through conventional soln spinning and postprocessing working procedures, obtains composite viscose fiber;
(3) will be sprayed on eider down by spray-on process after L-Ascorbic Acid L-O-Phosphate, castor oil polyoxyethylene ether and epoxidized soybean oil and suitable quantity of water mixing and stirring, mix with the composite viscose fiber in (2) after 60-80 DEG C of insulation 0.5-1h, again through shredding, combing, one-tenth net, pinprick reinforcement, to obtain final product.
Advantage of the present invention is:
Take viscose glue as host material, the toughness of material is promoted by adding pure acrylate elastic emulsion, resilience, the weatherability of material is promoted by adding Silicone acrylic emulsion, ABRASION RESISTANCE and the intensity of material is promoted by adding nano aluminium oxide, effectively improve mechanical performance and the weatherability of composite viscose fiber, simultaneously, introduce active component and by composite viscose fiber and eider down is blended prepares composite, make the existing good warmth retention property of eider down compound wadding material obtained, also has good intensity, pliability and weatherability, compressibility, breathable moisture permeability is moderate, resistance to ag(e)ing is good, durability is strong, processing characteristics and serviceability good.
Detailed description of the invention
Non-limiting examples of the present invention is as follows:
An ageing-resistant eider down compound wadding material, is prepared from by the component raw material of following weight (kg):
Duck's down 15, viscose stoste 120, coix seed 1.5, the fleece-flower root 1.5, gynostemma pentaphylla 1.5, rhodiola root 0.8, epoxidized soybean oil 1.5, castor oil polyoxyethylene ether 0.03, L-Ascorbic Acid L-O-Phosphate 0.015, nano imvite 1.5;
Wherein, viscose stoste is obtained by the raw material of following weight parts: viscose glue 110, Silicone acrylic emulsion 4, pure acrylate elastic emulsion 6, nano aluminium oxide 0.15, Tween-80 0.15; The preparation method of described viscose stoste be add after first Tween-80 and nano aluminium oxide being mixed in viscose glue and in 25 DEG C, 1500r/min stirs 10min, then adds all the other raw materials stir 10min under similarity condition, to obtain final product.
Wherein, viscose glue forms alkali cellulose by native cellulose through alkalization, then generate cellulose xanthate ester with carbon disulfide effect, and be dissolved in the viscous solution obtained in sig water, solid content is 15%.
The preparation method of ageing-resistant eider down compound wadding material comprises the following steps:
(1) coix seed, the fleece-flower root, gynostemma pentaphylla and rhodiola root are added heating in suitable quantity of water and boil 5h, cooled and filtered, removing filter residue also concentrates rear and nano imvite mixing and stirring, completely dry under 80 DEG C of conditions, obtains active powder after grinding is even;
(2) add in viscose stoste by the active powder in (1), dispersed with stirring even final vacuum deaeration removing gas, through conventional soln spinning and postprocessing working procedures, obtains composite viscose fiber;
(3) will be sprayed on eider down by spray-on process after L-Ascorbic Acid L-O-Phosphate, castor oil polyoxyethylene ether and epoxidized soybean oil and suitable quantity of water mixing and stirring, mix with the composite viscose fiber in (2) after 80 DEG C of insulation 0.5h, again through shredding, combing, one-tenth net, pinprick reinforcement, to obtain final product.
Carry out performance test to above-mentioned obtained eider down compound wadding material, result is as follows:
Insulation rate: 91.2%, compress ional resilience index: 94.5%.
Claims (3)
1. an ageing-resistant eider down compound wadding material, it is characterized in that, it is obtained by the raw material of following weight parts:
Duck's down 10-20, viscose stoste 100-150, coix seed 1-2, fleece-flower root 1-2, gynostemma pentaphylla 1-2, rhodiola root 0.5-1, epoxidized soybean oil 1-2, castor oil polyoxyethylene ether 0.02-0.04, L-Ascorbic Acid L-O-Phosphate 0.01-0.02, nano imvite 1-2;
Described viscose stoste is obtained by the raw material of following weight parts: viscose glue 100-120, Silicone acrylic emulsion 3-5, pure acrylate elastic emulsion 4-8, nano aluminium oxide 0.1-0.2, Tween-80 0.1-0.2; The preparation method of described viscose stoste be add after first Tween-80 and nano aluminium oxide being mixed in viscose glue and in 20-25 DEG C, 1000-1500r/min stirs 10-15min, add all the other raw materials again and stir 10-15min under similarity condition, to obtain final product.
2. one according to claim 1 ageing-resistant eider down compound wadding material, it is characterized in that: described viscose glue forms alkali cellulose by native cellulose through alkalization, generate cellulose xanthate ester with carbon disulfide effect again, be dissolved in the viscous solution obtained in sig water, solid content is 10-15%.
3. the preparation method of a kind of ageing-resistant eider down compound wadding material according to claim 1, is characterized in that, comprise the following steps:
(1) coix seed, the fleece-flower root, gynostemma pentaphylla and rhodiola root are added heating in suitable quantity of water and boil 4-6h, cooled and filtered, removing filter residue also concentrates rear and nano imvite mixing and stirring, completely dry under 70-80 DEG C of condition, obtains active powder after grinding is even;
(2) add in viscose stoste by the active powder in (1), dispersed with stirring even final vacuum deaeration removing gas, through conventional soln spinning and postprocessing working procedures, obtains composite viscose fiber;
(3) will be sprayed on eider down by spray-on process after L-Ascorbic Acid L-O-Phosphate, castor oil polyoxyethylene ether and epoxidized soybean oil and suitable quantity of water mixing and stirring, mix with the composite viscose fiber in (2) after 60-80 DEG C of insulation 0.5-1h, again through shredding, combing, one-tenth net, pinprick reinforcement, to obtain final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510500754.8A CN105113123A (en) | 2015-08-14 | 2015-08-14 | Ageing-resistant down feather composite wadding and preparation method thereof |
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| CN201510500754.8A CN105113123A (en) | 2015-08-14 | 2015-08-14 | Ageing-resistant down feather composite wadding and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110699967A (en) * | 2019-11-02 | 2020-01-17 | 六安市皖西羽绒有限公司 | Preparation method of high-filling-power down feather |
| CN116945705A (en) * | 2023-07-17 | 2023-10-27 | 广东启悦未来科技股份有限公司 | Down feather fabric and preparation process thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4167604A (en) * | 1978-06-30 | 1979-09-11 | Warnaco Inc. | Thermal insulation material comprising a mixture of down and synthetic fiber staple |
| CN1237658A (en) * | 1999-06-25 | 1999-12-08 | 张立文 | Down non-woven fabric |
| CN104762691A (en) * | 2015-03-27 | 2015-07-08 | 安徽省含山县富强羽绒制品有限公司 | Antimicrobial deodorizing down composite fiber and manufacturing method thereof |
| CN104762692A (en) * | 2015-03-27 | 2015-07-08 | 安徽省含山县富强羽绒制品有限公司 | Moisture-absorbing thermal-insulation down composite fiber and manufacturing method thereof |
-
2015
- 2015-08-14 CN CN201510500754.8A patent/CN105113123A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4167604A (en) * | 1978-06-30 | 1979-09-11 | Warnaco Inc. | Thermal insulation material comprising a mixture of down and synthetic fiber staple |
| CN1237658A (en) * | 1999-06-25 | 1999-12-08 | 张立文 | Down non-woven fabric |
| CN104762691A (en) * | 2015-03-27 | 2015-07-08 | 安徽省含山县富强羽绒制品有限公司 | Antimicrobial deodorizing down composite fiber and manufacturing method thereof |
| CN104762692A (en) * | 2015-03-27 | 2015-07-08 | 安徽省含山县富强羽绒制品有限公司 | Moisture-absorbing thermal-insulation down composite fiber and manufacturing method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 杭伟明: "《纤维化学及面料》", 30 November 2005, 北京：中国纺织出版社 * |
| 武继松 张如全: "《纺织科学入门》", 30 September 2011, 北京：中国纺织出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110699967A (en) * | 2019-11-02 | 2020-01-17 | 六安市皖西羽绒有限公司 | Preparation method of high-filling-power down feather |
| CN116945705A (en) * | 2023-07-17 | 2023-10-27 | 广东启悦未来科技股份有限公司 | Down feather fabric and preparation process thereof |
| CN116945705B (en) * | 2023-07-17 | 2024-04-16 | 广东启悦未来科技股份有限公司 | Down feather fabric and preparation process thereof |
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Application publication date: 20151202 |