CA2560936C - Process for producing 5-hydroxy-4-thiomethylpyrazole compound - Google Patents

Process for producing 5-hydroxy-4-thiomethylpyrazole compound Download PDF

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Publication number
CA2560936C
CA2560936C CA2560936A CA2560936A CA2560936C CA 2560936 C CA2560936 C CA 2560936C CA 2560936 A CA2560936 A CA 2560936A CA 2560936 A CA2560936 A CA 2560936A CA 2560936 C CA2560936 C CA 2560936C
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CA
Canada
Prior art keywords
group
hydroxy
mmol
represented
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CA2560936A
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English (en)
French (fr)
Other versions
CA2560936A1 (en
Inventor
Yukio Uchida
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ihara Chemical Industry Co Ltd
Original Assignee
Ihara Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=35063690&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2560936(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Ihara Chemical Industry Co Ltd filed Critical Ihara Chemical Industry Co Ltd
Publication of CA2560936A1 publication Critical patent/CA2560936A1/en
Application granted granted Critical
Publication of CA2560936C publication Critical patent/CA2560936C/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28—Two oxygen or sulfur atoms
    • C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA2560936A 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound Expired - Lifetime CA2560936C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2004-102963 2004-03-31
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 ５−ヒドロキシ−４−チオメチルピラゾール化合物の製造方法
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 ５－ヒドロキシ－４－チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
CA2560936A1 CA2560936A1 (en) 2005-10-13
CA2560936C true CA2560936C (en) 2013-01-08

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2560936A Expired - Lifetime CA2560936C (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound

Country Status (19)

Country Link
US (1) US7488831B2 (h)
EP (1) EP1767528B1 (h)
JP (1) JP4621939B2 (h)
KR (1) KR101205731B1 (h)
CN (1) CN1938278B (h)
AU (1) AU2005228017B2 (h)
BR (1) BRPI0509353B1 (h)
CA (1) CA2560936C (h)
CR (1) CR8640A (h)
ES (1) ES2508765T3 (h)
IL (1) IL178233A (h)
IN (1) IN2006DE05581A (h)
MX (1) MX280092B (h)
NZ (1) NZ550143A (h)
PL (1) PL1767528T3 (h)
RU (1) RU2386619C2 (h)
TW (1) TWI357899B (h)
UA (1) UA83910C2 (h)
WO (1) WO2005095352A1 (h)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2333977T3 (es) 2004-10-05 2010-03-03 Syngenta Limited Derivados de isoxazolina y su uso como herbicidas.
NZ554870A (en) * 2004-12-20 2009-09-25 Ihara Chemical Ind Co Process for production of (4,5-dihydroisoxazol-3-Yl)thio- carboxamidine salts
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd ５−ヒドロキシ−１−アルキルピラゾール誘導体の製造方法
AU2007216034B2 (en) * 2006-02-14 2011-08-04 Kumiai Chemical Industry Co., Ltd. Process for production of 5-alkoxy-4-hydroxymethylpyrazole compound
MX2009012749A (es) * 2007-05-25 2010-03-10 Abbott Gmbh & Co Kg Compuestos heterociclicos como moduladores positivos del receptor de glutamato metabotropico 2 (receptor mglu2).
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
DK2504321T3 (da) 2009-11-26 2014-07-14 Basf Se Fremgangsmåde til fremstilling af 5,5-disubstituerede 2-isoxazoliner
EP2504322B1 (de) 2009-11-26 2014-04-02 Basf Se Verfahren zur herstellung 5,5-disubstituierter 4,5-dihydroisoxazol-3-thiocarboxamidin-salze
KR20170102581A (ko) * 2010-05-20 2017-09-11 바이엘 인텔렉쳐 프로퍼티 게엠베하 1-알킬-3-디플루오르메틸-5-히드록시피라졸의 제조 방법
EP2737575B1 (en) 2011-07-29 2024-05-01 University of Saskatchewan Polymer-based resonator antennas
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
JP6400247B1 (ja) * 2015-11-16 2018-10-03 ロンザ・リミテッド １−メチル−３−（トリフルオロメチル）−１ｈ−ピラゾール−５−オールの調製方法
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
CN111542514B (zh) * 2017-12-27 2021-09-03 组合化学工业株式会社 硫基甲脒盐化合物的制造方法
JP6714785B2 (ja) * 2018-05-31 2020-06-24 クミアイ化学工業株式会社 含フッ素ピラゾール誘導体の製造方法及びその中間体
IL290169B2 (en) 2019-07-30 2025-04-01 Adama Agan Ltd Method and intermediates for preparing pyroxulfone
CN112969697A (zh) 2019-10-31 2021-06-15 组合化学工业株式会社 除草剂及其中间体的制造方法
US20230303546A1 (en) 2020-03-05 2023-09-28 Adama Agan Ltd. Process And Intermediates For The Preparation Of Pyroxasulfone
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177245A1 (en) 2020-07-10 2023-05-10 Adama Agan Ltd. Process and intermediates for the preparation of fenoxasulfone
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
TW202334128A (zh) 2021-10-29 2023-09-01 日商組合化學工業股份有限公司 二硫化物化合物、多硫化物化合物及其用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use
AR035912A1 (es) * 2000-03-02 2004-07-28 Aventis Cropscience Sa Compuestos de 4-tiometilpirazol, composicion plaguicida, metodo para el control de plagas en un lugar, semillas tratadas o recubiertas,uso de estos compuestos o composiciones para el control de plagas, uso de estos compuestos para preparar un medicamento veterinario, y,proceso para la preparacion de
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
DE60238194D1 (de) * 2001-06-21 2010-12-16 Kumiai Chemical Industry Co Isoxazolinderivate und herbizide
TW200409758A (en) * 2002-08-01 2004-06-16 Ihara Chemical Ind Co Pyrazole derivatives and process for production thereof
UA78071C2 (en) * 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition

Also Published As

Publication number Publication date
CA2560936A1 (en) 2005-10-13
BRPI0509353B1 (pt) 2019-01-02
KR20070003964A (ko) 2007-01-05
AU2005228017B2 (en) 2010-09-30
MXPA06011130A (es) 2007-01-25
UA83910C2 (ru) 2008-08-26
RU2006138241A (ru) 2008-05-10
TWI357899B (en) 2012-02-11
NZ550143A (en) 2010-04-30
JP4621939B2 (ja) 2011-02-02
WO2005095352A1 (ja) 2005-10-13
IL178233A (en) 2014-02-27
PL1767528T3 (pl) 2015-03-31
RU2386619C2 (ru) 2010-04-20
US20070185334A1 (en) 2007-08-09
EP1767528B1 (en) 2014-09-17
JP2005289824A (ja) 2005-10-20
MX280092B (es) 2010-10-18
US7488831B2 (en) 2009-02-10
ES2508765T3 (es) 2014-10-16
IL178233A0 (en) 2006-12-31
KR101205731B1 (ko) 2012-11-28
EP1767528A4 (en) 2010-04-21
CR8640A (es) 2007-08-28
EP1767528A1 (en) 2007-03-28
TW200536832A (en) 2005-11-16
BRPI0509353A8 (pt) 2017-09-19
AU2005228017A1 (en) 2005-10-13
CN1938278A (zh) 2007-03-28
CN1938278B (zh) 2012-12-12
IN2006DE05581A (h) 2007-08-31
BRPI0509353A (pt) 2007-09-11

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