CA2473146C - Process for production of molecular sieve adsorbent blends and process for production thereof - Google Patents

Process for production of molecular sieve adsorbent blends and process for production thereof Download PDF

Info

Publication number
CA2473146C
CA2473146C CA2473146A CA2473146A CA2473146C CA 2473146 C CA2473146 C CA 2473146C CA 2473146 A CA2473146 A CA 2473146A CA 2473146 A CA2473146 A CA 2473146A CA 2473146 C CA2473146 C CA 2473146C
Authority
CA
Canada
Prior art keywords
gaseous
molecular sieve
attapulgite
binder
feed stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CA2473146A
Other languages
English (en)
French (fr)
Other versions
CA2473146A1 (en
Inventor
Dave Jaussaud
Kerry Weston
Armin Pfenninger
Beat Kleeb
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zeochem LLC
Original Assignee
Zeochem LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=27609134&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2473146(C) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Zeochem LLC filed Critical Zeochem LLC
Publication of CA2473146A1 publication Critical patent/CA2473146A1/en
Application granted granted Critical
Publication of CA2473146C publication Critical patent/CA2473146C/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/18Synthetic zeolitic molecular sieves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/18Synthetic zeolitic molecular sieves
    • B01J20/183Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/106Silica or silicates
    • B01D2253/108Zeolites
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02CCAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00Capture or disposal of greenhouse gases
    • Y02C20/40Capture or disposal of greenhouse gases of CO2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Polyesters Or Polycarbonates (AREA)
CA2473146A 2002-01-22 2003-01-22 Process for production of molecular sieve adsorbent blends and process for production thereof Expired - Lifetime CA2473146C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/054,041 US6743745B2 (en) 2002-01-22 2002-01-22 Process for production of molecular sieve adsorbent blends
US10/054,041 2002-01-22
PCT/US2003/001863 WO2003061820A2 (en) 2002-01-22 2003-01-22 Process for production of molecular sieve adsorbent blends

Publications (2)

Publication Number Publication Date
CA2473146A1 CA2473146A1 (en) 2003-07-31
CA2473146C true CA2473146C (en) 2011-09-06

Family

ID=27609134

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2473146A Expired - Lifetime CA2473146C (en) 2002-01-22 2003-01-22 Process for production of molecular sieve adsorbent blends and process for production thereof

Country Status (13)

Country Link
US (2) US6743745B2 (zh)
EP (1) EP1467811B1 (zh)
JP (1) JP4244808B2 (zh)
KR (1) KR100931440B1 (zh)
CN (1) CN1281307C (zh)
AT (1) ATE438461T1 (zh)
AU (1) AU2003205275A1 (zh)
BR (1) BR0307063B1 (zh)
CA (1) CA2473146C (zh)
DE (1) DE60328659D1 (zh)
MX (1) MXPA04006944A (zh)
WO (1) WO2003061820A2 (zh)
ZA (1) ZA200405704B (zh)

Families Citing this family (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6743745B2 (en) * 2002-01-22 2004-06-01 Zeochem Process for production of molecular sieve adsorbent blends
US7300899B2 (en) * 2002-01-22 2007-11-27 Zeochem, Llc Lithium exchanged zeolite X adsorbent blends
US20050119112A1 (en) * 2002-01-22 2005-06-02 Zeochem, Llc Process for production of molecular sieve adsorbent blends
FR2850963B1 (fr) * 2003-02-11 2005-03-25 Ceca Sa Adsorbants agglomeres, leur procede de preparation et leur utilisation pour le sechage de composes organiques
EP1468731B1 (de) * 2003-04-14 2011-09-28 Zeochem AG Verfahren zur Herstellung von verformten Zeolithen und Verfahren zur Entfernung von Verunreinigungen aus einem Gasstrom
US7442233B2 (en) * 2005-07-06 2008-10-28 Basf Catalysts Llc Integrated heavy hydrocarbon removal, amine treating and dehydration
EP1922132A4 (en) 2005-07-26 2009-09-02 Exxonmobil Upstream Res Co METHOD FOR CLEANING HYDROCARBONS AND REGENERATING ADSORPTIONS USED THEREOF
US7396387B2 (en) * 2005-11-01 2008-07-08 Praxair Technology, Inc. Pressure swing adsorption process for large capacity oxygen production
US7763100B2 (en) * 2006-07-06 2010-07-27 Praxair Technology, Inc. Vacuum pressure swing adsorption process and enhanced oxygen recovery
US20080011163A1 (en) * 2006-07-17 2008-01-17 Mcclain Michael S Sorbent porous polymeric composite materials
EP2117699B1 (en) * 2007-03-08 2019-10-09 Praxair Technology, Inc. High rate and high crush-strength adsorbents
US7781372B2 (en) * 2007-07-31 2010-08-24 GE02 Technologies, Inc. Fiber-based ceramic substrate and method of fabricating the same
US7855163B2 (en) * 2007-05-14 2010-12-21 Geo2 Technologies, Inc. Low coefficient of thermal expansion bonding system for a high porosity ceramic body and methods of manufacture
DE102008046155B4 (de) 2008-03-03 2017-01-26 Chemiewerk Bad Köstritz GmbH Verfahren zur Herstellung eines Adsorptionsmittelgranulates
EP2297111B1 (de) 2008-05-02 2012-06-20 Basf Se Verfahren zur herstellung halogensubstituierter 2-(aminomethyliden)-3-oxobuttersäureester
CN102639229A (zh) * 2009-09-28 2012-08-15 熊海山 吸附合成物及其方法
US20110275877A1 (en) * 2010-05-07 2011-11-10 Exxonmobil Research And Engineering Company Separation of Normal Paraffins from Isoparaffins Using Rapid Cycle Pressure Swing Adsorption
DE102011104006A1 (de) 2010-12-10 2012-06-14 Süd-Chemie AG Granulierte Zeolithe mit hoher Adsorptionskapazität zur Adsorption von organischen Molekülen
US8551217B2 (en) 2011-01-11 2013-10-08 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8435328B2 (en) 2011-01-11 2013-05-07 Praxair Technology, Inc. Ten bed pressure swing adsorption process operating in normal and turndown modes
US8496733B2 (en) 2011-01-11 2013-07-30 Praxair Technology, Inc. Large scale pressure swing adsorption systems having process cycles operating in normal and turndown modes
US8491704B2 (en) 2011-01-11 2013-07-23 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8680344B2 (en) 2011-01-25 2014-03-25 Zeochem Llc Molecular sieve adsorbent blends and uses thereof
FR2973809B1 (fr) * 2011-04-08 2015-11-13 Ceca Sa Utilisation de zeolithes pour la stabilisation d'huiles
FR2973717B1 (fr) 2011-04-08 2013-03-29 Ceca Sa Procede de reduction de l'acidite totale de compositions frigorigenes
KR101203258B1 (ko) 2011-07-05 2012-11-21 한국화학연구원 BaX형 제올라이트 성형체 및 그의 제조방법
CN102397776B (zh) * 2011-10-24 2013-08-07 张彩云 一种控制吸附速率分子筛的生产方法
CN102580669A (zh) * 2012-01-12 2012-07-18 太原理工大学 一种空分制氧沸石吸附剂的制备方法
WO2014118054A1 (en) 2013-01-31 2014-08-07 Basf Se Stable spherical, porous metal-organic framework shaped bodies for gas storage and gas separation
KR20150112988A (ko) 2013-01-31 2015-10-07 바스프 에스이 고 패킹 밀도 및 조정가능한 기공 부피를 갖는 금속-유기 골격 압출물
FR3006608B1 (fr) * 2013-06-10 2021-01-01 Ifp Energies Now Adsorbant a base d'une zeolithe et d'une argile riche en silice et procede de purification de charges d'hydrocarbures contenant des molecules insaturees
CA2916159C (en) * 2013-06-20 2021-02-09 Zeochem Llc Molecular sieve adsorbent blends and uses thereof
CN103435498B (zh) * 2013-08-15 2015-04-15 江苏隆昌化工有限公司 一种用改型Cu-13X分子筛催化氨解氯化芳烃合成芳烃胺工艺
CN103435497B (zh) * 2013-08-15 2016-02-24 江苏隆昌化工有限公司 一种亚铜离子交换处理13x分子筛应用于芳烃氯化物氨解合成苯胺类化合物的方法
FR3024667B1 (fr) 2014-08-05 2022-01-14 Ceca Sa Adsorbants zeolithiques a faible taux de liant et a haute surface externe, leur procede de preparation et leurs utilisations
FR3025789B1 (fr) 2014-09-12 2018-04-20 Arkema France Agregats de nanocristaux de zeolithes
US10099201B1 (en) 2015-02-05 2018-10-16 Zeochem Llc Zeolite agglomerates with a halloysite clay binder
FR3038240B1 (fr) 2015-07-02 2019-08-09 Arkema France Article comprenant des particules zeolitiques reliees par une resine
KR102038760B1 (ko) * 2015-09-23 2019-10-30 유오피 엘엘씨 낮은 반응성 흡착제를 이용한 탄화수소 스트림의 정제 방법
WO2017089410A1 (en) 2015-11-27 2017-06-01 Basf Se Ultrafast high space-time-yield synthesis of metal-organic frameworks
CN109485058A (zh) * 2018-12-11 2019-03-19 中国地质科学院郑州矿产综合利用研究所 一种无粘结剂lsx分子筛的制备方法
FR3103393B1 (fr) 2019-11-27 2022-07-01 Arkema France Séparation des gaz de l’air
CN111545163B (zh) * 2020-05-15 2024-02-02 河北省廊坊水文水资源勘测局(河北省廊坊水平衡测试中心) 一种用于重金属废水处理的吸附剂及制备方法
CN115477311B (zh) * 2022-09-27 2023-12-01 洛阳建龙微纳新材料股份有限公司 一种Ag/M-MSX分子筛脱氢剂及其制备方法和应用
CN115701829B (zh) * 2022-10-17 2023-12-15 大连理工大学 一种小孔分子筛成型吸附剂的制备方法及在吸附不饱和烃制备电子级笑气中的应用

Family Cites Families (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2973327A (en) 1955-07-01 1961-02-28 Union Carbide Corp Bonded molecular sieves
GB827043A (en) 1956-11-05 1960-02-03 Union Carbide Corp Improvements in and relating to bonded molecular sieves
US3049449A (en) * 1960-03-29 1962-08-14 Minerals & Chem Philipp Corp Lightweight adsorbent clay product and method of making same
US3219590A (en) 1961-08-01 1965-11-23 Union Carbide Corp Bonded molecular sieves
JPS5147926A (ja) 1974-10-22 1976-04-24 Kogyo Gijutsuin Setsuchakuhoho
US5288396A (en) * 1979-10-15 1994-02-22 Union Oil Company Of California Hydrocracking process using a catalyst selective for making middle distillates
JPS6025369B2 (ja) 1981-03-10 1985-06-18 水澤化学工業株式会社 耐摩耗性粒状ゼオライト及びその製法
JPH0674136B2 (ja) * 1986-06-03 1994-09-21 日本化学工業株式会社 ゼオライト成形体およびその製造法
FR2618085A1 (fr) 1987-07-17 1989-01-20 Rhone Poulenc Chimie Adsorbant pour la purification des gaz et procede de purification
US5292360A (en) 1987-07-17 1994-03-08 Rhone-Poulenc Chimie 5A zeolite/kaolinite adsorbent for gas purification
FR2669242B1 (fr) 1990-11-16 1994-09-02 Ceca Sa Adsorbants industriels a base de zeolites x a basse teneur en silice pour la separation non cryogenique des gaz de l'air et leur procede de preparation.
ATE130831T1 (de) 1991-01-07 1995-12-15 Takeda Chemical Industries Ltd Verfahren zur formgebung und zum brennen von zeolith-pulver.
DE4202671A1 (de) 1991-05-27 1992-12-03 Degussa Formkoerper enthaltend dealuminierten zeolith y und das verfahren zu ihrer herstellung
JPH05147926A (ja) 1991-11-28 1993-06-15 Tosoh Corp 3a型ゼオライト成形体の製造方法
FR2678525B3 (fr) 1992-07-06 1994-10-07 Bitterfeld Wolfen Chemie Agent d'adsorption a base de tamis moleculaire pour la purification du gaz naturel, des composes sulfures.
US5413978A (en) * 1993-11-30 1995-05-09 Engelhard Corporation Catalytically inert particles for blending with petroleum cracking catalyst
US5493821A (en) * 1994-05-04 1996-02-27 Uop Adsorbent for use in double glazed windows
US5948726A (en) 1994-12-07 1999-09-07 Project Earth Industries, Inc. Adsorbent and/or catalyst and binder system and method of making therefor
DE69708790T2 (de) 1996-08-30 2002-08-08 Tosoh Corp Wärmebeständiges Zeolith mit niedrigem Kieselsäuregehalt und Verfahren zu dessen Herstellung und Verwendung
US5883034A (en) * 1997-07-09 1999-03-16 Phillips Petroleum Company Hydrocarbon conversion catalyst composition and processes therefor and therewith
JP4320797B2 (ja) 1998-03-04 2009-08-26 東ソー株式会社 A型ゼオライトビーズ成形体及びその製造方法
US6171370B1 (en) 1998-03-04 2001-01-09 Tosoh Corporation Adsorbent for separating gases
JPH11335117A (ja) * 1998-05-26 1999-12-07 Tosoh Corp 冷凍サイクル用乾燥剤及びその製造方法
US6183539B1 (en) 1998-07-01 2001-02-06 Zeochem Co. Molecular sieve adsorbent for gas purification and preparation thereof
US6444601B1 (en) * 1998-11-12 2002-09-03 Itc, Inc. Purified attapulgite clay
US6130179A (en) 1998-11-12 2000-10-10 Itc, Inc. Purified attapulgite clay
JP2000211915A (ja) * 1998-11-16 2000-08-02 Tosoh Corp 低シリカx型ゼオライト含有成形体及びその製造方法並びにその用途
WO2000034217A1 (en) * 1998-12-10 2000-06-15 Bp Chemicals Limited A method of dewatering organic liquids
US6543385B2 (en) * 2000-12-07 2003-04-08 Nestec, Ltd. Animal litter composition containing silica gel and methods therefor
US6743745B2 (en) * 2002-01-22 2004-06-01 Zeochem Process for production of molecular sieve adsorbent blends

Also Published As

Publication number Publication date
US20030171205A1 (en) 2003-09-11
JP2005515876A (ja) 2005-06-02
BR0307063B1 (pt) 2013-05-28
CA2473146A1 (en) 2003-07-31
ATE438461T1 (de) 2009-08-15
US6743745B2 (en) 2004-06-01
CN1281307C (zh) 2006-10-25
US6918948B2 (en) 2005-07-19
AU2003205275A1 (en) 2003-09-02
JP4244808B2 (ja) 2009-03-25
BR0307063A (pt) 2004-12-28
MXPA04006944A (es) 2004-12-06
US20040156766A1 (en) 2004-08-12
EP1467811B1 (en) 2009-08-05
KR20040075097A (ko) 2004-08-26
KR100931440B1 (ko) 2009-12-11
WO2003061820A3 (en) 2003-08-28
EP1467811A2 (en) 2004-10-20
DE60328659D1 (de) 2009-09-17
ZA200405704B (en) 2005-09-28
WO2003061820A2 (en) 2003-07-31
CN1638861A (zh) 2005-07-13

Similar Documents

Publication Publication Date Title
CA2473146C (en) Process for production of molecular sieve adsorbent blends and process for production thereof
US7300899B2 (en) Lithium exchanged zeolite X adsorbent blends
JP2005515876A6 (ja) モレキュラーシーブ吸着剤ブレンドの製造方法
US20050119112A1 (en) Process for production of molecular sieve adsorbent blends
CA2336321C (en) Molecular sieve adsorbent for gas purification and preparation thereof
US8680344B2 (en) Molecular sieve adsorbent blends and uses thereof
EP0940174B1 (en) Adsorbent for separating gases
US8969633B2 (en) Molecular sieve adsorbent blends and uses thereof
US8123835B2 (en) High rate and high crush-strength adsorbents
KR101203258B1 (ko) BaX형 제올라이트 성형체 및 그의 제조방법
RU2745299C1 (ru) Высококачественные композитные адсорбенты с компонентом типа "ядро в оболочке" для систем vsa/vpsa/psa
KR101005396B1 (ko) 변형된 제올라이트의 제조 방법 및 기체 흐름으로부터불순물의 제거 방법
JP3799678B2 (ja) 高強度低摩耗性ゼオライト粒状物、その製造方法及びそれを用いた吸着分離方法
US20140323289A1 (en) Zeolitic adsorbents for use in adsorptive separation processes and methods for manufacturing the same
JPH11314913A (ja) 高強度低摩耗性ゼオライト粒状物及びその製造方法
MXPA00012790A (en) Molecular sieve adsorbent for gas purification and preparation thereof

Legal Events

Date Code Title Description
EEER Examination request
MKEX Expiry

Effective date: 20230123