AU2016228933B2 - A method and a container for preparing a fused sample for analysis - Google Patents
A method and a container for preparing a fused sample for analysis Download PDFInfo
- Publication number
- AU2016228933B2 AU2016228933B2 AU2016228933A AU2016228933A AU2016228933B2 AU 2016228933 B2 AU2016228933 B2 AU 2016228933B2 AU 2016228933 A AU2016228933 A AU 2016228933A AU 2016228933 A AU2016228933 A AU 2016228933A AU 2016228933 B2 AU2016228933 B2 AU 2016228933B2
- Authority
- AU
- Australia
- Prior art keywords
- sample
- container
- region
- collector material
- cupel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000034 method Methods 0.000 title claims abstract description 73
- 238000004458 analytical method Methods 0.000 title claims abstract description 21
- 239000000463 material Substances 0.000 claims abstract description 92
- 239000010970 precious metal Substances 0.000 claims abstract description 43
- 238000010521 absorption reaction Methods 0.000 claims abstract description 30
- 239000011148 porous material Substances 0.000 claims abstract description 24
- 238000002844 melting Methods 0.000 claims abstract description 5
- 230000008018 melting Effects 0.000 claims abstract description 5
- 238000010438 heat treatment Methods 0.000 claims description 15
- 229910052709 silver Inorganic materials 0.000 claims description 15
- 239000004332 silver Substances 0.000 claims description 15
- 238000011068 loading method Methods 0.000 claims description 12
- 230000007246 mechanism Effects 0.000 claims description 12
- 230000003647 oxidation Effects 0.000 claims description 6
- 238000007254 oxidation reaction Methods 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 230000008859 change Effects 0.000 claims description 4
- 239000000523 sample Substances 0.000 description 87
- 239000011133 lead Substances 0.000 description 44
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 13
- 230000004907 flux Effects 0.000 description 13
- 229910052500 inorganic mineral Inorganic materials 0.000 description 11
- 239000011707 mineral Substances 0.000 description 11
- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 description 9
- 230000008569 process Effects 0.000 description 8
- 238000004611 spectroscopical analysis Methods 0.000 description 7
- 229910000464 lead oxide Inorganic materials 0.000 description 5
- 239000000155 melt Substances 0.000 description 5
- 238000001636 atomic emission spectroscopy Methods 0.000 description 4
- YEXPOXQUZXUXJW-UHFFFAOYSA-N lead(II) oxide Inorganic materials [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 4
- 239000000395 magnesium oxide Substances 0.000 description 4
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 4
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 4
- 239000002893 slag Substances 0.000 description 4
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000000608 laser ablation Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000012306 spectroscopic technique Methods 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 238000007499 fusion processing Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000010953 base metal Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012468 concentrated sample Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229910021397 glassy carbon Inorganic materials 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 230000033001 locomotion Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000011369 resultant mixture Substances 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 150000003378 silver Chemical class 0.000 description 1
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 description 1
- 238000007704 wet chemistry method Methods 0.000 description 1
- 238000004876 x-ray fluorescence Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
- B01L3/04—Crucibles
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B11/00—Obtaining noble metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B11/00—Obtaining noble metals
- C22B11/02—Obtaining noble metals by dry processes
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N1/405—Concentrating samples by adsorption or absorption
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2300/00—Additional constructional details
- B01L2300/08—Geometry, shape and general structure
- B01L2300/0848—Specific forms of parts of containers
- B01L2300/0851—Bottom walls
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Clinical Laboratory Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Sampling And Sample Adjustment (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2015900812A AU2015900812A0 (en) | 2015-03-06 | A method of preparing a fused sample for analysis | |
| AU2015900812 | 2015-03-06 | ||
| AU2015900849 | 2015-03-10 | ||
| AU2015900849A AU2015900849A0 (en) | 2015-03-10 | A method of preparing a fused sample for analysis | |
| PCT/AU2016/000069 WO2016141405A1 (en) | 2015-03-06 | 2016-03-04 | A method and a container for preparing a fused sample for analysis |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| AU2016228933A1 AU2016228933A1 (en) | 2017-08-24 |
| AU2016228933B2 true AU2016228933B2 (en) | 2021-07-22 |
Family
ID=56879812
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2016228933A Active AU2016228933B2 (en) | 2015-03-06 | 2016-03-04 | A method and a container for preparing a fused sample for analysis |
Country Status (10)
| Country | Link |
|---|---|
| CN (2) | CN112629963A (zh) |
| AU (1) | AU2016228933B2 (zh) |
| BR (1) | BR112017018916B1 (zh) |
| CA (1) | CA2977255C (zh) |
| CL (1) | CL2017002234A1 (zh) |
| DE (1) | DE112016001054T5 (zh) |
| MX (1) | MX2017011314A (zh) |
| RU (1) | RU2721764C2 (zh) |
| WO (1) | WO2016141405A1 (zh) |
| ZA (1) | ZA201705903B (zh) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016141405A1 (en) * | 2015-03-06 | 2016-09-15 | Imp Group (Pty) Ltd | A method and a container for preparing a fused sample for analysis |
| JP7123846B2 (ja) * | 2019-03-29 | 2022-08-23 | Ｊｘ金属株式会社 | 鉛ボタン投入用冶具及びそれを用いた鉛ボタンの灰吹き方法 |
| WO2022150511A1 (en) * | 2021-01-07 | 2022-07-14 | Fremonta Corporation | Devices, systems and methods for microbial sampling of frozen products |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4372543A (en) * | 1981-05-14 | 1983-02-08 | Gardiner Philip M | Cupel |
| AU5447386A (en) * | 1985-01-08 | 1986-09-11 | Western Biotechnology Ltd. | Fire assay cupel |
| US5279644A (en) * | 1993-02-18 | 1994-01-18 | Asarco Incorporated | Fire refining precious metals asay method |
| SE513273C2 (sv) * | 1997-03-17 | 2000-08-14 | Boliden Mineral Ab | Degel för framställning av analysprovkroppar samt tillverkning av sådan degel |
| WO2002004919A2 (en) * | 2000-07-12 | 2002-01-17 | Innovative Met Products (Pty) Limited | Method and apparatus for the assay of precious metals |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA821914A (en) * | 1969-09-02 | C. Mathews Ted | Ore concentration process | |
| US4113383A (en) * | 1976-12-10 | 1978-09-12 | Technicon Instruments Corporation | Method and apparatus for solute transfer |
| FR2531534A1 (fr) * | 1982-08-03 | 1984-02-10 | Charbonnages De France | Capteur individuel portatif de poussieres |
| AU781664B2 (en) * | 1999-09-21 | 2005-06-02 | Alastair John Inglis | Standards for monitoring assaying of precious metals |
| CN1928528B (zh) * | 2005-09-09 | 2012-11-14 | 贺利氏贵金属股份有限及两合公司 | 对潮湿含贵金属后处理材料均匀化及分析方法 |
| DE102005049702A1 (de) * | 2005-09-09 | 2007-03-22 | W.C. Heraeus Gmbh | Homogenisierungs- und ggf. Analyse-Verfahren bei der Aufarbeitung feuchter edelmetallhaltiger Aufarbeitungsmaterialien mit unbekanntem Edelmetallgehalt |
| DE102009040263A1 (de) * | 2009-09-04 | 2011-03-17 | Flsmidth Wadgassen Gmbh | Abdichtvorrichtung für eine Verkokungsanlage |
| CN102253072A (zh) * | 2011-06-14 | 2011-11-23 | 白银有色集团股份有限公司 | 能够控制铅扣质量的火法试金法 |
| CN102706860A (zh) * | 2012-06-29 | 2012-10-03 | 广州有色金属研究院 | 一种铑含量的化学分析方法 |
| CN103575609B (zh) * | 2013-11-07 | 2015-07-01 | 广州有色金属研究院 | 一种液态金水中金的分析方法 |
| CN103926372B (zh) * | 2014-03-26 | 2015-09-09 | 湖南水口山有色金属集团有限公司 | 一种高铋物料中银含量的测定方法 |
| WO2016141405A1 (en) * | 2015-03-06 | 2016-09-15 | Imp Group (Pty) Ltd | A method and a container for preparing a fused sample for analysis |
| JP7123846B2 (ja) * | 2019-03-29 | 2022-08-23 | Ｊｘ金属株式会社 | 鉛ボタン投入用冶具及びそれを用いた鉛ボタンの灰吹き方法 |
-
2016
- 2016-03-04 WO PCT/AU2016/000069 patent/WO2016141405A1/en active Application Filing
- 2016-03-04 RU RU2017132566A patent/RU2721764C2/ru active
- 2016-03-04 CN CN202011117117.XA patent/CN112629963A/zh active Pending
- 2016-03-04 MX MX2017011314A patent/MX2017011314A/es unknown
- 2016-03-04 CA CA2977255A patent/CA2977255C/en active Active
- 2016-03-04 BR BR112017018916-0A patent/BR112017018916B1/pt active IP Right Grant
- 2016-03-04 DE DE112016001054.0T patent/DE112016001054T5/de active Pending
- 2016-03-04 CN CN201680014097.9A patent/CN107430049A/zh active Pending
- 2016-03-04 AU AU2016228933A patent/AU2016228933B2/en active Active
-
2017
- 2017-08-30 ZA ZA2017/05903A patent/ZA201705903B/en unknown
- 2017-09-04 CL CL2017002234A patent/CL2017002234A1/es unknown
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4372543A (en) * | 1981-05-14 | 1983-02-08 | Gardiner Philip M | Cupel |
| AU5447386A (en) * | 1985-01-08 | 1986-09-11 | Western Biotechnology Ltd. | Fire assay cupel |
| US5279644A (en) * | 1993-02-18 | 1994-01-18 | Asarco Incorporated | Fire refining precious metals asay method |
| SE513273C2 (sv) * | 1997-03-17 | 2000-08-14 | Boliden Mineral Ab | Degel för framställning av analysprovkroppar samt tillverkning av sådan degel |
| WO2002004919A2 (en) * | 2000-07-12 | 2002-01-17 | Innovative Met Products (Pty) Limited | Method and apparatus for the assay of precious metals |
Non-Patent Citations (1)
| Title |
|---|
| MCINTOSH, K.S., "Integrating pyrometallurgy and robotic systems engineering: Fully automated fire assay laboratory for rapid PGE analysis", Vol. 19, No. 3, pp. 219-231, March 2006 * |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2016141405A1 (en) | 2016-09-15 |
| RU2017132566A (ru) | 2019-04-08 |
| BR112017018916B1 (pt) | 2021-10-05 |
| CL2017002234A1 (es) | 2018-05-04 |
| CA2977255C (en) | 2023-01-31 |
| MX2017011314A (es) | 2018-05-15 |
| CN107430049A (zh) | 2017-12-01 |
| CA2977255A1 (en) | 2016-09-15 |
| ZA201705903B (en) | 2018-12-19 |
| AU2016228933A1 (en) | 2017-08-24 |
| CN112629963A (zh) | 2021-04-09 |
| RU2721764C2 (ru) | 2020-05-22 |
| RU2017132566A3 (zh) | 2019-08-30 |
| BR112017018916A2 (pt) | 2018-05-15 |
| DE112016001054T5 (de) | 2018-01-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK1 | Application lapsed section 142(2)(a) - no request for examination in relevant period | ||
| PC1 | Assignment before grant (sect. 113) |
Owner name: FLSMIDTH A/S Free format text: FORMER APPLICANT(S): IMP GROUP (PTY) LTD |
|
| NB | Applications allowed - extensions of time section 223(2) |
Free format text: THE TIME IN WHICH TO REQUEST EXAMINATION HAS BEEN EXTENDED TO 26 FEB 2020 |
|
| FGA | Letters patent sealed or granted (standard patent) |