CA2021527A1 - Catalyseur pour l'oxydation selective de composes sulfures en soufre elementaire; methode de preparation de ce catalyseur; methode pour l'oxydation selective de composes sulfures en soufre elementaire - Google Patents

Catalyseur pour l'oxydation selective de composes sulfures en soufre elementaire; methode de preparation de ce catalyseur; methode pour l'oxydation selective de composes sulfures en soufre elementaire

Info

Publication number
CA2021527A1
CA2021527A1 CA2021527A CA2021527A CA2021527A1 CA 2021527 A1 CA2021527 A1 CA 2021527A1 CA 2021527 A CA2021527 A CA 2021527A CA 2021527 A CA2021527 A CA 2021527A CA 2021527 A1 CA2021527 A1 CA 2021527A1
Authority
CA
Canada
Prior art keywords
sulphur
catalyst
selective oxidation
elemental
compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2021527A
Other languages
English (en)
Other versions
CA2021527C (fr
Inventor
Peter John Van Den Brink
John Wilhelm Geus
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Worley Nederland BV
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2021527A1 publication Critical patent/CA2021527A1/fr
Application granted granted Critical
Publication of CA2021527C publication Critical patent/CA2021527C/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/86—Catalytic processes
    • B01D53/8603—Removing sulfur compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/86—Catalytic processes
    • B01D53/8603—Removing sulfur compounds
    • B01D53/8612—Hydrogen sulfide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/86—Chromium
    • B01J23/862—Iron and chromium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/185—Phosphorus; Compounds thereof with iron group metals or platinum group metals
    • B01J27/1853—Phosphorus; Compounds thereof with iron group metals or platinum group metals with iron, cobalt or nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/188—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with chromium, molybdenum, tungsten or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/02—Preparation of sulfur; Purification
    • C01B17/04—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides
    • C01B17/0404—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides by processes comprising a dry catalytic conversion of hydrogen sulfide-containing gases, e.g. the Claus process
    • C01B17/046—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides by processes comprising a dry catalytic conversion of hydrogen sulfide-containing gases, e.g. the Claus process without intermediate formation of sulfur dioxide
    • C01B17/0465—Catalyst compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/647—2-50 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/651—50-500 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Exhaust Gas After Treatment (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
CA002021527A 1989-07-21 1990-07-19 Catalyseur pour l'oxydation selective de composes sulfures en soufre elementaire; methode de preparation de ce catalyseur; methode pour l'oxydation selective de composes sulfures en soufre elementaire Expired - Lifetime CA2021527C (fr)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
NL8901893 1989-07-21
NL8901893A NL8901893A (nl) 1989-07-21 1989-07-21 Katalysator voor de selectieve oxidatie van zwavelverbindingen tot elementaire zwavel, werkwijze voor de bereiding van een dergelijke katalysator en werkwijze voor de selectieve oxidatie van zwavelverbindingen tot elementaire zwavel.
NL8902690 1989-10-31
NL8902690A NL8902690A (nl) 1989-07-21 1989-10-31 Katalysator voor de selectieve oxidatie van zwavelverbindingen tot elementaire zwavel, werkwijze voor de bereiding van een dergelijke katalysator en werkwijze voor de selectieve oxidatie van zwavelverbindingen tot elementaire zwavel.

Publications (2)

Publication Number Publication Date
CA2021527A1 true CA2021527A1 (fr) 1991-01-22
CA2021527C CA2021527C (fr) 2000-09-19

Family

ID=26646560

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002021527A Expired - Lifetime CA2021527C (fr) 1989-07-21 1990-07-19 Catalyseur pour l'oxydation selective de composes sulfures en soufre elementaire; methode de preparation de ce catalyseur; methode pour l'oxydation selective de composes sulfures en soufre elementaire

Country Status (26)

Country Link
US (2) US5286697A (fr)
EP (1) EP0409353B1 (fr)
JP (1) JP3037976B2 (fr)
KR (1) KR910002508A (fr)
CN (2) CN1032802C (fr)
AT (1) ATE128643T1 (fr)
AU (1) AU628195B2 (fr)
BR (1) BR9003526A (fr)
CA (1) CA2021527C (fr)
CZ (1) CZ285068B6 (fr)
DD (1) DD300080A5 (fr)
DE (1) DE69022790T2 (fr)
DK (1) DK0409353T3 (fr)
ES (1) ES2080103T3 (fr)
FI (1) FI102250B (fr)
GR (1) GR3017655T3 (fr)
HU (1) HU213040B (fr)
MX (1) MX171189B (fr)
NL (2) NL8901893A (fr)
NO (1) NO302020B1 (fr)
PL (1) PL166060B1 (fr)
PT (1) PT94783B (fr)
RU (1) RU2070089C1 (fr)
SG (1) SG49116A1 (fr)
SK (1) SK363090A3 (fr)
ZA (1) ZA905622B (fr)

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FI119915B2 (fi) * 2003-10-03 2011-06-15 Metsae Botnia Ab Oy Rikin poisto sellutehtaan hajukaasuista
CN1921943A (zh) * 2004-01-20 2007-02-28 国际壳牌研究有限公司 恢复失效加氢处理催化剂的催化活性的方法、所得恢复的催化剂及加氢处理方法
US7727507B2 (en) 2005-03-30 2010-06-01 Shell Oil Company Process for producing a gas stream depleted of hydrogen sulphide
DE602006009488D1 (de) 2005-03-31 2009-11-12 Shell Int Research Verfahren zur herstellung eines schwefelzementprodukts
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WO2007145676A1 (fr) * 2006-01-17 2007-12-21 Exxonmobil Research And Engineering Company Procédé de fabrication de corps en forme en silice
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EA014521B1 (ru) 2006-10-05 2010-12-30 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Способ удаления меркаптанов
CN102227251B (zh) 2008-11-28 2014-08-27 国际壳牌研究有限公司 生产纯化天然气的方法
EP2408852A1 (fr) * 2009-03-17 2012-01-25 T.D.E. Recovery Technologies Ltd. Procede ecologique pour l'utilisation de produits de pyrolyse
US20100240135A1 (en) * 2009-03-19 2010-09-23 Seeger David M System and method for sour gas well testing
CN101653688B (zh) * 2009-06-24 2013-07-10 成都华西工业气体有限公司 一种混合气脱除co2、h2s的工艺流程
IN2014KN02582A (fr) 2012-04-23 2015-05-08 Repsol Sa
CN102744077B (zh) * 2012-07-13 2014-03-12 浙江大学 一种烧结金属纤维束催化剂的制备方法、催化剂及装置
US9205364B2 (en) * 2013-06-21 2015-12-08 Phillips 66 Company Process for in-situ production of low dissolved hydrogen sulfide, degassed, sulfur from Claus sulfur recovery
CN105347311B (zh) * 2015-11-23 2018-05-08 山东迅达化工集团有限公司 H2s选择性氧化生成单质硫的工艺方法
RU2629193C1 (ru) * 2016-07-11 2017-08-25 Акционерное общество "Специальное конструкторско-технологическое бюро "Катализатор" Катализатор для селективного окисления сероводорода (варианты)
WO2018013009A1 (fr) * 2016-07-11 2018-01-18 Акционерное общество "Специальное конструкторско-технологическое бюро "Катализатор" Catalyseur d'oxydation sélective de sulfure d'hydrogène (et variantes) et différents processus l'utilisant
NL2017178B1 (en) 2016-07-15 2018-01-18 Jacobs Nederland Bv Selective oxidation of hydrogen sulfide
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ES2080103T3 (es) 1996-02-01
NO903255L (no) 1991-01-22
CN1032802C (zh) 1996-09-18
CN1062832C (zh) 2001-03-07
NO302020B1 (no) 1998-01-12
NL8902690A (nl) 1991-05-16
CZ363090A3 (cs) 1999-02-17
NL8901893A (nl) 1991-02-18
SK280795B6 (sk) 2000-07-11
FI102250B1 (fi) 1998-11-13
GR3017655T3 (en) 1996-01-31
SK363090A3 (en) 2000-07-11
NO903255D0 (no) 1990-07-20
EP0409353B1 (fr) 1995-10-04
DE69022790T2 (de) 1996-03-14
DD300080A5 (de) 1992-05-21
KR910002508A (ko) 1991-02-25
JP3037976B2 (ja) 2000-05-08
CN1049320A (zh) 1991-02-20
DK0409353T3 (da) 1996-02-05
JPH03150210A (ja) 1991-06-26
SG49116A1 (en) 1998-05-18
RU2070089C1 (ru) 1996-12-10
AU628195B2 (en) 1992-09-10
CZ285068B6 (cs) 1999-05-12
HUT54311A (en) 1991-02-28
US5286697A (en) 1994-02-15
CN1153136A (zh) 1997-07-02
AU5911490A (en) 1991-01-24
HU904559D0 (en) 1990-12-28
PT94783B (pt) 1997-04-30
ATE128643T1 (de) 1995-10-15
CA2021527C (fr) 2000-09-19
EP0409353A1 (fr) 1991-01-23
BR9003526A (pt) 1991-08-27
HU213040B (en) 1997-01-28
DE69022790D1 (de) 1995-11-09
ZA905622B (en) 1991-06-26
MX171189B (es) 1993-10-06
PT94783A (pt) 1991-03-20
PL286150A1 (en) 1991-04-22
FI102250B (fi) 1998-11-13
FI903673A0 (fi) 1990-07-20
US5352422A (en) 1994-10-04
PL166060B1 (pl) 1995-03-31

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