CN100368392C - 双官能异(硫)氰酸苯酯、其制备方法和中间体 - Google Patents

双官能异(硫)氰酸苯酯、其制备方法和中间体 Download PDF

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Publication number
CN100368392C
CN100368392C CNB2003801046055A CN200380104605A CN100368392C CN 100368392 C CN100368392 C CN 100368392C CN B2003801046055 A CNB2003801046055 A CN B2003801046055A CN 200380104605 A CN200380104605 A CN 200380104605A CN 100368392 C CN100368392 C CN 100368392C
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base
phenyl
formula
compound
group
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Chinese (zh)
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CN1717388A (zh
Inventor
G·汉普雷希特
M·普尔
R·赖因哈德
W·塞茨
B·沃尔夫
N·格策
M·凯尔
I·扎加塞尔
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72—Nitrogen atoms
    • C07D213/76—Nitrogen atoms to which a second hetero atom is attached
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C307/00—Amides of sulfuric acids, i.e. compounds having singly-bound oxygen atoms of sulfate groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C307/04—Diamides of sulfuric acids
    • C07C307/06—Diamides of sulfuric acids having nitrogen atoms of the sulfamide groups bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C331/00—Derivatives of thiocyanic acid or of isothiocyanic acid
    • C07C331/16—Isothiocyanates
    • C07C331/28—Isothiocyanates having isothiocyanate groups bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D207/20—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
    • C07D211/08—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms
    • C07D211/18—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms with substituted hydrocarbon radicals attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D211/68—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D211/70—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/22—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with hetero atoms directly attached to ring nitrogen atoms
    • C07D295/26—Sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/52—Radicals substituted by nitrogen atoms not forming part of a nitro radical
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D319/04—1,3-Dioxanes; Hydrogenated 1,3-dioxanes
    • C07D319/06—1,3-Dioxanes; Hydrogenated 1,3-dioxanes not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D333/00—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom
    • C07D333/02—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings
    • C07D333/04—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom
    • C07D333/06—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to the ring carbon atoms
    • C07D333/14—Radicals substituted by singly bound hetero atoms other than halogen
    • C07D333/20—Radicals substituted by singly bound hetero atoms other than halogen by nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Hydrogenated Pyridines (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
CNB2003801046055A 2002-10-30 2003-10-29 双官能异(硫)氰酸苯酯、其制备方法和中间体 Expired - Lifetime CN100368392C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10250614 2002-10-30
DE10250614.0 2002-10-30

Publications (2)

Publication Number Publication Date
CN1717388A CN1717388A (zh) 2006-01-04
CN100368392C true CN100368392C (zh) 2008-02-13

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Country Status (18)

Country Link
US (3) US7820846B2 (https=)
EP (2) EP1560810B1 (https=)
JP (1) JP4738812B2 (https=)
KR (1) KR101055954B1 (https=)
CN (1) CN100368392C (https=)
AR (1) AR041861A1 (https=)
AU (1) AU2003287972B2 (https=)
BR (2) BR0315932A (https=)
CA (1) CA2504410C (https=)
EA (1) EA010872B1 (https=)
ES (1) ES2565961T3 (https=)
HU (1) HUE027607T2 (https=)
IL (1) IL167983A (https=)
MX (1) MXPA05004546A (https=)
PL (1) PL214983B1 (https=)
UA (1) UA89941C2 (https=)
WO (1) WO2004039768A1 (https=)
ZA (1) ZA200504331B (https=)

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EA012035B1 (ru) 2004-07-22 2009-06-30 Басф Акциенгезельшафт Способ получения 3-фенилурацилов
JP5555426B2 (ja) * 2005-12-01 2014-07-23 ビーエーエスエフ ソシエタス・ヨーロピア スルホンアミド類の製造方法
DE102005057681A1 (de) * 2005-12-01 2007-06-06 Basf Ag Verfahren zur Herstellung fluorierter m-Nitro-Benzoesäurechloride
CN101821233B (zh) * 2007-10-12 2016-06-29 巴斯夫欧洲公司 生产磺酸二酰胺的方法
MX2012005501A (es) 2009-11-13 2012-07-10 Basf Se Compuestos 3- (3, 4- dihidro-2h-benzo [1, 4] -oxazin-6-il)-1h-piri midin-2, 4-diona como herbicidas.
US10436790B2 (en) 2011-09-28 2019-10-08 Waters Technologies Corporation Rapid fluorescence tagging of glycans and other biomolecules with enhanced MS signals
US11352325B2 (en) 2011-09-28 2022-06-07 Waters Technologies Corporation Rapid fluorescence tagging of glycans and other biomolecules with enhanced MS signals
EP3974412A1 (en) * 2011-09-28 2022-03-30 Waters Technologies Corporation Rapid fluorescence tagging of glycans and other biomolecules with enhanced ms signals
CN102702056B (zh) * 2012-05-31 2014-09-24 北京师范大学 一种一锅法合成取代间苯二异硫氰酸酯的方法、合成的取代间苯二异硫氰酸酯化合物
CN115753702A (zh) 2014-10-30 2023-03-07 沃特世科技公司 快速制备标记的葡糖基胺和分析生产所述标记的葡糖基胺的糖基化生物分子的方法
US10502720B2 (en) 2014-11-13 2019-12-10 Waters Technologies Corporation Methods for liquid chromatography calibration for rapid labeled N-glycans
WO2017202768A1 (en) 2016-05-24 2017-11-30 Basf Se Herbicidal uracilpyrid
US11061023B2 (en) 2016-06-21 2021-07-13 Waters Technologies Corporation Fluorescence tagging of glycans and other biomolecules through reductive amination for enhanced MS signals
WO2017222955A1 (en) 2016-06-21 2017-12-28 Waters Technologies Corporation Methods of electrospray ionization of glycans modified with amphipathic, strongly basic moieties
EP3479103B1 (en) 2016-07-01 2022-04-20 Waters Technologies Corporation Methods for the rapid preparation of labeled glycosylamines from complex matrices using molecular weight cut off filtration and on-filter deglycosylation
EP3587396A1 (en) 2018-06-27 2020-01-01 Basf Se A method of isolating a n-(3-nitrobenzoyl)sulfamide
IL305851A (en) 2021-03-26 2023-11-01 Adama Agan Ltd Preparation of 2-chloro-4-fluoro-5-nitrobenzoic acid
US20260085051A1 (en) 2022-08-31 2026-03-26 Adama Agan Ltd. Preparation of 2-chloro-4-fluoro-5-nitrobenzoic acid
WO2025124942A1 (en) 2023-12-12 2025-06-19 BASF Agro B.V. Process for preparing a saflufenacil intermediate

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PL214983B1 (pl) 2013-10-31
BRPI0315932B1 (pt) 2019-08-13
ES2565961T3 (es) 2016-04-07
US20110009640A1 (en) 2011-01-13
CA2504410C (en) 2012-03-20
EA010872B1 (ru) 2008-12-30
US7820846B2 (en) 2010-10-26
PL376995A1 (pl) 2006-01-23
KR101055954B1 (ko) 2011-08-09
IL167983A (en) 2010-11-30
JP2006504763A (ja) 2006-02-09
EP2537829B1 (de) 2016-03-02
EA200500598A1 (ru) 2006-06-30
WO2004039768A1 (de) 2004-05-13
ZA200504331B (en) 2006-07-26
BR0315932A (pt) 2005-09-13
EP1560810B1 (de) 2012-08-01
US20060004220A1 (en) 2006-01-05
UA89941C2 (ru) 2010-03-25
AR041861A1 (es) 2005-06-01
EP2537829A1 (de) 2012-12-26
MXPA05004546A (es) 2005-10-18
US8541611B2 (en) 2013-09-24
CA2504410A1 (en) 2004-05-13
KR20050090380A (ko) 2005-09-13
EP1560810A1 (de) 2005-08-10
US20120271049A1 (en) 2012-10-25
HUE027607T2 (en) 2016-10-28
JP4738812B2 (ja) 2011-08-03
AU2003287972A1 (en) 2004-05-25
CN1717388A (zh) 2006-01-04
AU2003287972B2 (en) 2010-04-22
US8232421B2 (en) 2012-07-31

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