BRPI0710332A2 - processo para a preparação de um copolioxadiazol randÈmico - Google Patents
processo para a preparação de um copolioxadiazol randÈmico Download PDFInfo
- Publication number
- BRPI0710332A2 BRPI0710332A2 BRPI0710332-8A BRPI0710332A BRPI0710332A2 BR PI0710332 A2 BRPI0710332 A2 BR PI0710332A2 BR PI0710332 A BRPI0710332 A BR PI0710332A BR PI0710332 A2 BRPI0710332 A2 BR PI0710332A2
- Authority
- BR
- Brazil
- Prior art keywords
- process according
- acid
- oil
- hydrazine
- oriented aromatic
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims abstract description 24
- FUSNOPLQVRUIIM-UHFFFAOYSA-N 4-amino-2-(4,4-dimethyl-2-oxoimidazolidin-1-yl)-n-[3-(trifluoromethyl)phenyl]pyrimidine-5-carboxamide Chemical compound O=C1NC(C)(C)CN1C(N=C1N)=NC=C1C(=O)NC1=CC=CC(C(F)(F)F)=C1 FUSNOPLQVRUIIM-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000012493 hydrazine sulfate Substances 0.000 claims abstract description 7
- 229910000377 hydrazine sulfate Inorganic materials 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims abstract description 4
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 claims abstract 4
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims description 38
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 33
- 125000003118 aryl group Chemical group 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 5
- 238000004090 dissolution Methods 0.000 claims description 4
- ZGCHATBSUIJLRL-UHFFFAOYSA-N hydrazine sulfate Chemical compound NN.OS(O)(=O)=O ZGCHATBSUIJLRL-UHFFFAOYSA-N 0.000 claims description 3
- WVDRSXGPQWNUBN-UHFFFAOYSA-N 4-(4-carboxyphenoxy)benzoic acid Chemical compound C1=CC(C(=O)O)=CC=C1OC1=CC=C(C(O)=O)C=C1 WVDRSXGPQWNUBN-UHFFFAOYSA-N 0.000 claims description 2
- NEQFBGHQPUXOFH-UHFFFAOYSA-N 4-(4-carboxyphenyl)benzoic acid Chemical compound C1=CC(C(=O)O)=CC=C1C1=CC=C(C(O)=O)C=C1 NEQFBGHQPUXOFH-UHFFFAOYSA-N 0.000 claims description 2
- RXOHFPCZGPKIRD-UHFFFAOYSA-N naphthalene-2,6-dicarboxylic acid Chemical compound C1=C(C(O)=O)C=CC2=CC(C(=O)O)=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-N 0.000 claims description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims 2
- SBBQDUFLZGOASY-OWOJBTEDSA-N 4-[(e)-2-(4-carboxyphenyl)ethenyl]benzoic acid Chemical compound C1=CC(C(=O)O)=CC=C1\C=C\C1=CC=C(C(O)=O)C=C1 SBBQDUFLZGOASY-OWOJBTEDSA-N 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 abstract description 12
- 229920000642 polymer Polymers 0.000 description 11
- 238000007792 addition Methods 0.000 description 7
- 239000007787 solid Substances 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 150000001735 carboxylic acids Chemical class 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000009987 spinning Methods 0.000 description 2
- 150000005072 1,3,4-oxadiazoles Chemical class 0.000 description 1
- KEQGZUUPPQEDPF-UHFFFAOYSA-N 1,3-dichloro-5,5-dimethylimidazolidine-2,4-dione Chemical compound CC1(C)N(Cl)C(=O)N(Cl)C1=O KEQGZUUPPQEDPF-UHFFFAOYSA-N 0.000 description 1
- NWHZQELJCLSKNV-UHFFFAOYSA-N 4-[(4-carboxyphenyl)diazenyl]benzoic acid Chemical compound C1=CC(C(=O)O)=CC=C1N=NC1=CC=C(C(O)=O)C=C1 NWHZQELJCLSKNV-UHFFFAOYSA-N 0.000 description 1
- DBLJAFVPFHRQSP-UHFFFAOYSA-N aminoazanium;sulfate Chemical compound NN.NN.OS(O)(=O)=O DBLJAFVPFHRQSP-UHFFFAOYSA-N 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- XTHPWXDJESJLNJ-UHFFFAOYSA-N chlorosulfonic acid Substances OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 231100000584 environmental toxicity Toxicity 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229940042795 hydrazides for tuberculosis treatment Drugs 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000008247 solid mixture Substances 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/08—Polyhydrazides; Polytriazoles; Polyaminotriazoles; Polyoxadiazoles
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
- C08G73/22—Polybenzoxazoles
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Polyamides (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/414,959 | 2006-05-01 | ||
| US11/414,959 US7582721B2 (en) | 2006-05-01 | 2006-05-01 | Two step preparation of random polyoxadiazole copolymer and articles resulting therefrom |
| PCT/US2007/010028 WO2007133408A2 (en) | 2006-05-01 | 2007-04-26 | Two step preparation of random polyoxadiazole copolymer and articles resulting therefrom |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BRPI0710332A2 true BRPI0710332A2 (pt) | 2011-08-09 |
Family
ID=38578537
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BRPI0710332-8A BRPI0710332A2 (pt) | 2006-05-01 | 2007-04-26 | processo para a preparação de um copolioxadiazol randÈmico |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US7582721B2 (enExample) |
| EP (1) | EP2013262B1 (enExample) |
| JP (1) | JP5036806B2 (enExample) |
| KR (1) | KR101415409B1 (enExample) |
| CN (1) | CN101437871B (enExample) |
| BR (1) | BRPI0710332A2 (enExample) |
| CA (1) | CA2648733C (enExample) |
| MX (1) | MX2008013839A (enExample) |
| WO (1) | WO2007133408A2 (enExample) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7528217B2 (en) | 2006-10-06 | 2009-05-05 | E.I. Du Pont De Nemours And Company | Polymers and fibers formed therefrom |
| CN103261275A (zh) * | 2010-12-16 | 2013-08-21 | 纳幕尔杜邦公司 | 磺化的聚噁二唑聚合物的制备 |
| WO2012082434A1 (en) | 2010-12-16 | 2012-06-21 | E. I. Du Pont De Nemours And Company | Flame resistant spun staple yarns made from blends of fibers derived from sulfonated polyoxadiazole polymers |
| CN103261274A (zh) * | 2010-12-16 | 2013-08-21 | 纳幕尔杜邦公司 | 磺化聚噁二唑聚合物制品 |
| CN104508007B (zh) * | 2012-06-15 | 2019-07-23 | 纳幕尔杜邦公司 | 磺化萘聚噁二唑聚合物 |
| US9150693B2 (en) | 2012-06-15 | 2015-10-06 | E I Du Pont De Nemours And Company | Preparation of sulfonated naphthalene polyoxadiazoles polymers |
| WO2013188328A1 (en) | 2012-06-15 | 2013-12-19 | E. I. Du Pont De Nemours And Company | Sulfonated polyoxadiazole polymers articles |
| JP6112683B2 (ja) | 2012-06-15 | 2017-04-12 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ | スルホン化ナフタレンポリオキサジアゾールポリマーより得られる繊維のブレンドから製造された難燃性紡績短繊維ヤーン |
| CN109401307A (zh) * | 2018-09-29 | 2019-03-01 | 刘文熙 | 一种高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109401308A (zh) * | 2018-09-29 | 2019-03-01 | 潘鑫 | 一种高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109280380A (zh) * | 2018-09-29 | 2019-01-29 | 刘文熙 | 一种高强度高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109280382A (zh) * | 2018-09-29 | 2019-01-29 | 王庭辉 | 一种耐紫外线高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293894A (zh) * | 2018-09-29 | 2019-02-01 | 王庭辉 | 一种高强度耐紫外线的芳杂环聚合物薄膜及其制备方法和应用 |
| CN109306182A (zh) * | 2018-09-29 | 2019-02-05 | 刘文熙 | 一种高强度高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109280381A (zh) * | 2018-09-29 | 2019-01-29 | 王庭辉 | 一种阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109306180A (zh) * | 2018-09-29 | 2019-02-05 | 王庭辉 | 一种高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109280384A (zh) * | 2018-09-29 | 2019-01-29 | 潘鑫 | 一种高强度耐紫外线高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109320924A (zh) * | 2018-09-29 | 2019-02-12 | 刘文熙 | 一种高强度耐紫外线阻燃的芳杂环聚合物薄膜及其制备方法和应用 |
| CN109280383A (zh) * | 2018-09-29 | 2019-01-29 | 刘文熙 | 一种高强度耐紫外线高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109401305A (zh) * | 2018-09-29 | 2019-03-01 | 刘文熙 | 一种耐紫外线的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109337049A (zh) * | 2018-09-29 | 2019-02-15 | 潘鑫 | 一种高强度耐紫外线高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109337048A (zh) * | 2018-09-29 | 2019-02-15 | 潘鑫 | 一种高强度耐紫外线的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109306181A (zh) * | 2018-09-29 | 2019-02-05 | 刘文熙 | 一种耐紫外线阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109320702A (zh) * | 2018-09-29 | 2019-02-12 | 王庭辉 | 一种高强度高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109337050A (zh) * | 2018-09-29 | 2019-02-15 | 潘鑫 | 一种高强度耐紫外线高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293891A (zh) * | 2018-09-29 | 2019-02-01 | 王庭辉 | 一种高强度的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293897A (zh) * | 2018-09-29 | 2019-02-01 | 王庭辉 | 一种高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293898A (zh) * | 2018-09-29 | 2019-02-01 | 潘鑫 | 一种耐紫外线高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293899A (zh) * | 2018-09-29 | 2019-02-01 | 潘鑫 | 一种高强度阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109306183A (zh) * | 2018-09-29 | 2019-02-05 | 王庭辉 | 一种高强度耐紫外线阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293893A (zh) * | 2018-09-29 | 2019-02-01 | 潘鑫 | 一种耐紫外线高透明的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109293896A (zh) * | 2018-09-29 | 2019-02-01 | 王庭辉 | 一种耐紫外线的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109320703A (zh) * | 2018-09-29 | 2019-02-12 | 刘文熙 | 一种耐紫外线阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109401306A (zh) * | 2018-09-29 | 2019-03-01 | 刘文熙 | 一种芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
| CN109401309A (zh) * | 2018-09-29 | 2019-03-01 | 刘文熙 | 一种耐紫外线高透明阻燃的芳杂环聚合物树脂及其制备方法和在纤维或薄膜的应用 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1977404A (en) * | 1931-07-29 | 1934-10-16 | George H Osgood | Vegetable protein glue |
| US1980420A (en) * | 1932-06-11 | 1934-11-13 | Westinghouse Air Brake Co | Locomotive brake equipment |
| US3642708A (en) * | 1967-02-22 | 1972-02-15 | Furukawa Electric Co Ltd | Oxadiazole-n-methylhydrazide copolymeric resin and a method of producing thereof |
| US3886251A (en) * | 1967-04-11 | 1975-05-27 | Furukawa Electric Co Ltd | Method for forming polyoxadiazole series resin solution into shaped articles |
| GB1252508A (enExample) * | 1968-10-23 | 1971-11-03 | ||
| CH545829A (enExample) | 1970-10-29 | 1974-02-15 | ||
| GB1339324A (en) * | 1971-02-02 | 1973-12-05 | Ici Ltd | Production of polyoxadiazole solutions |
| US4202962A (en) * | 1971-11-26 | 1980-05-13 | Monsanto Company | Fibers of arylene oxadiazole/arylene N-alkylhydrazide copolymer |
| BE791894A (fr) * | 1971-11-26 | 1973-05-24 | Monsanto Co | Procede de preparation de polymeres oxadiazole aromatique /hydrazide n-alkylique |
| JPS5110805B2 (enExample) * | 1972-07-07 | 1976-04-07 | ||
| US4115503A (en) * | 1973-08-22 | 1978-09-19 | Monsanto Company | Novel process for the preparation of fiber of arylene oxadiazole/arylene N-alkylhydrazide copolymer |
| JPS543240B2 (enExample) * | 1973-12-06 | 1979-02-20 | ||
| JPS5239680B2 (enExample) * | 1974-04-10 | 1977-10-06 | ||
| GB1527352A (en) * | 1974-09-17 | 1978-10-04 | Ici Ltd | Shaped articles of polyoxadiazoles |
| FR2318841A1 (fr) * | 1975-07-25 | 1977-02-18 | Comp Generale Electricite | Procede de liaison entre pieces en alumine beta alcaline et en alumine alpha |
| US4205038A (en) * | 1975-09-05 | 1980-05-27 | Imperial Chemical Industries Limited | Process for producing shaped articles of polyoxadiazoles |
| US4046731A (en) * | 1976-05-13 | 1977-09-06 | Monsanto Company | Process for preparing dopes from which shaped articles of oxadiazole/N-alkylhydrazide copolymers are obtained |
| US4500701A (en) * | 1982-09-27 | 1985-02-19 | Standard Oil Company (Indiana) | Co-polyoxadiazoles based on 5-t-butylisosphthalic acid |
| DE3620022A1 (de) | 1986-06-13 | 1987-12-17 | Basf Ag | Polyphenylen-1,3,4-oxadiazolpolymere |
| DD296277A5 (de) | 1990-06-29 | 1991-11-28 | Adw,Institut Fuer Polymerenchemie "Erich Correns",De | Verfahren zur herstellung von 1,3,4-oxadiazolen und von 1,3,4-oxadiazole enthaltenden polymeren |
-
2006
- 2006-05-01 US US11/414,959 patent/US7582721B2/en not_active Expired - Fee Related
-
2007
- 2007-04-26 EP EP07756011A patent/EP2013262B1/en not_active Not-in-force
- 2007-04-26 CA CA2648733A patent/CA2648733C/en active Active
- 2007-04-26 JP JP2009509609A patent/JP5036806B2/ja not_active Expired - Fee Related
- 2007-04-26 KR KR1020087029159A patent/KR101415409B1/ko not_active Expired - Fee Related
- 2007-04-26 WO PCT/US2007/010028 patent/WO2007133408A2/en not_active Ceased
- 2007-04-26 BR BRPI0710332-8A patent/BRPI0710332A2/pt not_active IP Right Cessation
- 2007-04-26 CN CN200780015848XA patent/CN101437871B/zh not_active Expired - Fee Related
- 2007-04-26 MX MX2008013839A patent/MX2008013839A/es active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| US20070255037A1 (en) | 2007-11-01 |
| EP2013262B1 (en) | 2012-02-01 |
| JP5036806B2 (ja) | 2012-09-26 |
| CA2648733A1 (en) | 2007-11-22 |
| KR20090008427A (ko) | 2009-01-21 |
| EP2013262A2 (en) | 2009-01-14 |
| CN101437871B (zh) | 2012-06-13 |
| CN101437871A (zh) | 2009-05-20 |
| KR101415409B1 (ko) | 2014-07-04 |
| US7582721B2 (en) | 2009-09-01 |
| MX2008013839A (es) | 2008-11-10 |
| CA2648733C (en) | 2014-10-28 |
| JP2009535481A (ja) | 2009-10-01 |
| WO2007133408A3 (en) | 2008-01-10 |
| WO2007133408A2 (en) | 2007-11-22 |
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