BR112014011308B1 - Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo - Google Patents

Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo Download PDF

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Publication number
BR112014011308B1
BR112014011308B1 BR112014011308-4A BR112014011308A BR112014011308B1 BR 112014011308 B1 BR112014011308 B1 BR 112014011308B1 BR 112014011308 A BR112014011308 A BR 112014011308A BR 112014011308 B1 BR112014011308 B1 BR 112014011308B1
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BR
Brazil
Prior art keywords
cha
frame structure
ppm
group
zeolitic material
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BR112014011308-4A
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English (en)
Portuguese (pt)
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BR112014011308A2 (pt
Inventor
Stefan Maurer
Hanpeng Jin
Jeff Yang
Ulrich Müller
Original Assignee
Basf Se
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Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112014011308A2 publication Critical patent/BR112014011308A2/pt
Publication of BR112014011308B1 publication Critical patent/BR112014011308B1/pt

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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015CHA-type, e.g. Chabazite, LZ-218
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/10Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least phosphorus atoms
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10After treatment, characterised by the effect to be obtained
    • B01J2229/18After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Compositions Of Oxide Ceramics (AREA)
BR112014011308-4A 2011-11-11 2012-11-09 Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo BR112014011308B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11188857 2011-11-11
EP11188857.4 2011-11-11
PCT/IB2012/056292 WO2013068976A1 (en) 2011-11-11 2012-11-09 Organotemplate-free synthetic process for the production of a zeolitic material of the cha-type structure

Publications (2)

Publication Number Publication Date
BR112014011308A2 BR112014011308A2 (pt) 2017-05-09
BR112014011308B1 true BR112014011308B1 (pt) 2021-04-13

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BR112014011308-4A BR112014011308B1 (pt) 2011-11-11 2012-11-09 Processo sintético livre de organotemplate para a produção de um material zeolítico, material zeolítico livre de organotemplate sintético e uso do mesmo

Country Status (12)

Country Link
EP (1) EP2776369B1 (enExample)
JP (1) JP6324895B2 (enExample)
KR (1) KR102032584B1 (enExample)
CN (1) CN104039704B (enExample)
BR (1) BR112014011308B1 (enExample)
CA (1) CA2855572C (enExample)
IN (1) IN2014CN03353A (enExample)
MX (1) MX375064B (enExample)
PL (1) PL2776369T3 (enExample)
RU (1) RU2612697C2 (enExample)
WO (1) WO2013068976A1 (enExample)
ZA (1) ZA201404210B (enExample)

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CN104837770B (zh) 2012-12-10 2017-04-26 埃克森美孚研究工程公司 铝硅酸盐分子筛的晶种合成
ES2574500B1 (es) * 2014-12-17 2017-03-31 Consejo Superior De Investigaciones Científicas (Csic) Síntesis de la zeolita con la estructura cristalina CHA, procedimiento de síntesis y su uso en aplicaciones catalíticas
WO2016099775A1 (en) * 2014-12-17 2016-06-23 Sabic Global Techologies B.V. Silicoaluminophosphate catalyst for chloromethane conversion
US10710059B2 (en) * 2015-12-22 2020-07-14 Basf Corporation Process for preparing iron(III)-exchanged zeolite composition
CN109219481A (zh) * 2016-06-08 2019-01-15 巴斯夫公司 来自无有机模板的合成的CHA骨架结构的铜助催化沸石材料及其在NOx的选择性催化还原中的用途
WO2017211237A1 (en) 2016-06-08 2017-12-14 Basf Corporation Copper-promoted gmelinite and use thereof in the selective catalytic reduction of nox
CN106145138B (zh) * 2016-06-27 2018-05-08 杨晓波 一种合成具有菱沸石结构的沸石分子筛的方法
CN106145137B (zh) * 2016-06-27 2018-06-05 杨晓波 一种直接水热合成中硅铝比菱沸石的方法
CN110139829B (zh) * 2016-12-02 2023-10-13 埃科莱布美国股份有限公司 聚铝盐及其在制备高纯度胶体铝-二氧化硅复合颗粒和沸石中的用途
WO2018210815A1 (en) 2017-05-15 2018-11-22 Basf Se A process for preparing a zeolitic material comprising a metal m and having framework type aei
US11224867B2 (en) 2017-05-15 2022-01-18 Basf Corporation Process for preparing a zeolitic material having framework type AEI
KR102578657B1 (ko) * 2017-07-11 2023-09-15 쉘 인터내셔날 리써취 마트샤피지 비.브이. 촉매 및 이의 사용 방법
JP2020533164A (ja) * 2017-09-07 2020-11-19 ビーエーエスエフ コーポレーション 骨格外アルミニウムを減じたゼオライト
CN108217681B (zh) * 2018-01-19 2021-07-06 山东齐鲁华信高科有限公司 一种高铁含量的Fe-ZSM-5分子筛的制备方法
CN108083292B (zh) * 2018-01-31 2020-12-29 吉林大学 一种磷掺杂cha分子筛、制备方法及其应用
EP3801891A4 (en) 2018-05-25 2022-03-09 Basf Se RARE EARTH ELEMENT WITH ALUMINUM RICH ZEOLITE MATERIAL
JP7494174B2 (ja) 2018-07-27 2024-06-03 ビーエーエスエフ ソシエタス・ヨーロピア 骨格型ferを有するゼオライト材料の製造方法
KR102881133B1 (ko) 2019-05-15 2025-11-05 바스프 모바일 에미션스 카탈리스츠 엘엘씨 Cha-aft 제올라이트 연정 coe-10의 제조 방법 및 비균질 촉매작용에서의 이의 용도
CN111348660B (zh) * 2020-03-16 2022-08-09 江西师范大学 一种中硅cha型分子筛及其制备方法和应用
CN111762795B (zh) * 2020-07-13 2022-10-14 包头稀土研究院 含有稀土元素的分子筛及其生产方法
CN111762794B (zh) * 2020-07-13 2022-08-05 包头稀土研究院 分子筛及其制备方法
EP4015454A1 (en) * 2020-12-21 2022-06-22 Tosoh Corporation Cha-type zeolite and manufacturing method thereof
CN112919493B (zh) * 2021-02-05 2022-10-14 正大能源材料(大连)有限公司 一种低成本制备ssz-13分子筛的方法及应用

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SU833498A1 (ru) * 1979-06-25 1981-05-30 Институт Общей И Неорганической Химииан Армянской Ccp Способ получени шабазита
SU1640112A1 (ru) * 1987-12-28 1991-04-07 Предприятие П/Я Р-6518 Синтетический натриево-цезиевый цеолит типа шабазит
EP1105347B1 (en) * 1998-07-29 2012-11-28 ExxonMobil Chemical Patents Inc. Processes for manufacture of molecular sieves
JP4508654B2 (ja) * 2002-03-15 2010-07-21 エクソンモービル・ケミカル・パテンツ・インク 高シリカシャバサイト、その合成及びオキシジェネート類のオレフィン類への変換におけるその使用
WO2005063622A2 (en) 2003-12-23 2005-07-14 Exxonmobil Chemical Patents Inc. Chabazite-type molecular sieve, its synthesis and its use in the conversion of oxygenates to olefins
US20090196812A1 (en) * 2008-01-31 2009-08-06 Basf Catalysts Llc Catalysts, Systems and Methods Utilizing Non-Zeolitic Metal-Containing Molecular Sieves Having the CHA Crystal Structure
US10583424B2 (en) * 2008-11-06 2020-03-10 Basf Corporation Chabazite zeolite catalysts having low silica to alumina ratios
JP5238908B2 (ja) * 2009-06-18 2013-07-17 ビーエーエスエフ ソシエタス・ヨーロピア ゼオライト材料を生成するための有機テンプレート不要の合成プロセス
WO2011064186A1 (en) * 2009-11-24 2011-06-03 Basf Se Process for the preparation of zeolites having cha structure
CN102134081A (zh) * 2010-01-25 2011-07-27 天津海赛纳米材料有限公司 无模板剂存在下一种sapo-34分子筛的合成方法
CN102285666B (zh) * 2010-06-18 2015-02-04 江西师范大学 一种菱沸石及菱沸石膜的制备方法
CN103561865B (zh) * 2011-04-18 2016-09-07 Pq公司 大晶体、不含有机物的菱沸石以及制造和使用其的方法
CN102442679B (zh) * 2011-09-29 2013-08-14 南开大学 一种菱沸石的合成方法

Also Published As

Publication number Publication date
MX2014005537A (es) 2014-09-16
JP2015511919A (ja) 2015-04-23
PL2776369T3 (pl) 2022-06-20
ZA201404210B (en) 2015-08-26
CN104039704B (zh) 2017-10-24
EP2776369A4 (en) 2015-08-05
KR20140093982A (ko) 2014-07-29
JP6324895B2 (ja) 2018-05-16
IN2014CN03353A (enExample) 2015-07-03
RU2014123614A (ru) 2015-12-20
CA2855572C (en) 2020-04-28
WO2013068976A1 (en) 2013-05-16
CN104039704A (zh) 2014-09-10
EP2776369A1 (en) 2014-09-17
MX375064B (es) 2025-03-06
BR112014011308A2 (pt) 2017-05-09
KR102032584B1 (ko) 2019-10-15
RU2612697C2 (ru) 2017-03-13
CA2855572A1 (en) 2013-05-16
EP2776369B1 (en) 2022-02-23

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B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 09/11/2012, OBSERVADAS AS CONDICOES LEGAIS.

B25A Requested transfer of rights approved

Owner name: BASF CATALYSTS LLC (US)

B25A Requested transfer of rights approved

Owner name: BASF MOBILE EMISSIONS CATALYSTS LLC (US)