BR112019023115A2 - Método para fabricação de 1,4-bis(4-fenoxibenzoil)benzeno usando cloreto de tereftaloíla substancialmente não hidrolisado - Google Patents

Método para fabricação de 1,4-bis(4-fenoxibenzoil)benzeno usando cloreto de tereftaloíla substancialmente não hidrolisado Download PDF

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Publication number
BR112019023115A2
BR112019023115A2 BR112019023115-3A BR112019023115A BR112019023115A2 BR 112019023115 A2 BR112019023115 A2 BR 112019023115A2 BR 112019023115 A BR112019023115 A BR 112019023115A BR 112019023115 A2 BR112019023115 A2 BR 112019023115A2
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BR
Brazil
Prior art keywords
benzene
bis
chloride
terephthaloyl chloride
tereftaloyl
Prior art date
Application number
BR112019023115-3A
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English (en)
Inventor
Le Guillaume
Jouanneau Julien
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Arkema France
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Publication date
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Publication of BR112019023115A2 publication Critical patent/BR112019023115A2/pt

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/46—Friedel-Crafts reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/76—Ketones containing a keto group bound to a six-membered aromatic ring
    • C07C49/84—Ketones containing a keto group bound to a six-membered aromatic ring containing ether groups, groups, groups, or groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G61/12—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule
    • C08G61/127—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from carbon dioxide, carbonyl halide, carboxylic acids or their derivatives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
    • C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
    • C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
    • C08G65/4093—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group characterised by the process or apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L65/00—Compositions of macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/30—Monomer units or repeat units incorporating structural elements in the main chain
    • C08G2261/34—Monomer units or repeat units incorporating structural elements in the main chain incorporating partially-aromatic structural elements in the main chain
    • C08G2261/344—Monomer units or repeat units incorporating structural elements in the main chain incorporating partially-aromatic structural elements in the main chain containing heteroatoms
    • C08G2261/3442—Polyetherketones
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/40—Polymerisation processes
    • C08G2261/45—Friedel-Crafts-type
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/28—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type
    • C08G2650/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type containing oxygen in addition to the ether group
    • C08G2650/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type containing oxygen in addition to the ether group containing ketone groups, e.g. polyarylethylketones, PEEK or PEK
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/62—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the nature of monomer used

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Polyethers (AREA)

Abstract

a invenção refere-se a um método para fabricação de 1,4-bis(4-fenoxibenzoil)benzeno compreendendo: - prover cloreto de tereftaloíla, éter de difenila, um solvente e um ácido de lewis, em que o cloreto de tereftaloíla é de um grau de pureza de modo que, 10 minutos após introdução dele em uma concentração de referência de 6,5% em peso no dito solvente, em uma temperatura de 20º c, uma solução é obtida tendo uma turbidez de menos de 500 ntu; - misturar o cloreto de tereftaloíla, o éter de difenila e o solvente de modo a produzir uma mistura reagente; - adicionar o ácido de lewis à mistura reagente de modo a realizar a reação do cloreto de tereftaloíla com o éter de difenila; - recuperar uma mistura de produto compreendendo um complexo de 1,4-bis(4-fenoxibenzoil)benzeno-ácido de lewis.
BR112019023115-3A 2017-05-16 2018-05-16 Método para fabricação de 1,4-bis(4-fenoxibenzoil)benzeno usando cloreto de tereftaloíla substancialmente não hidrolisado BR112019023115A2 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP17305562.5A EP3404010B1 (en) 2017-05-16 2017-05-16 Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene using substantially non-hydrolyzed terephthaloyl chloride
EP17305562.5 2017-05-16
PCT/EP2018/062813 WO2018210971A1 (en) 2017-05-16 2018-05-16 Method for manufacturing 1,4-bis(4—phenoxybenzoylbenzene) using substantially non-hydrolyzed terephthaloyl chloride

Publications (1)

Publication Number Publication Date
BR112019023115A2 true BR112019023115A2 (pt) 2020-05-26

Family

ID=58779041

Family Applications (1)

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BR112019023115-3A BR112019023115A2 (pt) 2017-05-16 2018-05-16 Método para fabricação de 1,4-bis(4-fenoxibenzoil)benzeno usando cloreto de tereftaloíla substancialmente não hidrolisado

Country Status (11)

Country Link
US (2) US10807933B2 (pt)
EP (2) EP3404010B1 (pt)
JP (1) JP2020520360A (pt)
KR (1) KR20200007871A (pt)
CN (1) CN110621649B (pt)
BR (1) BR112019023115A2 (pt)
CA (1) CA3061435A1 (pt)
ES (1) ES2829260T3 (pt)
MX (1) MX2019013005A (pt)
RU (1) RU2019141279A (pt)
WO (1) WO2018210971A1 (pt)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3404009B1 (en) * 2017-05-16 2019-12-25 Arkema France Method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene in supersaturation conditions
US10793500B2 (en) 2017-05-16 2020-10-06 Arkema France Dissociation of 1,4-bis (4-phenoxybenzoyl)benzene—Lewis acid complex in a protic solvent
ES2829260T3 (es) 2017-05-16 2021-05-31 Arkema France Método para fabricar 1,4-bis(4-fenoxibenzoil)benceno usando cloruro de tereftaloílo sustancialmente no hidrolizado
EP3404012B1 (en) 2017-05-18 2020-09-09 Arkema France Ripening of 1,4-bis (4-phenoxybenzoyl)benzene
EP3404008B1 (en) 2017-05-16 2020-08-12 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene at an elevated temperature
ES2829267T3 (es) 2017-05-18 2021-05-31 Arkema France Disociación de un complejo de 1,4-bis(4-fenoxibenzoilo)benceno-ácido de Lewis en una disolución acuosa
EP3438085A1 (en) * 2017-08-04 2019-02-06 Arkema France Process for producing polyether ketone ketone
EP3650433B1 (en) 2018-11-09 2024-04-24 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoylbenzene) at an elevated temperature
FR3110572B1 (fr) * 2020-05-19 2022-10-07 Arkema France Dérivé de xanthène, mélanges le comprenant, procédé de fabrication et utilisations correspondants
KR20220028244A (ko) * 2020-08-28 2022-03-08 한화솔루션 주식회사 1,4-비스(4-페녹시벤조일)벤젠을 제조하는 방법 및 이에 의해 제조된 1,4-비스(4-페녹시벤조일)벤젠

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EP3404013B1 (en) 2017-05-18 2021-10-27 Arkema France Purification of 1,4-bis (4-phenoxybenzoyl)benzene by centrifugal filtration
US10793500B2 (en) 2017-05-16 2020-10-06 Arkema France Dissociation of 1,4-bis (4-phenoxybenzoyl)benzene—Lewis acid complex in a protic solvent
EP3404009B1 (en) 2017-05-16 2019-12-25 Arkema France Method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene in supersaturation conditions
ES2829260T3 (es) 2017-05-16 2021-05-31 Arkema France Método para fabricar 1,4-bis(4-fenoxibenzoil)benceno usando cloruro de tereftaloílo sustancialmente no hidrolizado
EP3404012B1 (en) 2017-05-18 2020-09-09 Arkema France Ripening of 1,4-bis (4-phenoxybenzoyl)benzene
EP3404008B1 (en) 2017-05-16 2020-08-12 Arkema France Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene at an elevated temperature
ES2829267T3 (es) 2017-05-18 2021-05-31 Arkema France Disociación de un complejo de 1,4-bis(4-fenoxibenzoilo)benceno-ácido de Lewis en una disolución acuosa
EP3438085A1 (en) 2017-08-04 2019-02-06 Arkema France Process for producing polyether ketone ketone

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Publication number Publication date
RU2019141279A (ru) 2021-06-16
CA3061435A1 (en) 2018-11-22
JP2020520360A (ja) 2020-07-09
US20180334419A1 (en) 2018-11-22
US10807933B2 (en) 2020-10-20
EP3404010B1 (en) 2020-08-12
KR20200007871A (ko) 2020-01-22
EP3625203A1 (en) 2020-03-25
MX2019013005A (es) 2020-02-05
WO2018210971A1 (en) 2018-11-22
EP3404010A1 (en) 2018-11-21
CN110621649B (zh) 2023-05-09
US10611715B2 (en) 2020-04-07
CN110621649A (zh) 2019-12-27
US20200079717A1 (en) 2020-03-12
ES2829260T3 (es) 2021-05-31

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