CN104278359A - Cotton fibers with antibacterial and insect-resisting effects and production method of cotton fibers - Google Patents
Cotton fibers with antibacterial and insect-resisting effects and production method of cotton fibers Download PDFInfo
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- CN104278359A CN104278359A CN201410540677.4A CN201410540677A CN104278359A CN 104278359 A CN104278359 A CN 104278359A CN 201410540677 A CN201410540677 A CN 201410540677A CN 104278359 A CN104278359 A CN 104278359A
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Abstract
The invention discloses cotton fibers with antibacterial and insect-resisting effects. The cotton fibers are characterized by being prepared from the following raw materials in parts by weight: 21-24 parts of cotton fibers, 10-12 parts of apocynum venetum fibers, 6-8 parts of silk fibers, 7-9 parts of cashmere fibers, 9-11 parts of pineapple fibers, 4-7 parts of polypropylene fibers, 6-8 parts of taxus chinensis superfine micro-powder, 3-5 parts of ailanthus altissima leaf extracted powder, 1-3 parts of zeolite powder, 1.1-2.3 parts of chitosan, 0.5-0.7 part of magnesium nitride, 0.8-1.4 parts of N,N-dicyanoethylaniline, 5-7 parts of sulfonated castor oil, 15-18 parts of fatty alcohol alkoxy ether, 1-2 parts of mashed garlic, 1.3-2.5 parts of cnidium monnieri cuss, 2.1-3.6 parts of coptis chinensis, 90-95 parts of 1-ethyl-3-methylimidazolium diethylphosphate, 95-100 parts of 1-butyl-3-methylimidazolium acetate, 3-6 parts of an addition agent and a proper amount of water. According to the cotton fibers, the taxus chinensis superfine micro-powder is added into raw materials by adopting an ultrasonic technology and a prepared cotton textile has a very good health effect and a useful pain-relieving effect on tumor patients and female symptoms; furthermore, the other active ingredients are added so that the good clothes properties of sweat absorption, breathability, softness, allergy prevention, easiness of washing, low probability of fuzzing and balling up and the like of natural cotton fibers are maintained, and the cotton fibers have good antibacterial and insect-resisting functions, a good electromagnetic radiation shielding function and the like.
Description
Technical field
The present invention relates to textile material technical field, be specifically related to a kind of to there is cotton fiber of antibacterial insect protected effect and preparation method thereof.
Background technology
Cotton fiber is fiber coating on the seed of Malvaceae cotton, and also known as cotton, being called for short cotton, is the main raw material of China's textile industry.The moisture absorption of cotton fiber goods and good permeability, wear-resisting washable, soft and warming, wear warmth retention property winter good, dress in summer is ventilative nice and cool, is widely used in garment material, drapery.
But cotton fiber makes it apply to be restricted because it exists many defects in the prior art.Such as cotton fiber goods are subject to microbial action, are easily corroded by bacterium, mould, and antibacterial and mouldproof effect is not remarkable; The anti-uv-ray of cotton fiber own is poor, makes it make summer clothes and skin chromogenesis precipitation can be caused even to cause cutaneum carcinoma; Cotton fiber flame retardant effect is poor, and the disaster hidden-trouble caused thus is in rising trend.For overcoming the deficiencies in the prior art, be necessary natural cotton fiber in addition modification, thus be obtainedly applicable to the cotton fiber with functions such as cost low, function diversification, fire-retardant, intensity high, sterilization uvioresistant, radiation proofs of modern for the different demands of cotton fiber goods.
Summary of the invention
Object of the present invention is just to provide a kind ofly has cotton fiber of antibacterial insect protected effect and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of cotton fiber with antibacterial insect protected effect, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 21-24, apocynum fibre 10-12, silk fiber 6-8, cashmere fiber 7-9, pina fibre 9-11, polypropylene fiber 4-7, Chinese yew super fine 6-8, tree-of-heaven leaf extract powder 3-5, zeolite powder 1-3, shitosan 1.1-2.3, magnesium nitride 0.5-0.7, N, N-dicyanoethyl-aniline 0.8-1.4, sulfonated castor oil 5-7, fatty alcohol alkoxyl ether 15-18, garlic powder 1-2, frutus cnidii 1.3-2.5, coptis 2.1-3.6, 1-ethyl-3-methylimidazole diethyl phosphate 90-95, 1-butyl-3-N-Methylimidazoleacetic salt 95-100, auxiliary agent 3-6, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: bleeding agent OE-35 1-3, lemon 2-5, butyl 10-13, diepoxy triethylene glycol glycidol ether 8-10, thymol 4-6, chitosan 1.2-2.2, nanoscale Tourmaline 3-5, Tea Saponin 0.5-0.8, dimethyl silicone polymer two quaternary amine 4.5-6.5, its preparation method is by the swelling 2-3 hour of nanoscale Tourmaline room temperature in distilled water, form suspension, then butyl, diepoxy triethylene glycol glycidol ether, thymol, dimethyl silicone polymer two quaternary amine mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
Described a kind of preparation method with the cotton fiber of antibacterial insect protected effect, is characterized in that comprising the following steps:
(1) get garlic powder, frutus cnidii, the coptis put into hot water and soak filtration in 6-8 hour, cotton fiber, apocynum fibre, silk fiber, cashmere fiber, pina fibre, polypropylene fiber immersion 7-10 hour is added in filtrate, filtering drying, sprays into Chinese yew super fine, tree-of-heaven leaf extract powder sonic oscillation grinding 1-2 hour;
(2) by zeolite powder high-temperature calcination 30-40 minute, add shitosan, magnesium nitride adds water and grind spraying dry after 30-50 minute together, add sulfonated castor oil, fatty alcohol alkoxyl ether, N, N-dicyanoethyl-aniline stir and evenly mix, be warming up to 140-165 DEG C, keep temperature to stir 2-3 hour;
(3) step (1) product is dipped in step (2) and adopts two leaching two roll process, then steam treatment 5-10 minute, also dewatered drying adds 1-ethyl-3-methylimidazole diethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt stirs 20-40 minute in cleaning, be heated to 90-100 DEG C, add other residual components again and stir 40-60 minute, obtained spinning solution is through spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: Chinese yew super fine adopts ultrasonic technology to add in raw material by the present invention, obtained COTTON FABRIC has well health care and lenitive effect to tumor patient and women's illness, in addition, the present invention also added other active ingredients not only remain absorbing sweat that natural cotton fiber has, ventilative, softness, anti-sensitivity, easily clean, not easily the excellent easing characteristic such as fluffing, balling-up also there is the functions such as good antibacterial insect protected and electromagnetic radiation shielding.
Detailed description of the invention
Described a kind of cotton fiber with antibacterial insect protected effect, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 23, apocynum fibre 11, silk fiber 6, cashmere fiber 8, pina fibre 11, polypropylene fiber 4, Chinese yew super fine 7, tree-of-heaven leaf extract powder 4, zeolite powder 1, shitosan 1.9, magnesium nitride 0.6, N, N-dicyanoethyl-aniline 0.9, sulfonated castor oil 5, fatty alcohol alkoxyl ether 17, garlic powder 1, frutus cnidii 1.7, the coptis 2.7, 1-ethyl-3-methylimidazole diethyl phosphate 94, 1-butyl-3-N-Methylimidazoleacetic salt 100, auxiliary agent 3, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: bleeding agent OE-35 1, lemon 3, butyl 12, diepoxy triethylene glycol glycidol ether 9, thymol 5, chitosan 1.8, nanoscale Tourmaline 4, Tea Saponin 0.6, dimethyl silicone polymer two quaternary amine 4.9, its preparation method is by the swelling 2-3 hour of nanoscale Tourmaline room temperature in distilled water, form suspension, then butyl, diepoxy triethylene glycol glycidol ether, thymol, dimethyl silicone polymer two quaternary amine mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
Preparation method comprises the following steps:
(1) get garlic powder, frutus cnidii, the coptis put into hot water and soak filtration in 6-8 hour, cotton fiber, apocynum fibre, silk fiber, cashmere fiber, pina fibre, polypropylene fiber immersion 7-10 hour is added in filtrate, filtering drying, sprays into Chinese yew super fine, tree-of-heaven leaf extract powder sonic oscillation grinding 1-2 hour;
(2) by zeolite powder high-temperature calcination 30-40 minute, add shitosan, magnesium nitride adds water and grind spraying dry after 30-50 minute together, add sulfonated castor oil, fatty alcohol alkoxyl ether, N, N-dicyanoethyl-aniline stir and evenly mix, be warming up to 140-165 DEG C, keep temperature to stir 2-3 hour;
(3) step (1) product is dipped in step (2) and adopts two leaching two roll process, then steam treatment 5-10 minute, also dewatered drying adds 1-ethyl-3-methylimidazole diethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt stirs 20-40 minute in cleaning, be heated to 90-100 DEG C, add other residual components again and stir 40-60 minute, obtained spinning solution is through spinning, winding, boundling, stretching and get final product.
The technical parameter index of the cotton fiber using the present invention to produce is as follows:
(1) pliability is fluffy smooth flexible, and intensity is high, flame retardant effect is excellent;
(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99%.
Claims (2)
1. one kind has the cotton fiber of antibacterial insect protected effect, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 21-24, apocynum fibre 10-12, silk fiber 6-8, cashmere fiber 7-9, pina fibre 9-11, polypropylene fiber 4-7, Chinese yew super fine 6-8, tree-of-heaven leaf extract powder 3-5, zeolite powder 1-3, shitosan 1.1-2.3, magnesium nitride 0.5-0.7, N, N-dicyanoethyl-aniline 0.8-1.4, sulfonated castor oil 5-7, fatty alcohol alkoxyl ether 15-18, garlic powder 1-2, frutus cnidii 1.3-2.5, coptis 2.1-3.6, 1-ethyl-3-methylimidazole diethyl phosphate 90-95, 1-butyl-3-N-Methylimidazoleacetic salt 95-100, auxiliary agent 3-6, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: bleeding agent OE-35 1-3, lemon 2-5, butyl 10-13, diepoxy triethylene glycol glycidol ether 8-10, thymol 4-6, chitosan 1.2-2.2, nanoscale Tourmaline 3-5, Tea Saponin 0.5-0.8, dimethyl silicone polymer two quaternary amine 4.5-6.5, its preparation method is by the swelling 2-3 hour of nanoscale Tourmaline room temperature in distilled water, form suspension, then butyl, diepoxy triethylene glycol glycidol ether, thymol, dimethyl silicone polymer two quaternary amine mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
2. a kind of preparation method with the cotton fiber of antibacterial insect protected effect according to claim 1, is characterized in that comprising the following steps:
(1) get garlic powder, frutus cnidii, the coptis put into hot water and soak filtration in 6-8 hour, cotton fiber, apocynum fibre, silk fiber, cashmere fiber, pina fibre, polypropylene fiber immersion 7-10 hour is added in filtrate, filtering drying, sprays into Chinese yew super fine, tree-of-heaven leaf extract powder sonic oscillation grinding 1-2 hour;
(2) by zeolite powder high-temperature calcination 30-40 minute, add shitosan, magnesium nitride adds water and grind spraying dry after 30-50 minute together, add sulfonated castor oil, fatty alcohol alkoxyl ether, N, N-dicyanoethyl-aniline stir and evenly mix, be warming up to 140-165 DEG C, keep temperature to stir 2-3 hour;
(3) step (1) product is dipped in step (2) and adopts two leaching two roll process, then steam treatment 5-10 minute, also dewatered drying adds 1-ethyl-3-methylimidazole diethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt stirs 20-40 minute in cleaning, be heated to 90-100 DEG C, add other residual components again and stir 40-60 minute, obtained spinning solution is through spinning, winding, boundling, stretching and get final product.
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| CN104911737A (en) * | 2015-05-20 | 2015-09-16 | 铜陵宏正网络科技有限公司 | Nanometer antibacterial mothproof cashmere composite fiber and manufacturing method thereof |
| CN104911735A (en) * | 2015-05-20 | 2015-09-16 | 铜陵宏正网络科技有限公司 | Multi-fiber-blended anti-pilling warming cashmere composite fiber and manufacturing method thereof |
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Application publication date: 20150114 |