CA3071926A1 - Procede de preparation de composes ethyleneamines - Google Patents

Procede de preparation de composes ethyleneamines Download PDF

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Publication number
CA3071926A1
CA3071926A1 CA3071926A CA3071926A CA3071926A1 CA 3071926 A1 CA3071926 A1 CA 3071926A1 CA 3071926 A CA3071926 A CA 3071926A CA 3071926 A CA3071926 A CA 3071926A CA 3071926 A1 CA3071926 A1 CA 3071926A1
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CA
Canada
Prior art keywords
compound
adduct
moiety
polyethyleneamine
compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA3071926A
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English (en)
Other versions
CA3071926C (fr
Inventor
Rens VENEMAN
Antoon Jacob Berend Ten Kate
Michiel Jozef Thomas RAAIJMAKERS
Slavisa JOVIC
Rolf Krister EDVINSSON
Eike Nicolas Kantzer
Karl Fredrik LAKE
Ina EHLERS
Hendrik VAN DAM
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Nouryon Chemicals International BV
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Nouryon Chemicals International BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Nouryon Chemicals International BV filed Critical Nouryon Chemicals International BV
Publication of CA3071926A1 publication Critical patent/CA3071926A1/fr
Application granted granted Critical
Publication of CA3071926C publication Critical patent/CA3071926C/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/62—Preparation of compounds containing amino groups bound to a carbon skeleton by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/08—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions not involving the formation of amino groups, hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/18—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic with hydroxy groups and at least two amino groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/02—Polyamines
    • C08G73/0206—Polyalkylene(poly)amines
    • C08G73/0213—Preparatory process
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

L'invention concerne un procédé de fabrication de composés polyéthylèneannines choisis dans le groupe des polyéthylèneamines et des hydroxyéthyléthylèneamines comprenant - une étape d'adduction consistant à fournir un produit d'addition de CO2 d'un composé de départ comprenant une fraction -NH-CH2-CH2-NH- ou une fraction -NH-CH2-CH2-OH, ou HO-CH2-CH2-OH, - une étape de réaction consistant à faire réagir un composé à fonction hydroxy choisi dans le groupe des éthanolamines et du dihydroxyéthane avec un composé à fonction amine, au moins une partie des composés à fonction hydroxy et des composés à fonction amine étant fournie sous forme d'un produit d'addition de CO2, pour former un produit d'addition de CO2 d'un composé de polyéthylèneannine produit, - une étape d'élimination consistant à convertir le produit d'addition de CO2 du composé de polyéthylèneannine produit en un composé d'amine de polyéthylène produit correspondant, une fraction comprenant un composé de recyclage comprenant une fraction -NH-CH2-CH2-NH- ou une fraction -NH-CH2-CH2-OH, ou HO-CH2-CH2-OH, ou des produits d'addition de CO2 de celle-ci, est fournie à partir de la fin de l'étape de réaction ou de l'étape d'élimination à l'étape d'adduction ou à l'étape de réaction, le composé de recyclage ayant par molécule, en moyenne moins du total des fractions -NH-CH2-CH2-NH- et des fractions -NH-CH2-CH2-OH par rapport au composé de polyéthylèneannine produit.
CA3071926A 2017-08-11 2018-08-07 Procede de preparation de composes ethyleneamines Active CA3071926C (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP17186001.8 2017-08-11
EP17186001 2017-08-11
PCT/EP2018/071324 WO2019030194A1 (fr) 2017-08-11 2018-08-07 Procédé de préparation de composés éthylèneamines

Publications (2)

Publication Number Publication Date
CA3071926A1 true CA3071926A1 (fr) 2019-02-14
CA3071926C CA3071926C (fr) 2024-02-27

Family

ID=59677029

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3071926A Active CA3071926C (fr) 2017-08-11 2018-08-07 Procede de preparation de composes ethyleneamines

Country Status (10)

Country Link
US (1) US11072686B2 (fr)
EP (1) EP3665155B1 (fr)
JP (1) JP7199418B2 (fr)
KR (1) KR102623955B1 (fr)
CN (1) CN111032618B (fr)
BR (1) BR112020002479B1 (fr)
CA (1) CA3071926C (fr)
MX (1) MX2020001588A (fr)
TW (1) TWI774813B (fr)
WO (1) WO2019030194A1 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI761545B (zh) * 2017-07-10 2022-04-21 荷蘭商安科智諾貝爾化學國際公司 製備伸乙基胺及伸乙基胺衍生物之方法
CN110997621A (zh) * 2017-08-11 2020-04-10 诺力昂化学品国际有限公司 将环状亚烷基脲转化成其相应亚烷基胺的方法
BR112020006431B1 (pt) * 2017-10-27 2023-03-21 Basf Se Processo para remover nmeda de uma mistura
US11878954B2 (en) 2019-02-13 2024-01-23 Nouryon Chemicals International B.V. Process for manufacturing ethyleneamine compounds
CN113557224A (zh) * 2019-02-13 2021-10-26 诺力昂化学品国际有限公司 用于制造亚乙基胺化合物的方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2497309A (en) * 1944-05-04 1950-02-14 Du Pont Process for the preparation of ethyleneurea
US2806017A (en) * 1952-08-09 1957-09-10 American Cyanamid Co Polymerization of cyclic carbamates
US2812333A (en) * 1954-09-27 1957-11-05 Union Carbide Corp Process for the preparation of 1-(2-hydroxyethyl) imidazolidine-2
US2847418A (en) * 1955-05-06 1958-08-12 Union Carbide Corp Di(hydroxyethyl) imidazolidone-2 and production of n, n'-di-(2-hydroxyethyl) ethylene diamine
US3383417A (en) 1964-12-21 1968-05-14 Jefferson Chem Co Inc Method for the preparation of aminoethylethanolamine
US4503250A (en) * 1981-09-30 1985-03-05 Union Carbide Corporation Preparation of polyalkylene polyamines
US4387249A (en) * 1981-12-18 1983-06-07 The Dow Chemical Company Process for the manufacture of diethylenetriamine
KR840000593A (ko) * 1982-07-30 1984-02-25 이용철 Tpa와 eg 혼합물의 유동성을 개선하는 방법
NL8204546A (nl) * 1982-11-23 1984-06-18 Akzo Nv Werkwijze voor het winnen van ethyleenamines uit waterige oplossing.
JPS59155364A (ja) * 1983-02-24 1984-09-04 Nissan Chem Ind Ltd １，３−ジメチル−２−イミダゾリジノンの製造方法
JPS59161338A (ja) * 1983-03-04 1984-09-12 Toyo Soda Mfg Co Ltd エチレンアミン類炭酸塩水溶液からエチレンアミン類を得る方法
JPS6065117A (ja) * 1983-09-19 1985-04-13 Unitika Ltd ゴム補強用ポリエステル繊維の製造法
JPS60120842A (ja) * 1983-12-03 1985-06-28 Toyo Soda Mfg Co Ltd エチレンアミン類炭酸塩からエチレンアミン類を得る方法
JPS60126248A (ja) * 1983-12-09 1985-07-05 Toyo Soda Mfg Co Ltd エチレンアミン類炭酸塩水溶液の脱炭酸方法
TWI241924B (en) * 2001-08-31 2005-10-21 Exxonmobil Chem Patents Inc Low pressure separation of dimethyl ether from an olefin stream
GB0203058D0 (en) * 2002-02-09 2002-03-27 Bp Chem Int Ltd Production of olefins
DE102004011320A1 (de) * 2004-03-09 2005-09-22 Degussa Ag Verfahren zur Herstellung von Aminen aus Carbodiimidgruppen aufweisenden Verbindungen durch Hydrolyse mit Wasser
DE102004046171A1 (de) * 2004-09-23 2006-04-13 Basf Ag Verfahren zur Herstellung von Cyclopentanon
CN101384542B (zh) 2006-02-14 2012-07-04 巴斯夫欧洲公司 由单乙二醇(meg)生产亚乙基胺和乙醇胺的方法

Also Published As

Publication number Publication date
JP7199418B2 (ja) 2023-01-05
RU2020109525A3 (fr) 2021-10-08
CN111032618A (zh) 2020-04-17
BR112020002479B1 (pt) 2023-03-21
EP3665155B1 (fr) 2022-10-05
CA3071926C (fr) 2024-02-27
BR112020002479A2 (pt) 2020-07-28
RU2020109525A (ru) 2021-09-13
US11072686B2 (en) 2021-07-27
MX2020001588A (es) 2020-07-20
US20200362111A1 (en) 2020-11-19
CN111032618B (zh) 2023-04-25
KR102623955B1 (ko) 2024-01-10
JP2020529455A (ja) 2020-10-08
EP3665155A1 (fr) 2020-06-17
WO2019030194A1 (fr) 2019-02-14
TW201920068A (zh) 2019-06-01
TWI774813B (zh) 2022-08-21
KR20200038974A (ko) 2020-04-14

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JP6836596B2 (ja) 高級エチレンアミンおよびエチレンアミン誘導体を調製する方法
CN111032614B (zh) 将环状亚烷基脲转化为其相应亚烷基胺的方法
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