CN105434298A - Natural Chinese prescription mouthwash - Google Patents
Natural Chinese prescription mouthwash Download PDFInfo
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Abstract
The invention discloses a natural Chinese prescription mouthwash, which is prepared from the following raw materials in percentage by mass: 0.2%-5.0% of a licorice extract, 0.1%-5.0% of a tea extract, 0.1%-3.0% of a scutellaria extract, 0.1%-3.0% of a cortex phellodendri extract, 0.1%-5.0% of a gallnut extract, 0.1%-5.0% of a honeysuckle extract, 0.1%-3.0% of a cassia twig extract, 0.01%-3.0% of menthyl lactate, 0.01%-3.0% of citric acid, 0.5%-8.0% of glycerinum, 0.5%-8.0% of sorbitol and 0.1%-1.0% of polysorbate-20. The mouthwash disclosed by the invention has a bacteriostasis function and is interesting in use.
Description
Technical field
The present invention relates to a kind of hygienic article, relate to a kind of natural Chinese prescription collutory particularly.
Background technology
Collutory, is also called oral washing liquid, is dental health product, has bacteriostasis and sterilization and prevents effect of dental caries, gingivitis and the halitosis caused by microorganism.Recent years, collutory is receiving an acclaim on the market gradually, has a lot of people often can help not free removing in halitosis meets with client.Mainly because collutory is convenient and simple.Although collutory is easy to use, but the collutory peddled out on the market major part composition is all that industrial chemical makes, easily there is oral problem in life-time service, easy tooth and oral mucosal surface painted, the sense of taste of taste bud is reduced, and suppress the secretion of saliva, cause the malaise symptoms such as xerostomia, causalgia.
Therefore, new mouthrinse product is needed to adapt to the demand in market.
Summary of the invention
The object of the present invention is to provide a kind of natural Chinese prescription collutory, to solve the above-mentioned problems in the prior art.
Technical scheme provided by the invention is as follows:
A kind of natural Chinese prescription collutory, in mass ratio, comprising: Radix Glycyrrhizae extract: 0.2-5.0%; Folium Camelliae sinensis extract: 0.1-5.0%; Radix Scutellariae extract: 0.1-3.0%; Cortex Phellodendri extract: 0.1-3.0%; Galla Chinensis extract: 0.1-5.0%; Flos Lonicerae: 0.1-5.0%; Ramulus Cinnamomi extract: 0.1-3.0%;
Wherein, also menthyl lactate is comprised in this collutory: 0.01-3.0%; Citric acid: 0.01-3.0%; Glycerol: 0.5-8.0%; Sorbitol: 0.5-8.0%, polysorbate-20 (Tween20): 0.1-1.0%, above composition mainly works effects such as improving mouthfeel.
Described Radix Glycyrrhizae extract, Folium Camelliae sinensis extract, Radix Scutellariae extract, Cortex Phellodendri extract, Galla Chinensis extract, Flos Lonicerae extract, Ramulus Cinnamomi extract are water or ethanol extraction.
The preparation method of each extract is respectively: Radix Glycyrrhizae is with 50-100% alcohol extraction, and after concentrated, lyophilizing is for subsequent use;
Folium Camelliae sinensis is with 0-50% ethanol (preferred 50-30%) extraction, and after concentrated, lyophilizing is for subsequent use;
Radix Scutellariae, with concentrated after 60-100% alcohol extraction, concentrates the 1/2-1/3 being preferably concentrated into original volume, and concentrate is again with 0-50% ethanol (preferred 5-30%) extraction, concentrated freeze-dried rear for subsequent use;
Cortex Phellodendri, with concentrated after 60-100% alcohol extraction, concentrates the 1/2-1/3 being preferably concentrated into original volume, and concentrate is again with 0-50% ethanol (preferred 5-30%) extraction, and after concentrated, lyophilizing is for subsequent use;
Galla Chinensis is with concentrated after 60-100% alcohol extraction, and the concentrated 1/2-1/3 being preferably concentrated into original volume, concentrate is again with 0-50% ethanol (preferred 5-30%) extraction, and after concentrated, lyophilizing is for subsequent use
Flos Lonicerae is with concentrated freeze-dried for subsequent use after 60-100% alcohol extraction
Ramulus Cinnamomi extracts with 60-100%, and after concentrated, lyophilizing is for subsequent use.
Described extraction is at least one in immersion, reflux or ultrasonic extraction.
Wherein, during raw material abstraction, be preferably crushed to below 20 orders, be more preferably and be crushed to below 80 orders.
When adopting immersion way extraction, preferably soak more than 12h, more preferably soak more than 24h.Extract added during immersion needs abundant submergence raw material, and extract volume is preferably 1-3 times of volume of raw material.
When adopting reflux mode to extract, preferably reflux 2-4h.
During use, each extract uses homogenizer average twice after adding pure water mixing to scale, and muddy thing is filtered removal.
Composition of the present invention is as follows:
Radix Glycyrrhizae: containing compositions such as glycyrrhizin, liquorice flavonoids compound and Radix Asparagi phthalein amine, mannitol in Radix Glycyrrhizae.The alcohol extract of Radix Glycyrrhizae and Monosodium glycyrrhetin all have inhibitory action to staphylococcus aureus, tubercule bacillus, escherichia coli, ameba and infusorian in vitro, have stronger antibacterial effect.It contains glycyrrhizic acid elite simultaneously, growth for mutant has inhibitory action, and have and strengthen the active function of cellular immunity, repair damaged cell, suppress to divide the bad and sebum film of immunity and secrete effect that incomplete Skin Cell produces again.This product is effective adding ingredient with the ethanolic extract of Radix Glycyrrhizae, strengthen by this product antibiotic and sterilizing effect and reach oral mucosa repair effect.
Folium Camelliae sinensis: the primary efficacy composition of Folium Camelliae sinensis is tea polyphenols, tea polyphenols is the polyphenols in Folium Camelliae sinensis, tans or tea tannin also known as tea.Tea polyphenols has stronger antioxidation, effectively can remove harmful free radicals, blocks lipid peroxidation process, improves the activity of human enzymes, thus plays the effect of mutation, anticancer.Except antioxidation, tea polyphenols also has bacteriostasis, by the astriction of bind protein, can be combined and cause bacterial death with bacterium protein, having stronger inhibitory action to staphylococcus, escherichia coli, bacillus subtilis etc.Tea polyphenols can also adsorb the abnormal flavour in food, therefore has certain deodorization.This product is effective adding ingredient with tea extraction thing, nationality tea polyphenols antioxidation and antibacterial ability, strengthens the antibiotic and sterilizing of product and effect of deodorization.
Flos Lonicerae: just extensive and famous with its medical value since ancient times.Its effect mainly heat-clearing and toxic substances removing.Modern study proves, Flos Lonicerae contains the pharmacological component such as chlorogenic acid, luteolin glycosides, there is the effect of good anti-inflammation, and has a broad antifungal spectrum, have Bacillus typhi, Salmonella paratyphi, staphylococcus aureus, Hemolytic streptococcus, dysentery bacterium, vibrio cholera etc. and significantly suppress killing action.In addition, Flos Lonicerae also has the several functions such as antiviral, antiinflammatory, pathogenic fire purging are antipyretic, immunity moderation.This product is effective adding ingredient with honeysuckle extract, to reach the effect of bacteriostasis and sterilization.
Cortex Phellodendri: Cortex Phellodendri is practised and claims " Cortex Phellodendri " is the bark of rutaceae Cortex Phellodendri or wampee.Cortex Phellodendri antibiotic effective ingredient is berberine.In vitro tests is all effective to staphylococcus aureus, streptococcus pneumoniae, diphtheria corynebacterium, Streptococcus viridans, dysentery bacterium (except Song Nei Shi) etc.In addition, Cortex Phellodendri also has antifungal effect, and its ether extract has stronger bacteriostasis to Cryptococcus histolyticus and trichophyton purpureatum.This product is effective adding ingredient with the ethanolic extract of Cortex Phellodendri, strengthens antibiotic and sterilizing effect of product by this.
Radix Scutellariae: another name Radix Scutellariae, tsuchikane tea root.Main containing flavone compound.The test of Radix Scutellariae alcohol immersion Plating has inhibitory action to escherichia coli, Fructus Citri tangerinae grass bacillus, staphylococcus aureus, dysentery bacterium, Bacillus typhi, vibrio cholera, Bacillus proteus, bacillus pyocyaneus, hemolytic vessel used to hold grain at the imperial sacrifice coccus, Diplococcus pneumoniae.This product is effective adding ingredient with the ethanolic extract of Radix Scutellariae, strengthens antibiotic and sterilizing effect of product by this.
Galla Chinensis: containing tannic acid, by playing effect of bacteriostasis and sterilization in conjunction with tropina.In vitro tests shows, Galla Chinensis decoct all has significantly antibacterial and bactericidal action to staphylococcus aureus, beta hemolytic streptococcus, streptococcus pneumoniae, bacillus pyocyaneus, dysentery bacterium, anthrax bacillus, diphtheria corynebacterium, escherichia coli, Typhoid and paratyphoid bacillus etc.This product is effective adding ingredient with gallic ethanolic extract, strengthens antibiotic and sterilizing effect of product by this.
Ramulus Cinnamomi: rectification of name Cortex Cinnamomi, has another name called beautiful osmanthus, Cortex cinnamomi japonici (Ramulus Cinnamomi) etc., main containing compositions such as volatile oil cinnamic aldehyde.Ramulus Cinnamomi ethanol extract can suppress escherichia coli in vitro, bacillus subtilis and staphylococcus aureus, and valid density is 25 mg/ml or following; To Staphylococcus albus, dysentery bacterium, Typhoid and paratyphoid first bacillus, streptococcus pneumoniae, aerobacteria, Bacillus proteus, anthrax bacillus, Salmonella enteritidis, vibrio cholera etc. also have inhibitory action, this product is effective adding ingredient with the ethanolic extract of Ramulus Cinnamomi, strengthens antibiotic and sterilizing effect of product by this.
Menthyl lactate: formula teacher designed cold-type yellow (clear) product and can only adopt Herba Menthae in the past, did not have other to select.But the volatility of Herba Menthae and zest are very large, cause cooling effect strong and very brief.The menthyl lactate that the present invention adopts is a kind of Herba Menthae derivant, have slight Herba Menthae fragrance, taste almost insipidness, but with lasting, pleasant cooling effect, having the features such as long-acting, tasteless, non-stimulated, is the best substitute of Herba Menthae.
Citric acid: citric acid is mainly used in refreshment drink and the curing foods etc. such as soda pop, fruit drink, lactic acid beverage in food additive.The characteristic of the chelation that citric acid has and adjustment acid-base value, makes it can play seasoning effect on the one hand; The heat resistance of microorganism can also be weakened on the other hand and suppress its growth, increasing the performance of antioxidant, inhibitory enzyme activity, extend the storage life of product.
Glycerol: glycerol is sweet, the colourless syrupy liq of a kind of taste, usually used as sweeting agent and wetting agent in food processing industry.Add glycerol in food, its mouthfeel and smooth degree can be regulated, make product smooth good to eat.
Sorbitol: sorbitol is a kind of broad-spectrum industrial chemicals, have in industries such as food, daily use chemicals, medicine and apply very widely, can be used as the uses such as sweeting agent, wetting agent, chelating agen and antiseptic, there is the nutritional advantages of polyhydric alcohol simultaneously, i.e. the effect such as low heat value, low sugar, anti-caries.In food, add sorbitol can also play the effect regulating mouthfeel and smoothness.
Polysorbate-20 (Tween20): edible solubilizing agent.
Advantage of the present invention is as follows: collutory of the present invention has been arranged in pairs or groups the pure Chinese medicine extraction liquid of many moneys, and all formula components are the raw material of food stage, not containing ethanol, pigment and other chemical compositions, is a really natural rinse product.There is sterilizing, antihalitosis, to the gingival hemorrhage caused by gingivitis, periodontitis, pericoronitis, tooth meat swells and ache, recurrent oral ulcer, has the effect shown.Result of use is obvious, and abnormal smells from the patient is pure and fresh, excellent taste.
In addition, the much impurity be combined with buccal smears can be produced after mouthwash of the present invention discharge, after consumer uses collutory of the present invention, obviously can observe the collutory difference spued before using and after using, there is suitable entertaining, and point out the importance of gargling.
Accompanying drawing explanation
Fig. 1 is the figure that the present invention uses front collutory, A is top view, and B is side view, the concentric ring shape at the bottom of can clearly seeing glass;
Fig. 2 is the collutory figure after the present invention uses, A is top view, and B is side view, can see that collutory is muddy state, and the inside is containing white, light yellow precipitate, and cup Bottom Shape is invisible.
Detailed description of the invention
Each raw material of Chinese medicine in following examples is commercial
Embodiment 1
First after Radix Glycyrrhizae, Folium Camelliae sinensis, Radix Scutellariae, Cortex Phellodendri, Galla Chinensis, Flos Lonicerae, Ramulus Cinnamomi being crushed to about 60 orders respectively
Radix Glycyrrhizae, with 75% ethanol of 2 times of volumes, soaks extraction 12h, and concentrated (extract, lower same) lyophilizing is for subsequent use afterwards;
Folium Camelliae sinensis is with 30% ethanol of 2 times of volumes, and soak extraction 12h, after concentrated, lyophilizing is for subsequent use;
Radix Scutellariae is with 75% ethanol of 2 times of volumes, and soak extraction 12h, be concentrated into 1/2 of original volume after extraction, concentrate is again with 30% ethanol reextraction 3h of 1 times of volume, and extraction fluid is concentrated freeze-dried rear for subsequent use;
Cortex Phellodendri, with 75% ethanol of 2 times of volumes, is soaked extraction 12h, is concentrated into 1/2 of original volume after extraction, and concentrate is again with 30% ethanol reextraction 3h of 1 times of volume, and after extraction fluid is concentrated, lyophilizing is for subsequent use;
Galla Chinensis, with 75% ethanol of 2 times of volumes, is concentrated into 1/2 of original volume after soaking extraction 12h, and concentrate is again with 30% ethanol reextraction 3h of 1 times of volume, and after extraction fluid is concentrated, lyophilizing is for subsequent use;
Flos Lonicerae is with after 75% soak with ethanol extraction 12h of 2 times of volumes, and concentrated, lyophilizing is for subsequent use;
Ramulus Cinnamomi is with after 75% soak with ethanol extraction 12h of 2 times of volumes, and concentrated, lyophilizing is for subsequent use.
By following mass ratio configuration collutory, after each extract freeze-drying powder being added to scale pure water mixing, with homogenizer homogenizing twice, and muddy thing filtration is removed and be get final product:
Radix Glycyrrhizae extract: 2.0%; Folium Camelliae sinensis extract: 2.0%; Radix Scutellariae extract: 3.0%; Cortex Phellodendri extract: 0.3%; Galla Chinensis extract: 0.5%; Flos Lonicerae: 0.5%; Ramulus Cinnamomi extract: 3.0%; Menthyl lactate: 0.03%; Citric acid: 0.08%; Glycerol: 0.5%; Sorbitol: 1.5%, polysorbate-20:0.1%.
Embodiment 2
The lyophilized powder of the present embodiment is identical with embodiment 1, and difference is, collutory in mass ratio, comprising: Radix Glycyrrhizae extract: 5.0%; Folium Camelliae sinensis extract: 0.5%; Radix Scutellariae extract: 3.0%; Cortex Phellodendri extract: 0.1%; Galla Chinensis extract: 1.5%; Flos Lonicerae: 0.1%; Ramulus Cinnamomi extract: 3.0%; Menthyl lactate: 0.1%; Citric acid: 0.1%; Glycerol: 0.8%; Sorbitol: 0.8%, polysorbate-20:0.5%.
Embodiment 3
The lyophilized powder of the present embodiment is identical with embodiment 1, and difference is, collutory in mass ratio, comprising: Radix Glycyrrhizae extract: 2.5%; Folium Camelliae sinensis extract: 4.0%; Radix Scutellariae extract: 3.0%; Cortex Phellodendri extract: 0.7%; Galla Chinensis extract: 3.5%; Flos Lonicerae: 1.5%; Ramulus Cinnamomi extract: 1.3%; Menthyl lactate: 0.1%; Citric acid: 0.3%; Glycerol: 1.0%; Sorbitol: 0.5%, polysorbate-20 (Tween20): 0.2%.
Embodiment 4
The lyophilized powder of the present embodiment is identical with embodiment 1, and difference is, collutory in mass ratio, comprising: Radix Glycyrrhizae extract: 4.2%; Folium Camelliae sinensis extract: 2.5%; Radix Scutellariae extract: 1.8%; Cortex Phellodendri extract: 2.3%; Galla Chinensis extract: 1.5%; Flos Lonicerae: 2.5%; Ramulus Cinnamomi extract: 2.5%; Menthyl lactate: 0.3%; Citric acid: 0.01%; Glycerol: 1.5%; Sorbitol: 0.5%, polysorbate-20 (Tween20): 0.5%.
Embodiment 5
The lyophilized powder of the present embodiment is identical with embodiment 1, and difference is, collutory in mass ratio, comprising: Radix Glycyrrhizae extract: 0.2%; Folium Camelliae sinensis extract: 5.0%; Radix Scutellariae extract: 0.1%; Cortex Phellodendri extract: 3.0%; Galla Chinensis extract: 0.1%; Flos Lonicerae: 04.0%; Ramulus Cinnamomi extract: 3.0%; Menthyl lactate: 0.6%; Citric acid: 0.05%; Glycerol: 2.5%; Sorbitol: 2.5%, polysorbate-20:0.7%.
Embodiment 6,
Substantially identical with embodiment 1, difference is, Folium Camelliae sinensis extracts with the water soaking of 2 times of volumes.
Embodiment 8
Substantially identical with embodiment 1, difference is, Radix Scutellariae, Cortex Phellodendri and gallic extraction fluid are respectively water.
Embodiment 9
Collutory ratio according to embodiment 1 mixes each lyophilized powder, carry out bacteriostatic experiment (bacteriostasis) with filter paper diffusion method, assessment lyophilized powder is to the effect of Propiobacterium (Propionibacteriumacne), golden yellow Portugal coccus (Staphylococcusaureus), escherichia coli (Escherichiacoli).Result shows mouthwash formula lyophilized powder of the present invention and all shows three kinds of strains and have biocidal property, is that 31.2mm, 32.8mm and 44.8mm display has bacteriostasis (as figure below) respectively to Propiobacterium, golden yellow Portugal coccus, escherichia coli inhibition zone.
The lyophilized powder bacteriostatic experiment of this mouthwash formula
Each numerical value is all the meansigma methodss of carrying out 5 repetitions
In addition, Fig. 1 and Fig. 2 respectively illustrate the embodiment of the present invention 1 do not use before collutory, and the contrast of collutory after using, Fig. 1, before using, collutory is clear shape; Fig. 2, after using, collutory is overall muddy, containing white, light yellow precipitate, this phenomenon is that the combination of the composition in these plant extracts and the composition in oral cavity is formed, obviously can observe the collutory difference spued before using and after using, there is suitable entertaining, and point out the importance of gargling.
Claims (6)
1. a natural Chinese prescription collutory, in mass ratio, comprising: Radix Glycyrrhizae extract: 0.2-5.0%; Folium Camelliae sinensis extract: 0.1-5.0%; Radix Scutellariae extract: 0.1-3.0%; Cortex Phellodendri extract: 0.1-3.0%; Galla Chinensis extract: 0.1-5.0%; Flos Lonicerae extract: 0.1-5.0%; Ramulus Cinnamomi extract: 0.1-3.0%.
2. natural Chinese prescription collutory according to claim 1, is characterized in that, also comprise: menthyl lactate: 0.01-3.0%; Citric acid: 0.01-3.0%; Glycerol: 0.5-8.0%; Sorbitol: 0.5-8.0%, polysorbate-20:0.1-1.0%.
3. natural Chinese prescription collutory according to claim 1, is characterized in that: described Radix Glycyrrhizae extract, Folium Camelliae sinensis extract, Radix Scutellariae extract, Cortex Phellodendri extract, Galla Chinensis extract, Flos Lonicerae extract, Ramulus Cinnamomi extract are water or ethanol extraction.
4. the natural Chinese prescription collutory of one according to claim 3, is characterized in that: the preparation method of each extract is respectively: Radix Glycyrrhizae is with 50-100% alcohol extraction, and after concentrated, lyophilizing is for subsequent use;
Folium Camelliae sinensis is with 0-50% alcohol extraction, and after concentrated, lyophilizing is for subsequent use;
Radix Scutellariae is with concentrated after 60-100% alcohol extraction, and concentrate is again with 0-50% alcohol extraction, concentrated freeze-dried rear for subsequent use;
Cortex Phellodendri is with concentrated after 60-100% alcohol extraction, and concentrate is again with 0-50% alcohol extraction, and after concentrated, lyophilizing is for subsequent use;
Galla Chinensis is with concentrated after 60-100% alcohol extraction, and concentrate is again with 0-50% alcohol extraction, and after concentrated, lyophilizing is for subsequent use;
Flos Lonicerae is with concentrated freeze-dried for subsequent use after 60-100% alcohol extraction
Ramulus Cinnamomi extracts with 60-100%, and after concentrated, lyophilizing is for subsequent use.
5. the natural Chinese prescription collutory of one according to claim 4, is characterized in that: described extraction is at least one in immersion, reflux or ultrasonic extraction.
6. the natural Chinese prescription collutory of one according to claim 4, is characterized in that: during use, and each extract uses homogenizer average twice after adding pure water mixing to scale, and muddy thing is filtered removal.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106038389A (en) * | 2016-06-21 | 2016-10-26 | 江苏奇力康皮肤药业有限公司 | Long-effective bacterial inhibition type mouth wash |
| CN107157837A (en) * | 2017-06-01 | 2017-09-15 | 南京辅安堂药业有限公司 | A kind of black tea gargle and preparation method thereof |
| CN107174566A (en) * | 2016-11-08 | 2017-09-19 | 黄秀芳 | Clean the teeth sterilization flavouring multipurpose gargle |
| CN107334748A (en) * | 2017-06-30 | 2017-11-10 | 常州市协旺纺织品有限公司 | A kind of periodontitis is with to medicine film and preparation method thereof |
| CN107412122A (en) * | 2017-05-05 | 2017-12-01 | 杭州蜂耘科技有限公司 | A kind of pure natural oral nursing liquid |
| CN107714595A (en) * | 2016-08-12 | 2018-02-23 | 张彬梅 | One kind cleaning mouthwash formula and production method |
| CN108721176A (en) * | 2018-08-31 | 2018-11-02 | 黄冈师范学院 | A kind of mouthwash and preparation method thereof |
| CN108785161A (en) * | 2018-07-02 | 2018-11-13 | 亿利耐雀生物科技有限公司 | A kind of antibacterial mouthwash and preparation method thereof containing licoflavone |
| CN114642616A (en) * | 2022-01-17 | 2022-06-21 | 西南大学 | Mouth wash based on mulberry leaf polyphenol and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038389A (en) * | 2016-06-21 | 2016-10-26 | 江苏奇力康皮肤药业有限公司 | Long-effective bacterial inhibition type mouth wash |
| CN107714595A (en) * | 2016-08-12 | 2018-02-23 | 张彬梅 | One kind cleaning mouthwash formula and production method |
| CN107174566A (en) * | 2016-11-08 | 2017-09-19 | 黄秀芳 | Clean the teeth sterilization flavouring multipurpose gargle |
| CN107412122A (en) * | 2017-05-05 | 2017-12-01 | 杭州蜂耘科技有限公司 | A kind of pure natural oral nursing liquid |
| CN107157837A (en) * | 2017-06-01 | 2017-09-15 | 南京辅安堂药业有限公司 | A kind of black tea gargle and preparation method thereof |
| CN107334748A (en) * | 2017-06-30 | 2017-11-10 | 常州市协旺纺织品有限公司 | A kind of periodontitis is with to medicine film and preparation method thereof |
| CN108785161A (en) * | 2018-07-02 | 2018-11-13 | 亿利耐雀生物科技有限公司 | A kind of antibacterial mouthwash and preparation method thereof containing licoflavone |
| CN108785161B (en) * | 2018-07-02 | 2021-07-30 | 亿利耐雀生物科技有限公司 | Antibacterial mouth wash containing licoflavone and preparation method thereof |
| CN108721176A (en) * | 2018-08-31 | 2018-11-02 | 黄冈师范学院 | A kind of mouthwash and preparation method thereof |
| CN114642616A (en) * | 2022-01-17 | 2022-06-21 | 西南大学 | Mouth wash based on mulberry leaf polyphenol and preparation method thereof |
| CN114642616B (en) * | 2022-01-17 | 2024-01-26 | 西南大学 | Mulberry leaf polyphenol-based mouthwash and preparation method thereof |
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| CN105434298B (en) | 2018-11-02 |
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