CN104278357A - Cotton fibers capable of releasing far infrared negative ions and production method of cotton fibers - Google Patents

Cotton fibers capable of releasing far infrared negative ions and production method of cotton fibers Download PDF

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Publication number
CN104278357A
CN104278357A CN201410540669.XA CN201410540669A CN104278357A CN 104278357 A CN104278357 A CN 104278357A CN 201410540669 A CN201410540669 A CN 201410540669A CN 104278357 A CN104278357 A CN 104278357A
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China
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parts
infrared negative
cotton fibers
hour
minute
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CN201410540669.XA
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Chinese (zh)
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储荣生
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安徽天鹅科技实业(集团)有限公司
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Priority to CN201410540669.XA priority Critical patent/CN104278357A/en
Publication of CN104278357A publication Critical patent/CN104278357A/en

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Abstract

The invention discloses cotton fibers capable of releasing far infrared negative ions. The cotton fibers are characterized by being prepared from the following raw materials in parts by weight: 20-23 parts of cotton fibers, 7-9 part of active carbon fibers, 6-10 parts of camel hair fiber, 10-12 parts of ramie fibers, 5-7 parts of polypropylene fibers, 3-5 parts of fructus xanthii extract, 2-4 parts of far infrared negative ion powder, 1-2 parts of nano aluminum oxide, 1-3 parts of medical stones, 2.1-3.5 parts of hot melt adhesive powder, 15-18 parts of C12 alcohol polyoxyethylene ether, 9-12 parts of citric acid, 12-15 parts of monoacetin, 2-4 parts of divaricate saposhnikovia root, 1-3 parts of isatis tinctoria, 100-110 parts of 1-ethyl-3-methylimidazolium diethylphosphate, 95-105 parts of 1-butyl-3-methylimidazolium acetate, 4-6 parts of an addition agent and a proper amount of water. According to the cotton fibers capable of releasing the far infrared negative ions, the fructus xanthii extract is added into the raw materials by using an ultrasonic technology and has a good bacterium inhibition effect on staphylococcus aureus; and meanwhile, active ingredients including the far infrared negative ion powder, divaricate saposhnikovia root, isatis tinctoria and the like are added so that the prepared cotton fibers can release the negative ions beneficial to a human body and also have the effects of resisting bacteria, preventing mites, retarding flame and the like.

Description

A kind of cotton fiber discharging far-infrared negative-ion and preparation method thereof

Technical field

The present invention relates to textile material technical field, be specifically related to a kind of cotton fiber discharging far-infrared negative-ion and preparation method thereof.

Background technology

Cotton fiber is fiber coating on the seed of Malvaceae cotton, and also known as cotton, being called for short cotton, is the main raw material of China's textile industry.The moisture absorption of cotton fiber goods and good permeability, wear-resisting washable, soft and warming, wear warmth retention property winter good, dress in summer is ventilative nice and cool, is widely used in garment material, drapery.

But cotton fiber makes it apply to be restricted because it exists many defects in the prior art.Such as cotton fiber goods are subject to microbial action, are easily corroded by bacterium, mould, and antibacterial and mouldproof effect is not remarkable; The anti-uv-ray of cotton fiber own is poor, makes it make summer clothes and skin chromogenesis precipitation can be caused even to cause cutaneum carcinoma; Cotton fiber flame retardant effect is poor, and the disaster hidden-trouble caused thus is in rising trend.For overcoming the deficiencies in the prior art, be necessary natural cotton fiber in addition modification, thus be obtainedly applicable to the cotton fiber with functions such as cost low, function diversification, fire-retardant, intensity high, sterilization uvioresistant, radiation proofs of modern for the different demands of cotton fiber goods.

Summary of the invention

Object of the present invention is just to provide a kind of cotton fiber discharging far-infrared negative-ion and preparation method thereof, to overcome the deficiencies in the prior art.

The object of the present invention is achieved like this:

A kind of cotton fiber discharging far-infrared negative-ion, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 20-23, activated carbon fiber 7-9, camel wool fiber 6-10, ramee 10-12, polypropylene fibre 5-7, xanthium sibiricum 3-5, far-infrared negative-ion powder 2-4, nano aluminium oxide 1-2, medical stone 1-3, hot-melt adhesive powder 2.1-3.5, C12 alcohol polyoxyethylene ether 15-18, citric acid 9-12, single triacetin 12-15, windproof 2-4, Radix Isatidis 1-3, 1-ethyl-3-methylimidazole diethyl phosphate 100-110, 1-butyl-3-N-Methylimidazoleacetic salt 95-105, auxiliary agent 4-6, suitable quantity of water.

Described auxiliary agent is made up of following raw materials in part by weight: bleeding agent OE-35 1-3, lemon 2-5, butyl 10-13, diepoxy triethylene glycol glycidol ether 8-10, thymol 4-6, chitosan 1.2-2.2, nanoscale Tourmaline 3-5, Tea Saponin 0.5-0.8, dimethyl silicone polymer two quaternary amine 4.5-6.5, its preparation method is by the swelling 2-3 hour of nanoscale Tourmaline room temperature in distilled water, form suspension, then butyl, diepoxy triethylene glycol glycidol ether, thymol, dimethyl silicone polymer two quaternary amine mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.

Described a kind of preparation method discharging the cotton fiber of far-infrared negative-ion, is characterized in that comprising the following steps:

(1) get windproof, Radix Isatidis to put into hot water and soak filtration in 6-8 hour, cotton fiber, activated carbon fiber, camel wool fiber, ramee, polypropylene fibre immersion 7-10 hour is added in filtrate, filtering drying, sprays into xanthium sibiricum, far-infrared negative-ion powder sonic oscillation grinding 1-2 hour;

(2) by medical stone high-temperature calcination 30-40 minute, add nano aluminium oxide to add water and grind spraying dry after 30-50 minute together, add C12 alcohol polyoxyethylene ether, citric acid, single triacetin stir and evenly mix, be warming up to 150-170 DEG C, keep temperature to stir 2-3 hour;

(3) step (1) product is dipped in step (2) and adopts two leaching two roll process, then steam treatment 5-10 minute, also dewatered drying adds 1-ethyl-3-methylimidazole diethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt stirs 20-40 minute in cleaning, be heated to 90-100 DEG C, add other residual components again and stir 40-60 minute, obtained spinning solution is through spinning, winding, boundling, stretching and get final product.

The present invention has following beneficial effect: xanthium sibiricum utilizes ultrasonic technology to add in raw material by the present invention, good bacteriostasis is had to staphylococcus aureus, also added the active ingredients such as far-infrared negative-ion powder, windproof, Radix Isatidis simultaneously, obtained cotton fiber can not only discharge the anion useful to human body, also has the effects such as antibiosis anti-acarien is fire-retardant.

Detailed description of the invention

Described a kind of cotton fiber discharging far-infrared negative-ion, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 22, activated carbon fiber 7, camel wool fiber 10, ramee 11, polypropylene fibre 5, xanthium sibiricum 4, far-infrared negative-ion powder 2, nano aluminium oxide 2, medical stone 1, hot-melt adhesive powder 2.6, C12 alcohol polyoxyethylene ether 15, citric acid 9, single triacetin 13, windproof 2, Radix Isatidis 1,1-ethyl-3-methylimidazole diethyl phosphate 100,1-butyl-3-N-Methylimidazoleacetic salt 95, auxiliary agent 4, suitable quantity of water.

Described auxiliary agent is made up of following raw materials in part by weight: bleeding agent OE-35 1, lemon 3, butyl 12, diepoxy triethylene glycol glycidol ether 9, thymol 5, chitosan 1.8, nanoscale Tourmaline 4, Tea Saponin 0.6, dimethyl silicone polymer two quaternary amine 4.9, its preparation method is by the swelling 2-3 hour of nanoscale Tourmaline room temperature in distilled water, form suspension, then butyl, diepoxy triethylene glycol glycidol ether, thymol, dimethyl silicone polymer two quaternary amine mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.

Preparation method comprises the following steps:

(1) get windproof, Radix Isatidis to put into hot water and soak filtration in 6-8 hour, cotton fiber, activated carbon fiber, camel wool fiber, ramee, polypropylene fibre immersion 7-10 hour is added in filtrate, filtering drying, sprays into xanthium sibiricum, far-infrared negative-ion powder sonic oscillation grinding 1-2 hour;

(2) by medical stone high-temperature calcination 30-40 minute, add nano aluminium oxide to add water and grind spraying dry after 30-50 minute together, add C12 alcohol polyoxyethylene ether, citric acid, single triacetin stir and evenly mix, be warming up to 150-170 DEG C, keep temperature to stir 2-3 hour;

(3) step (1) product is dipped in step (2) and adopts two leaching two roll process, then steam treatment 5-10 minute, also dewatered drying adds 1-ethyl-3-methylimidazole diethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt stirs 20-40 minute in cleaning, be heated to 90-100 DEG C, add other residual components again and stir 40-60 minute, obtained spinning solution is through spinning, winding, boundling, stretching and get final product.

The technical parameter index of the cotton fiber using the present invention to produce is as follows:

(1) pliability is fluffy smooth flexible, and intensity is high, flame retardant effect is excellent;

(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99.3%.

Claims (2)

1. one kind can discharge the cotton fiber of far-infrared negative-ion, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 20-23, activated carbon fiber 7-9, camel wool fiber 6-10, ramee 10-12, polypropylene fibre 5-7, xanthium sibiricum 3-5, far-infrared negative-ion powder 2-4, nano aluminium oxide 1-2, medical stone 1-3, hot-melt adhesive powder 2.1-3.5, C12 alcohol polyoxyethylene ether 15-18, citric acid 9-12, single triacetin 12-15, windproof 2-4, Radix Isatidis 1-3, 1-ethyl-3-methylimidazole diethyl phosphate 100-110, 1-butyl-3-N-Methylimidazoleacetic salt 95-105, auxiliary agent 4-6, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: bleeding agent OE-35 1-3, lemon 2-5, butyl 10-13, diepoxy triethylene glycol glycidol ether 8-10, thymol 4-6, chitosan 1.2-2.2, nanoscale Tourmaline 3-5, Tea Saponin 0.5-0.8, dimethyl silicone polymer two quaternary amine 4.5-6.5, its preparation method is by the swelling 2-3 hour of nanoscale Tourmaline room temperature in distilled water, form suspension, then butyl, diepoxy triethylene glycol glycidol ether, thymol, dimethyl silicone polymer two quaternary amine mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
2. a kind of preparation method discharging the cotton fiber of far-infrared negative-ion according to claim 1, is characterized in that comprising the following steps:
(1) get windproof, Radix Isatidis to put into hot water and soak filtration in 6-8 hour, cotton fiber, activated carbon fiber, camel wool fiber, ramee, polypropylene fibre immersion 7-10 hour is added in filtrate, filtering drying, sprays into xanthium sibiricum, far-infrared negative-ion powder sonic oscillation grinding 1-2 hour;
(2) by medical stone high-temperature calcination 30-40 minute, add nano aluminium oxide to add water and grind spraying dry after 30-50 minute together, add C12 alcohol polyoxyethylene ether, citric acid, single triacetin stir and evenly mix, be warming up to 150-170 DEG C, keep temperature to stir 2-3 hour;
(3) step (1) product is dipped in step (2) and adopts two leaching two roll process, then steam treatment 5-10 minute, also dewatered drying adds 1-ethyl-3-methylimidazole diethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt stirs 20-40 minute in cleaning, be heated to 90-100 DEG C, add other residual components again and stir 40-60 minute, obtained spinning solution is through spinning, winding, boundling, stretching and get final product.
CN201410540669.XA 2014-10-14 2014-10-14 Cotton fibers capable of releasing far infrared negative ions and production method of cotton fibers CN104278357A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105088768A (en) * 2015-08-31 2015-11-25 安徽天威羊绒制品有限公司 Hydrophobic modified antimicrobial cashmere fiber and manufacturing method of hydrophobic modified antimicrobial cashmere fiber

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101117747A (en) * 2006-08-01 2008-02-06 上海宜美家装饰用品有限公司 Multifunctional composite fiber fabric and manufacturing method therefor
WO2008153239A1 (en) * 2007-06-11 2008-12-18 Nanopoly Co., Ltd Manufacture method of wet-tissue with antimicrobial and anti-fungus function
CN101352943A (en) * 2008-08-26 2009-01-28 江苏紫荆花纺织科技股份有限公司 Sandwich cocoon fibre filling core material
CN101870820A (en) * 2010-06-07 2010-10-27 华中农业大学 Antibacterial decorative material made by utilizing cotton stalk and preparation method thereof
CN102051701A (en) * 2011-01-14 2011-05-11 浙江民心生态科技有限公司 Production process of bamboo charcoal fiber

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101117747A (en) * 2006-08-01 2008-02-06 上海宜美家装饰用品有限公司 Multifunctional composite fiber fabric and manufacturing method therefor
WO2008153239A1 (en) * 2007-06-11 2008-12-18 Nanopoly Co., Ltd Manufacture method of wet-tissue with antimicrobial and anti-fungus function
CN101352943A (en) * 2008-08-26 2009-01-28 江苏紫荆花纺织科技股份有限公司 Sandwich cocoon fibre filling core material
CN101870820A (en) * 2010-06-07 2010-10-27 华中农业大学 Antibacterial decorative material made by utilizing cotton stalk and preparation method thereof
CN102051701A (en) * 2011-01-14 2011-05-11 浙江民心生态科技有限公司 Production process of bamboo charcoal fiber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105088768A (en) * 2015-08-31 2015-11-25 安徽天威羊绒制品有限公司 Hydrophobic modified antimicrobial cashmere fiber and manufacturing method of hydrophobic modified antimicrobial cashmere fiber

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Application publication date: 20150114