BR9814561A - Processos para a regeneração de catalisadores de tipo catalisador de tipo raney para a hidrogenação total ou parcial de funções nitrila em funções amina de compostos orgânicos, e para a hidrogenação de compostos, e, para a semi-hidrogenação de compostos - Google Patents
Processos para a regeneração de catalisadores de tipo catalisador de tipo raney para a hidrogenação total ou parcial de funções nitrila em funções amina de compostos orgânicos, e para a hidrogenação de compostos, e, para a semi-hidrogenação de compostosInfo
- Publication number
- BR9814561A BR9814561A BR9814561-4A BR9814561A BR9814561A BR 9814561 A BR9814561 A BR 9814561A BR 9814561 A BR9814561 A BR 9814561A BR 9814561 A BR9814561 A BR 9814561A
- Authority
- BR
- Brazil
- Prior art keywords
- hydrogenation
- compounds
- catalyst
- regeneration
- functions
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title abstract 10
- 238000005984 hydrogenation reaction Methods 0.000 title abstract 8
- 238000000034 method Methods 0.000 title abstract 7
- 230000008929 regeneration Effects 0.000 title abstract 5
- 238000011069 regeneration method Methods 0.000 title abstract 5
- 150000001875 compounds Chemical class 0.000 title abstract 4
- 150000001412 amines Chemical group 0.000 title abstract 3
- 150000002825 nitriles Chemical group 0.000 title abstract 2
- 150000002894 organic compounds Chemical class 0.000 title abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title 1
- 239000007868 Raney catalyst Substances 0.000 title 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 239000003637 basic solution Substances 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J25/00—Catalysts of the Raney type
- B01J25/04—Regeneration or reactivation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
"PROCESSOS PARA A REGENERAçãO DE CATALISADORES DE TIPO CATALISADOR DE TIPO RANEY PARA A HIDROGENAçãO TOTAL OU PARCIAL DE FUNçõES NITRILA EM FUNçõES AMINA DE COMPOSTOS ORGâNICOS, E PARA A HIDROGENAçãO DE COMPOSTOS, E, PARA A SEMI-HIDROGENAçãO DE COMPOSTOS". A invenção refere-se a um processo para a regeneração de catalisador de hidrogenação, e processos de hidrogenação realizados com um catalisador compreendendo pelo menos um catalisador regenerado. Mais particularmente, ela se refere a um processo para a regeneração de catalisadores tipo Raney usados em processos de hidrocarboneto totais ou parciais de compostos compreendendo funções nitrila em funções amina. O referido processo consiste no tratamento de catalisador gasto com uma solução básica e opcionalmente em submeter referido catalisador a hidrogenação antes de uma lavagem para eliminar as impurezas presentes no catalisador. Assim, o processo de regeneração permite recuperar até 100% da atividade catalítica.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9716832A FR2773086B1 (fr) | 1997-12-29 | 1997-12-29 | Procede de regeneration d'un catalyseur d'hydrogenation procede d'hydrogenation de composes comprenant des fonctions nitriles |
PCT/FR1998/002856 WO1999033561A1 (fr) | 1997-12-29 | 1998-12-23 | Procede de regeneration d'un catalyseur d'hydrogenation procede d'hydrogenation de composes comprenant des fonctions nitriles |
Publications (1)
Publication Number | Publication Date |
---|---|
BR9814561A true BR9814561A (pt) | 2001-10-16 |
Family
ID=9515406
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR9814561-4A BR9814561A (pt) | 1997-12-29 | 1998-12-23 | Processos para a regeneração de catalisadores de tipo catalisador de tipo raney para a hidrogenação total ou parcial de funções nitrila em funções amina de compostos orgânicos, e para a hidrogenação de compostos, e, para a semi-hidrogenação de compostos |
Country Status (15)
Country | Link |
---|---|
US (1) | US6518449B1 (pt) |
EP (1) | EP1042068B1 (pt) |
JP (1) | JP3725422B2 (pt) |
KR (1) | KR100529200B1 (pt) |
CN (1) | CN1194815C (pt) |
BR (1) | BR9814561A (pt) |
CA (1) | CA2316821C (pt) |
CZ (1) | CZ20002448A3 (pt) |
DE (1) | DE69837162T2 (pt) |
FR (1) | FR2773086B1 (pt) |
PL (1) | PL341404A1 (pt) |
RU (1) | RU2190469C2 (pt) |
SK (1) | SK9902000A3 (pt) |
UA (1) | UA62988C2 (pt) |
WO (1) | WO1999033561A1 (pt) |
Families Citing this family (37)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2806081B1 (fr) * | 2000-03-08 | 2003-03-14 | Rhodia Polyamide Intermediates | Procede d'hydrogenation de fonctions nitriles en fonctions amines |
DE10047703A1 (de) | 2000-09-25 | 2002-04-11 | Basf Ag | Verfahren zur Regenerierung von Katalysatoren |
FR2834984B1 (fr) * | 2002-01-21 | 2005-08-19 | Rhodia Polyamide Intermediates | Procede continu d'hydrogenation de nitriles ou composes nitres en amines |
WO2004066703A2 (en) * | 2003-01-31 | 2004-08-12 | Dsm Ip Assets B.V. | Process for the catalytic hydrogenation of a nitrile |
JP5415287B2 (ja) | 2007-03-01 | 2014-02-12 | ビーエーエスエフ ソシエタス・ヨーロピア | Eddnを経由するtetaの新規製法 |
CN101675025B (zh) | 2007-03-01 | 2015-04-08 | 巴斯夫欧洲公司 | 制备四亚乙基五胺的方法 |
JP5409393B2 (ja) * | 2007-03-01 | 2014-02-05 | ビーエーエスエフ ソシエタス・ヨーロピア | エチレンアミンの製造方法 |
US7960590B2 (en) * | 2007-03-01 | 2011-06-14 | Basf Se | Method for producing ethyleneamines from untreated AAN |
JP5393486B2 (ja) | 2007-03-01 | 2014-01-22 | ビーエーエスエフ ソシエタス・ヨーロピア | トリエチレンテトラアミンの製造方法 |
FR2921922B1 (fr) * | 2007-10-04 | 2009-12-04 | Rhodia Operations | Procede de fabrication d'amines par hydrogenation de composes nitriles |
CN101590411B (zh) * | 2008-05-28 | 2012-11-07 | 北京三聚环保新材料股份有限公司 | 一种非贵金属加氢催化剂及其制备方法 |
FR2935704B1 (fr) * | 2008-09-09 | 2010-08-27 | Rhodia Operations | Procede de fabrication d'amines |
CN102803213B (zh) | 2009-06-18 | 2015-05-13 | 巴斯夫欧洲公司 | 甲基取代的teta化合物 |
FR2971248B1 (fr) | 2011-02-04 | 2013-08-16 | Rhodia Operations | Preparation de diamine via la preparation d'aminonitrile |
JP5934339B2 (ja) * | 2011-04-15 | 2016-06-15 | ラディチ キミカ ソシエタ ペル アチオニ | ヘキサメチレンジアミンを製造するための改良された方法 |
EP2731926B1 (en) | 2011-07-07 | 2016-12-28 | Solvay (Zhangjiagang) Speciality Chemicals Co., Ltd. | Process for the preparation of aminonitrile and diamine |
WO2013030144A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn, edmn, teta und deta |
US8952156B2 (en) | 2011-08-31 | 2015-02-10 | Basf Se | Process for working up reaction outputs from the hydrogenation of EDDN or EDMN |
US8946459B2 (en) | 2011-08-31 | 2015-02-03 | Basf Se | Process for preparing EDDN and/or EDMN by reacting EDFA and/or EDMFA with HCN |
CN103764614A (zh) | 2011-08-31 | 2014-04-30 | 巴斯夫欧洲公司 | Eddn或edmn氢化反应出料的后处理方法 |
WO2013030174A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von edfa und/oder edmfa und deta und/oder teta |
WO2013030255A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn und/oder edmn sowie verfahren zur herstellung von deta und/oder teta |
WO2013030023A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn und/oder edmn sowie ein verfahren zur herstellung von deta und/oder teta |
US9012638B2 (en) | 2011-08-31 | 2015-04-21 | Basf Se | Process for preparing EDDN and/or EDMN by conversion of FACH and EDA |
WO2013030254A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von teta und/oder deta |
IN2014CN00791A (pt) | 2011-08-31 | 2015-04-03 | Basf Se | |
WO2013030259A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von teta |
US9096497B2 (en) | 2011-08-31 | 2015-08-04 | Basf Se | Process for preparing EDDN and EDMN |
EP2751068A1 (de) | 2011-08-31 | 2014-07-09 | Basf Se | Verfahren zur herstellung von eddn und/oder edmn durch umsetzung von fach und eda |
WO2013030172A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur regenierung von raney-katalysatoren |
CN103764617B (zh) | 2011-08-31 | 2015-12-02 | 巴斯夫欧洲公司 | 通过使edfa和/或edmfa与hcn反应制备eddn和/或edmn的方法 |
WO2013030249A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von aminen durch hydrierung von nitrilen |
CN105073712B (zh) | 2013-01-30 | 2017-09-22 | 巴斯夫欧洲公司 | 2,6‑双(氨基甲基)哌啶衍生物 |
CN105051003B (zh) | 2013-02-28 | 2017-05-03 | 巴斯夫欧洲公司 | 使用不含so2的氢氰酸制备eda的方法 |
BR112015031493A2 (pt) * | 2013-06-17 | 2017-07-25 | Basf Se | processo para a regeneração de um catalisador de metal nobre suportado |
CN114436852B (zh) * | 2020-11-03 | 2024-05-07 | 中国石油化工股份有限公司 | 己二腈加氢制备己二胺的方法 |
CN113649084B (zh) * | 2021-09-08 | 2024-02-23 | 天津理工大学 | 安全性多孔镍催化剂活性恢复的方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE832604C (de) * | 1947-12-05 | 1952-02-25 | Ici Ltd | Verfahren zur Herstellung von porigen Nickel-Aluminium-Katalysatoren |
GB642861A (en) * | 1948-08-13 | 1950-09-13 | Peter William Reynolds | Improvements in and relating to the preparation of foraminate catalysts |
NL90034C (pt) * | 1956-10-15 | |||
JPS5338719B2 (pt) * | 1972-12-25 | 1978-10-17 |
-
1997
- 1997-12-29 FR FR9716832A patent/FR2773086B1/fr not_active Expired - Fee Related
-
1998
- 1998-12-23 BR BR9814561-4A patent/BR9814561A/pt not_active IP Right Cessation
- 1998-12-23 KR KR20007007291A patent/KR100529200B1/ko not_active IP Right Cessation
- 1998-12-23 RU RU2000120191/04A patent/RU2190469C2/ru not_active IP Right Cessation
- 1998-12-23 US US09/582,657 patent/US6518449B1/en not_active Expired - Lifetime
- 1998-12-23 JP JP2000526298A patent/JP3725422B2/ja not_active Expired - Fee Related
- 1998-12-23 EP EP98963616A patent/EP1042068B1/fr not_active Expired - Lifetime
- 1998-12-23 SK SK990-2000A patent/SK9902000A3/sk unknown
- 1998-12-23 UA UA2000063814A patent/UA62988C2/uk unknown
- 1998-12-23 WO PCT/FR1998/002856 patent/WO1999033561A1/fr active IP Right Grant
- 1998-12-23 PL PL98341404A patent/PL341404A1/xx unknown
- 1998-12-23 CA CA002316821A patent/CA2316821C/fr not_active Expired - Fee Related
- 1998-12-23 CZ CZ20002448A patent/CZ20002448A3/cs unknown
- 1998-12-23 DE DE69837162T patent/DE69837162T2/de not_active Expired - Lifetime
- 1998-12-23 CN CNB988133490A patent/CN1194815C/zh not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE69837162D1 (de) | 2007-04-05 |
RU2190469C2 (ru) | 2002-10-10 |
CA2316821A1 (fr) | 1999-07-08 |
DE69837162T2 (de) | 2007-11-15 |
UA62988C2 (en) | 2004-01-15 |
FR2773086A1 (fr) | 1999-07-02 |
KR20010033766A (ko) | 2001-04-25 |
CN1194815C (zh) | 2005-03-30 |
EP1042068B1 (fr) | 2007-02-21 |
CN1284010A (zh) | 2001-02-14 |
FR2773086B1 (fr) | 2000-02-11 |
CA2316821C (fr) | 2004-05-11 |
KR100529200B1 (ko) | 2005-11-17 |
WO1999033561A1 (fr) | 1999-07-08 |
JP3725422B2 (ja) | 2005-12-14 |
US6518449B1 (en) | 2003-02-11 |
CZ20002448A3 (cs) | 2001-02-14 |
PL341404A1 (en) | 2001-04-09 |
EP1042068A1 (fr) | 2000-10-11 |
JP2001526956A (ja) | 2001-12-25 |
SK9902000A3 (en) | 2000-11-07 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 23/12/1998, OBSERVADAS AS CONDICOES LEGAIS. |
|
B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time | ||
B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |