CA2064655C - Process for preparing detergent compositions - Google Patents
Process for preparing detergent compositionsInfo
- Publication number
- CA2064655C CA2064655C CA002064655A CA2064655A CA2064655C CA 2064655 C CA2064655 C CA 2064655C CA 002064655 A CA002064655 A CA 002064655A CA 2064655 A CA2064655 A CA 2064655A CA 2064655 C CA2064655 C CA 2064655C
- Authority
- CA
- Canada
- Prior art keywords
- surfactant
- nonionic
- anionic
- liquid
- process according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 49
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 5
- 239000003599 detergent Substances 0.000 title description 16
- 239000007788 liquid Substances 0.000 claims abstract description 34
- 238000000034 method Methods 0.000 claims abstract description 29
- 239000004094 surface-active agent Substances 0.000 claims abstract description 28
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 27
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 24
- 239000002253 acid Substances 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002243 precursor Substances 0.000 claims abstract description 14
- -1 alkyl sulphate Chemical compound 0.000 claims abstract description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 10
- 229910021653 sulphate ion Inorganic materials 0.000 claims abstract description 8
- 150000004996 alkyl benzenes Chemical group 0.000 claims description 5
- 150000002191 fatty alcohols Chemical class 0.000 claims description 5
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 2
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 claims 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 24
- 125000000129 anionic group Chemical group 0.000 description 11
- 229920001983 poloxamer Polymers 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- 125000004432 carbon atom Chemical group C* 0.000 description 5
- 238000006386 neutralization reaction Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- QTDIEDOANJISNP-UHFFFAOYSA-N 2-dodecoxyethyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOCCOS(O)(=O)=O QTDIEDOANJISNP-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 239000002826 coolant Substances 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 239000011552 falling film Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 206010013710 Drug interaction Diseases 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000012683 anionic precursor Substances 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004851 dishwashing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB919107092A GB9107092D0 (en) | 1991-04-04 | 1991-04-04 | Process for preparing detergent compositions |
| GB9107092.0 | 1991-04-04 | ||
| IN111BO1992 IN173189B (ko) | 1991-04-04 | 1992-04-03 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2064655A1 CA2064655A1 (en) | 1992-10-05 |
| CA2064655C true CA2064655C (en) | 1996-12-10 |
Family
ID=26298685
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002064655A Expired - Fee Related CA2064655C (en) | 1991-04-04 | 1992-04-01 | Process for preparing detergent compositions |
Country Status (11)
| Country | Link |
|---|---|
| EP (1) | EP0507402B1 (ko) |
| JP (1) | JPH0778234B2 (ko) |
| KR (1) | KR950013226B1 (ko) |
| AU (1) | AU652812B2 (ko) |
| BR (1) | BR9201203A (ko) |
| CA (1) | CA2064655C (ko) |
| DE (1) | DE69228330T2 (ko) |
| ES (1) | ES2127202T3 (ko) |
| GB (1) | GB9107092D0 (ko) |
| IN (1) | IN173189B (ko) |
| ZA (1) | ZA922465B (ko) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9324129D0 (en) * | 1993-11-24 | 1994-01-12 | Unilever Plc | Detergent compositions and process for preparing them |
| JPH09505349A (ja) * | 1993-11-24 | 1997-05-27 | ユニリーバー・ナームローゼ・ベンノートシヤープ | 洗剤組成物 |
| TW326472B (en) * | 1994-08-12 | 1998-02-11 | Kao Corp | Method for producing nonionic detergent granules |
| DE19529232A1 (de) * | 1995-08-09 | 1997-02-13 | Henkel Kgaa | Verfahren zur Herstellung von Tensidzusammensetzungen |
| GB9618877D0 (en) * | 1996-09-10 | 1996-10-23 | Unilever Plc | Process for preparing high bulk density detergent compositions |
| GB9618875D0 (en) * | 1996-09-10 | 1996-10-23 | Unilever Plc | Process for preparing high bulk density detergent compositions |
| DE19844523A1 (de) | 1998-09-29 | 2000-03-30 | Henkel Kgaa | Granulationsverfahren |
| GB0009087D0 (en) | 2000-04-12 | 2000-05-31 | Unilever Plc | Process for preparing fluid detergent compositions |
| DE10163603B4 (de) | 2001-12-21 | 2006-05-04 | Henkel Kgaa | Verfahren zur Herstellung builderhaltiger Tensidgranulate |
| DE102004025859A1 (de) * | 2004-05-24 | 2005-12-22 | Henkel Kgaa | Kit aus Schwamm und Reiniger |
| EP2130897B1 (en) * | 2008-06-02 | 2011-08-31 | The Procter & Gamble Company | Surfactant concentrate |
| JP5875226B2 (ja) * | 2010-12-28 | 2016-03-02 | 花王株式会社 | 界面活性剤組成物 |
| JP5868747B2 (ja) * | 2012-03-19 | 2016-02-24 | 花王株式会社 | 界面活性剤混合物の製造方法 |
| DE102012221360A1 (de) * | 2012-11-22 | 2014-05-22 | Henkel Ag & Co. Kgaa | Kontinuierliches Verfahren zur Herstellung von flüssigen Wasch- oder Reinigungsmitteln |
| MX2016003051A (es) * | 2013-09-09 | 2016-06-10 | Procter & Gamble | Proceso para elaborar una composicion liquida de limpieza. |
| DE102015212131A1 (de) * | 2015-06-30 | 2017-01-05 | Henkel Ag & Co. Kgaa | Verfahren zur Herstellung einer flüssigen, Tensid enthaltenden Zusammensetzung |
| CN105062705A (zh) * | 2015-08-14 | 2015-11-18 | 浙江赞宇科技股份有限公司 | 一种无水乙氧基化烷基硫酸盐浓缩物及其制备方法与装置 |
| US11352468B2 (en) | 2016-04-18 | 2022-06-07 | Monosol, Llc | Perfume microcapsules and related film and detergent compositions |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2232341A1 (de) * | 1972-07-01 | 1974-01-17 | Orthmann & Herbst | Vorrichtung zur kontinuierlichen neutralisation von saeure- oder laugehaltigen abwaessern |
| JPS5278828A (en) * | 1975-12-26 | 1977-07-02 | Lion Corp | Preparation of high concentration olefin sulfonate solution |
| EP0043148A1 (de) * | 1980-06-27 | 1982-01-06 | Joseph Hanssens | Wasserenteisenungsanlage |
| JPS6032676B2 (ja) * | 1980-07-11 | 1985-07-29 | ライオン株式会社 | 高濃度界面活性剤スラリ− |
| DE3305430A1 (de) * | 1983-02-17 | 1984-08-23 | Henkel KGaA, 4000 Düsseldorf | Verwendung von alkoholen und deren derivaten als viskositaetsregler fuer hochviskose technische tensid-konzentrate |
| GB8625104D0 (en) * | 1986-10-20 | 1986-11-26 | Unilever Plc | Detergent compositions |
| JPS6447755A (en) * | 1987-08-18 | 1989-02-22 | Dai Ichi Kogyo Seiyaku Co Ltd | Production of organic sulfuric acid ester salt or organic sulfonic acid salt |
| JPH02105900A (ja) * | 1988-10-15 | 1990-04-18 | Sunstar Inc | 容器入洗剤組成物 |
| JP2589365B2 (ja) * | 1989-02-21 | 1997-03-12 | 花王株式会社 | アルキル硫酸エステル塩の製造方法 |
-
1991
- 1991-04-04 GB GB919107092A patent/GB9107092D0/en active Pending
-
1992
- 1992-03-30 DE DE69228330T patent/DE69228330T2/de not_active Expired - Fee Related
- 1992-03-30 EP EP92200908A patent/EP0507402B1/en not_active Revoked
- 1992-03-30 ES ES92200908T patent/ES2127202T3/es not_active Expired - Lifetime
- 1992-04-01 CA CA002064655A patent/CA2064655C/en not_active Expired - Fee Related
- 1992-04-03 ZA ZA922465A patent/ZA922465B/xx unknown
- 1992-04-03 BR BR929201203A patent/BR9201203A/pt not_active IP Right Cessation
- 1992-04-03 JP JP4082499A patent/JPH0778234B2/ja not_active Expired - Lifetime
- 1992-04-03 AU AU14053/92A patent/AU652812B2/en not_active Ceased
- 1992-04-03 IN IN111BO1992 patent/IN173189B/en unknown
- 1992-04-04 KR KR92005631A patent/KR950013226B1/ko not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| BR9201203A (pt) | 1992-12-01 |
| DE69228330T2 (de) | 1999-06-17 |
| EP0507402A1 (en) | 1992-10-07 |
| GB9107092D0 (en) | 1991-05-22 |
| AU652812B2 (en) | 1994-09-08 |
| KR920019919A (ko) | 1992-11-20 |
| DE69228330D1 (de) | 1999-03-18 |
| ES2127202T3 (es) | 1999-04-16 |
| JPH0778234B2 (ja) | 1995-08-23 |
| ZA922465B (en) | 1993-10-04 |
| AU1405392A (en) | 1992-10-08 |
| EP0507402B1 (en) | 1999-02-03 |
| IN173189B (ko) | 1994-02-26 |
| KR950013226B1 (en) | 1995-10-26 |
| CA2064655A1 (en) | 1992-10-05 |
| JPH05112797A (ja) | 1993-05-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |