BR112019022946A2 - amadurecimento de 1,4-bis(4-fenoxibenzoil)benzeno - Google Patents

amadurecimento de 1,4-bis(4-fenoxibenzoil)benzeno Download PDF

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Publication number
BR112019022946A2
BR112019022946A2 BR112019022946A BR112019022946A BR112019022946A2 BR 112019022946 A2 BR112019022946 A2 BR 112019022946A2 BR 112019022946 A BR112019022946 A BR 112019022946A BR 112019022946 A BR112019022946 A BR 112019022946A BR 112019022946 A2 BR112019022946 A2 BR 112019022946A2
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BR
Brazil
Prior art keywords
phenoxybenzoyl
benzene
bis
phase
lewis acid
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BR112019022946A
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English (en)
Inventor
Vincent Guillaume
Jouanneau Julien
Amstutz Jérome
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Arkema France
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Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of BR112019022946A2 publication Critical patent/BR112019022946A2/pt

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/46—Friedel-Crafts reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/30—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with halogen containing compounds, e.g. hypohalogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/41—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrogenolysis or reduction of carboxylic groups or functional derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/79—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G61/12—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule
    • C08G61/127—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from carbon dioxide, carbonyl halide, carboxylic acids or their derivatives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
    • C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
    • C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
    • C08G65/4043—(I) or (II) containing oxygen other than as phenol or carbonyl group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L65/00—Compositions of macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/30—Monomer units or repeat units incorporating structural elements in the main chain
    • C08G2261/34—Monomer units or repeat units incorporating structural elements in the main chain incorporating partially-aromatic structural elements in the main chain
    • C08G2261/344—Monomer units or repeat units incorporating structural elements in the main chain incorporating partially-aromatic structural elements in the main chain containing heteroatoms
    • C08G2261/3442—Polyetherketones
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/40—Polymerisation processes
    • C08G2261/45—Friedel-Crafts-type

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Polyethers (AREA)

Abstract

a presente invenção refere-se a um método para fabricação de 1,4-bis(4-fenoxibenzoil)benzeno compreendendo: reagir cloreto de tereftaloíla com éter de difenila em um solvente de reação e na presença de um ácido de lewis, de modo a obter uma mistura de produto compreendendo complexo de ácido 1,4-bis(4-fenoxibenzoil)benzeno-lewis; pôr a mistura de produto em contato com um solvente prótico, de modo a obter uma primeira fase contendo ácido de lewis e uma segunda fase contendo 1,4-bis(4-fenoxibenzoil)benzeno; aquecer pelo menos a segunda fase até uma temperatura máxima, seguido por esfriamento da segunda fase para uma temperatura de separação; submeter pelo menos a segunda fase a uma etapa de separação sólido/líquido na temperatura de separação, de modo a recuperar 1,4-bis(4-fenoxibenzoil)benzeno sólido.
BR112019022946A 2017-05-18 2018-05-17 amadurecimento de 1,4-bis(4-fenoxibenzoil)benzeno BR112019022946A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17305582.3A EP3404012B1 (en) 2017-05-18 2017-05-18 Ripening of 1,4-bis (4-phenoxybenzoyl)benzene
PCT/EP2018/063017 WO2018211048A1 (en) 2017-05-18 2018-05-17 Ripening of 1,4-bis (4-phenoxybenzoyl) benzene

Publications (1)

Publication Number Publication Date
BR112019022946A2 true BR112019022946A2 (pt) 2020-06-09

Family

ID=58779048

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112019022946A BR112019022946A2 (pt) 2017-05-18 2018-05-17 amadurecimento de 1,4-bis(4-fenoxibenzoil)benzeno

Country Status (10)

Country Link
US (2) US10981852B2 (pt)
EP (2) EP3404012B1 (pt)
JP (1) JP2020520362A (pt)
KR (1) KR102416475B1 (pt)
CN (1) CN110637004B (pt)
BR (1) BR112019022946A2 (pt)
CA (1) CA3061562A1 (pt)
MX (1) MX2019013010A (pt)
RU (1) RU2019141826A (pt)
WO (1) WO2018211048A1 (pt)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10793500B2 (en) * 2017-05-16 2020-10-06 Arkema France Dissociation of 1,4-bis (4-phenoxybenzoyl)benzene—Lewis acid complex in a protic solvent
EP3404011B1 (en) 2017-05-18 2020-08-26 Arkema France Dissociation of a 1,4-bis(4-phenoxybenzoyl)benzene-lewis acid-complex in an aqueous solution
ES2829260T3 (es) 2017-05-16 2021-05-31 Arkema France Método para fabricar 1,4-bis(4-fenoxibenzoil)benceno usando cloruro de tereftaloílo sustancialmente no hidrolizado
EP3404008B1 (en) 2017-05-16 2020-08-12 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene at an elevated temperature
EP3650433B1 (en) 2018-11-09 2024-04-24 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoylbenzene) at an elevated temperature
KR20220028244A (ko) * 2020-08-28 2022-03-08 한화솔루션 주식회사 1,4-비스(4-페녹시벤조일)벤젠을 제조하는 방법 및 이에 의해 제조된 1,4-비스(4-페녹시벤조일)벤젠

Family Cites Families (27)

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SU626555A1 (ru) 1973-03-05 1979-07-25 Институт высокомолекулярных соединений 1,4 Бис (4-ацетил-4-феноксибензоил) бензол-мономер дл прочного при изгибе и термостойкого полимера
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CA1246297A (en) 1985-03-11 1988-12-06 Robert A. Clendinning Process for preparing poly(aryl ether ketones)
US4891167A (en) 1985-05-02 1990-01-02 Amoco Corporation Block polymers containing a poly(aryl ether ketone) and methods for their production
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DE3789354T2 (de) * 1986-11-20 1994-08-04 Asahi Chemical Ind Aromatischer Polyether und Verfahren zur Herstellung eines Polyethers.
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EP3404009B1 (en) 2017-05-16 2019-12-25 Arkema France Method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene in supersaturation conditions
ES2829260T3 (es) 2017-05-16 2021-05-31 Arkema France Método para fabricar 1,4-bis(4-fenoxibenzoil)benceno usando cloruro de tereftaloílo sustancialmente no hidrolizado
EP3404011B1 (en) 2017-05-18 2020-08-26 Arkema France Dissociation of a 1,4-bis(4-phenoxybenzoyl)benzene-lewis acid-complex in an aqueous solution
US10793500B2 (en) 2017-05-16 2020-10-06 Arkema France Dissociation of 1,4-bis (4-phenoxybenzoyl)benzene—Lewis acid complex in a protic solvent
EP3404008B1 (en) 2017-05-16 2020-08-12 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene at an elevated temperature
EP3404013B1 (en) 2017-05-18 2021-10-27 Arkema France Purification of 1,4-bis (4-phenoxybenzoyl)benzene by centrifugal filtration
EP3438085A1 (en) 2017-08-04 2019-02-06 Arkema France Process for producing polyether ketone ketone

Also Published As

Publication number Publication date
KR102416475B1 (ko) 2022-07-01
CA3061562A1 (en) 2018-11-22
RU2019141826A (ru) 2021-06-18
EP3404012B1 (en) 2020-09-09
JP2020520362A (ja) 2020-07-09
EP3404012A1 (en) 2018-11-21
MX2019013010A (es) 2020-02-05
US10981852B2 (en) 2021-04-20
CN110637004B (zh) 2023-04-18
WO2018211048A1 (en) 2018-11-22
US20210155570A1 (en) 2021-05-27
CN110637004A (zh) 2019-12-31
EP3625207A1 (en) 2020-03-25
US20190152886A1 (en) 2019-05-23
KR20200009037A (ko) 2020-01-29

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B350 Update of information on the portal [chapter 15.35 patent gazette]
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