CN104862803A - Antibiosis acarus killing textile material and preparation method - Google Patents
Antibiosis acarus killing textile material and preparation method Download PDFInfo
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- CN104862803A CN104862803A CN201510312420.8A CN201510312420A CN104862803A CN 104862803 A CN104862803 A CN 104862803A CN 201510312420 A CN201510312420 A CN 201510312420A CN 104862803 A CN104862803 A CN 104862803A
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Abstract
The invention discloses an antibiosis acarus killing textile material and a preparation method thereof. The antibiosis acarus killing textile material is prepared from the following components in parts by weight: 75-80 parts of natural fiber, 15-20 parts of propylene oxide tert-butyl ether, 5-8 parts of hyaluronic acid, 3-8 parts of butyral resin, 3-5 parts of calcium carbonate, 2-6 parts of hydroxypropyl methyl cellulose, 1-3 parts of di-(phenyl dimethyl siloxane) methyl silicone glycol, 0.2-1.8 parts of 70 acid anhydride and 0.5-1 part of zinc borate. The invention also provides the preparation method of the antibiosis acarus killing textile material.
Description
Technical field
The invention belongs to textile material field, particularly a kind of antibacterial mite-removing textile material and preparation method thereof.
Background technology
Along with improving constantly of people's living standard, the requirement for weaving face fabric also gets more and more, and functional textile, except having basic fabric property, also needs to possess the effects such as antiultraviolet, antibacterial, aspect, health care.
Antibacterial fine textile material refers to be killed microorganisms such as bacterium, fungi and viruses or inhibiting fiber or fabric, its object is not only to prevent textiles from being stain by microorganism and damages, the more important thing is to prevent communicate illness, ensure the health of human body and comfortable and easy to wear, reduce the cross-infection rate of PE, make textiles obtain the New function of health care.
Antibiotic fabric makes fabric obtain the functions such as good antibacterial, mildew-resistant, deodorization, effectively can suppress the microbial growth in fibre, prevent communicate illness, to ensure healthiness.
Summary of the invention
For above-mentioned demand, invention especially provides a kind of antibacterial mite-removing textile material and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
A kind of antibacterial mite-removing textile material, be made up of the component comprising following weight portion:
Described natural fabric is selected from one or more in cotton fiber, flax fibre, wool fibre and silk fiber.
Described component also comprises glass microballoon 0-2 weight portion.
Described calcium carbonate is nano-calcium carbonate calcium powder.
A preparation method for antibacterial mite-removing textile material, the method comprises the following steps:
(1) epoxy propane butyl ether 15-20 weight portion, hyaluronic acid 5-8 weight portion, polyvinyl butyral resin 3-8 weight portion, calcium carbonate 3-5 weight portion, hydroxypropyl methylcellulose 2-6 weight portion, two-(phenyldimethicones) methyl silanol 1-3 weight portion is taken, at 85-100 DEG C, stir;
(2) glass microballoon 0-2 weight portion, natural fabric 75-80 weight portion is added successively, at 180-220 DEG C, melting under 21-25MPa, stir 5-15 minute, slowly add 70 acid anhydrides 0.2-1.8 weight portions and Firebrake ZB 0.5-1 weight portion under agitation, spinning, by tractive process, degassed, drying, obtained antibacterial mite-removing textile material.
Described drying condition is at 65-80 DEG C, dries 1-4 hour.
Compared with prior art, its beneficial effect is in the present invention:
(1) the antibacterial mite-removing textile material that obtains of the present invention, by adding polyvinyl butyral resin, two-(phenyldimethicones) methyl silanol, 70 acid anhydrides and Firebrake ZB, make the textile material obtained have good antibacterial mite-removing, there is good pliability and feel simultaneously.
(2) the antibacterial mite-removing textile material that obtains of the present invention is by adding hydroxypropyl methylcellulose, calcium carbonate, makes obtained material have good mechanical strength, and has longer service life.
(3) antibacterial mite-removing textile material of the present invention, its preparation method is simple, is easy to suitability for industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) epoxy propane butyl ether 15kg, hyaluronic acid 5kg, polyvinyl butyral resin 3kg, nano-calcium carbonate calcium powder 3kg, hydroxypropyl methylcellulose 2kg, two-(phenyldimethicones) methyl silanol 1kg is taken, at 85 DEG C, stir;
(2) add cotton fiber 75kg successively, at 180 DEG C, melting under 21MPa, stir 5 minutes, slowly add 70 acid anhydrides 0.2kg and Firebrake ZB 0.5kg under agitation, spinning, by tractive process, degassed, dry 1 hour at 65 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Embodiment 2
(1) epoxy propane butyl ether 15kg, hyaluronic acid 5kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 3kg, hydroxypropyl methylcellulose 2kg, two-(phenyldimethicones) methyl silanol 1kg is taken, at 85 DEG C, stir;
(2) add cotton fiber 75kg successively, at 180 DEG C, melting under 21MPa, stir 5 minutes, slowly add 70 acid anhydrides 0.2kg and Firebrake ZB 0.5kg under agitation, spinning, by tractive process, degassed, dry 1 hour at 65 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Embodiment 3
(1) epoxy propane butyl ether 20kg, hyaluronic acid 8kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 5kg, hydroxypropyl methylcellulose 6kg, two-(phenyldimethicones) methyl silanol 3kg is taken, at 100 DEG C, stir;
(2) glass microballoon 2kg, flax fibre 80kg is added successively, at 220 DEG C, melting under 25MPa, stir 15 minutes, slowly add 70 acid anhydrides 1.8kg and Firebrake ZB 1kg under agitation, spinning, by tractive process, degassed, dry 4 hours at 80 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Embodiment 4
(1) epoxy propane butyl ether 20kg, hyaluronic acid 8kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 5kg, hydroxypropyl methylcellulose 6kg, two-(phenyldimethicones) methyl silanol 3kg is taken, at 100 DEG C, stir;
(2) glass microballoon 2kg, flax fibre 80kg is added successively, at 220 DEG C, melting under 25MPa, stir 15 minutes, slowly add 70 acid anhydrides 0.2kg and Firebrake ZB 1kg under agitation, spinning, by tractive process, degassed, dry 4 hours at 80 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Embodiment 5
(1) epoxy propane butyl ether 20kg, hyaluronic acid 8kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 5kg, hydroxypropyl methylcellulose 6kg, two-(phenyldimethicones) methyl silanol 3kg is taken, at 100 DEG C, stir;
(2) glass microballoon 2kg, wool fibre 80kg is added successively, at 220 DEG C, melting under 25MPa, stir 15 minutes, slowly add 70 acid anhydrides 0.2kg and Firebrake ZB 0.5kg under agitation, spinning, by tractive process, degassed, dry 4 hours at 80 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Comparative example 1
(1) epoxy propane butyl ether 20kg, hyaluronic acid 8kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 5kg, hydroxypropyl methylcellulose 6kg, two-(phenyldimethicones) methyl silanol 3kg is taken, at 100 DEG C, stir;
(2) add glass microballoon 2kg, wool fibre 80kg successively, at 220 DEG C, melting under 25MPa, stir 15 minutes, slowly add 70 acid anhydrides 0.2kg under agitation, spinning, by tractive process, degassed, dry 4 hours at 80 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Comparative example 2
(1) epoxy propane butyl ether 20kg, hyaluronic acid 8kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 5kg, hydroxypropyl methylcellulose 6kg, two-(phenyldimethicones) methyl silanol 3kg is taken, at 100 DEG C, stir;
(2) add glass microballoon 2kg, wool fibre 80kg successively, at 220 DEG C, melting under 25MPa, stir 15 minutes, slowly add Firebrake ZB 0.5kg under agitation, spinning, by tractive process, degassed, dry 4 hours at 80 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Comparative example 3
(1) take epoxy propane butyl ether 20kg, hyaluronic acid 8kg, polyvinyl butyral resin 8kg, nano-calcium carbonate calcium powder 5kg, hydroxypropyl methylcellulose 6kg, at 100 DEG C, stir;
(2) glass microballoon 2kg, wool fibre 80kg is added successively, at 220 DEG C, melting under 25MPa, stir 15 minutes, slowly add Firebrake ZB 0.5kg, 70 acid anhydrides 0.2kg under agitation, spinning, by tractive process, degassed, dry 4 hours at 80 DEG C, obtained antibacterial mite-removing textile material.
The performance test results of obtained antibacterial mite-removing textile material is as shown in table 1.
Table 1
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (6)
1. an antibacterial mite-removing textile material, is characterized in that, is made up of the component comprising following weight portion:
2. antibacterial mite-removing textile material according to claim 1, it is characterized in that, described natural fabric is selected from one or more in cotton fiber, flax fibre, wool fibre and silk fiber.
3. antibacterial mite-removing textile material according to claim 1, it is characterized in that, described component also comprises glass microballoon 0-2 weight portion.
4. antibacterial mite-removing textile material according to claim 1, it is characterized in that, described calcium carbonate is nano-calcium carbonate calcium powder.
5. a preparation method for antibacterial mite-removing textile material, is characterized in that, the method comprises the following steps:
(1) epoxy propane butyl ether 15-20 weight portion, hyaluronic acid 5-8 weight portion, polyvinyl butyral resin 3-8 weight portion, calcium carbonate 3-5 weight portion, hydroxypropyl methylcellulose 2-6 weight portion, two-(phenyldimethicones) methyl silanol 1-3 weight portion is taken, at 85-100 DEG C, stir;
(2) glass microballoon 0-2 weight portion, natural fabric 75-80 weight portion is added successively, at 180-220 DEG C, melting under 21-25MPa, stir 5-15 minute, slowly add 70 acid anhydrides 0.2-1.8 weight portions and Firebrake ZB 0.5-1 weight portion under agitation, spinning, by tractive process, degassed, drying, obtained antibacterial mite-removing textile material.
6. the preparation method of antibacterial mite-removing textile material according to claim 5, is characterized in that, described drying condition is at 65-80 DEG C, dries 1-4 hour.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106283657A (en) * | 2016-08-19 | 2017-01-04 | 常熟市大正纺织制版有限公司 | The postfinishing process of wool knitting fabrics |
| CN111592767A (en) * | 2020-06-16 | 2020-08-28 | 浦江环彩纺织有限公司 | Novel health-care material and preparation method thereof |
| JP2022049637A (en) * | 2020-09-16 | 2022-03-29 | 青島迦南美地家居用品有限公司 | Hyaluronic microcapsule, fiber containing the same, preparation method and usage |
| CN114606770A (en) * | 2022-03-21 | 2022-06-10 | 浙江隆腾医用新材料有限公司 | Processing method for improving spinnability of carboxymethyl cellulose fiber |
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| CN104294400A (en) * | 2014-10-14 | 2015-01-21 | 安徽天鹅科技实业（集团）有限公司 | Cotton fibers with antibacterial anti-mite effects and manufacturing method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106283657A (en) * | 2016-08-19 | 2017-01-04 | 常熟市大正纺织制版有限公司 | The postfinishing process of wool knitting fabrics |
| CN111592767A (en) * | 2020-06-16 | 2020-08-28 | 浦江环彩纺织有限公司 | Novel health-care material and preparation method thereof |
| JP2022049637A (en) * | 2020-09-16 | 2022-03-29 | 青島迦南美地家居用品有限公司 | Hyaluronic microcapsule, fiber containing the same, preparation method and usage |
| JP7140950B2 (en) | 2020-09-16 | 2022-09-22 | 青島迦南美地家居用品有限公司 | Hyaluronic acid microcapsules, fibers containing same, method of preparation and use |
| CN114606770A (en) * | 2022-03-21 | 2022-06-10 | 浙江隆腾医用新材料有限公司 | Processing method for improving spinnability of carboxymethyl cellulose fiber |
| CN114606770B (en) * | 2022-03-21 | 2024-02-06 | 浙江隆腾医用新材料有限公司 | Treatment method for improving spinnability of carboxymethyl cellulose fiber |
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Application publication date: 20150826 |