AU2015221373C1 - Methods for treating lithium-containing materials - Google Patents

Methods for treating lithium-containing materials Download PDF

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Publication number
AU2015221373C1
AU2015221373C1 AU2015221373A AU2015221373A AU2015221373C1 AU 2015221373 C1 AU2015221373 C1 AU 2015221373C1 AU 2015221373 A AU2015221373 A AU 2015221373A AU 2015221373 A AU2015221373 A AU 2015221373A AU 2015221373 C1 AU2015221373 C1 AU 2015221373C1
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AU
Australia
Prior art keywords
lithium
aqueous composition
lithium sulfate
bisulfate
sulfate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
AU2015221373A
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English (en)
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AU2015221373B2 (en
AU2015221373A1 (en
Inventor
Pierre Bouchard
Guy BOURASSA
Genevieve Clayton
J. David Genders
Mykolas GLADKOVAS
Nicolas Laroche
Stephen Charles MACKIE
Jean-Francois Magnan
Gary PEARSE
Peter Symons
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Nemaska Lithium Inc
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Nemaska Lithium Inc
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Publication date
Application filed by Nemaska Lithium Inc filed Critical Nemaska Lithium Inc
Publication of AU2015221373A1 publication Critical patent/AU2015221373A1/en
Priority to AU2019203355A priority Critical patent/AU2019203355B2/en
Publication of AU2015221373B2 publication Critical patent/AU2015221373B2/en
Application granted granted Critical
Publication of AU2015221373C1 publication Critical patent/AU2015221373C1/en
Priority to AU2021204689A priority patent/AU2021204689B2/en
Priority to AU2024203143A priority patent/AU2024203143A1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • C25B1/01Products
    • C25B1/14Alkali metal compounds
    • C25B1/16Hydroxides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025Reverse osmosis; Hyperfiltration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/422Electrodialysis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44Ion-selective electrodialysis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58Multistep processes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D1/00Oxides or hydroxides of sodium, potassium or alkali metals in general
    • C01D1/04Hydroxides
    • C01D1/20Preparation by reacting oxides or hydroxides with alkali metal salts
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/02Oxides; Hydroxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/06Sulfates; Sulfites
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00Preliminary treatment of ores or scrap
    • C22B1/02Roasting processes
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00Preliminary treatment of ores or scrap
    • C22B1/02Roasting processes
    • C22B1/06Sulfating roasting
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10Obtaining alkali metals
    • C22B26/12Obtaining lithium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/08Sulfuric acid, other sulfurated acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/70Assemblies comprising two or more cells
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2311/00Details relating to membrane separation process operations and control
    • B01D2311/26Further operations combined with membrane separation processes
    • B01D2311/2684Electrochemical processes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Water Supply & Treatment (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Urology & Nephrology (AREA)
  • Electrochemistry (AREA)
  • Nanotechnology (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Processing Of Solid Wastes (AREA)
  • Treatment Of Sludge (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Electrolytic Production Of Metals (AREA)
AU2015221373A 2014-02-24 2015-02-24 Methods for treating lithium-containing materials Active AU2015221373C1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
AU2019203355A AU2019203355B2 (en) 2014-02-24 2019-05-14 Methods for treating lithium-containing materials
AU2021204689A AU2021204689B2 (en) 2014-02-24 2021-07-05 Methods for treating lithium-containing materials
AU2024203143A AU2024203143A1 (en) 2014-02-24 2024-05-13 Methods for treating lithium-containing materials

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201461943700P 2014-02-24 2014-02-24
US61/943,700 2014-02-24
PCT/CA2015/000115 WO2015123762A1 (en) 2014-02-24 2015-02-24 Methods for treating lithium-containing materials

Related Child Applications (1)

Application Number Title Priority Date Filing Date
AU2019203355A Division AU2019203355B2 (en) 2014-02-24 2019-05-14 Methods for treating lithium-containing materials

Publications (3)

Publication Number Publication Date
AU2015221373A1 AU2015221373A1 (en) 2016-09-29
AU2015221373B2 AU2015221373B2 (en) 2019-05-30
AU2015221373C1 true AU2015221373C1 (en) 2019-09-05

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AU2015221373A Active AU2015221373C1 (en) 2014-02-24 2015-02-24 Methods for treating lithium-containing materials
AU2019203355A Active AU2019203355B2 (en) 2014-02-24 2019-05-14 Methods for treating lithium-containing materials
AU2021204689A Active AU2021204689B2 (en) 2014-02-24 2021-07-05 Methods for treating lithium-containing materials
AU2024203143A Pending AU2024203143A1 (en) 2014-02-24 2024-05-13 Methods for treating lithium-containing materials

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AU2019203355A Active AU2019203355B2 (en) 2014-02-24 2019-05-14 Methods for treating lithium-containing materials
AU2021204689A Active AU2021204689B2 (en) 2014-02-24 2021-07-05 Methods for treating lithium-containing materials
AU2024203143A Pending AU2024203143A1 (en) 2014-02-24 2024-05-13 Methods for treating lithium-containing materials

Country Status (15)

Country Link
US (5) US10544512B2 (cg-RX-API-DMAC7.html)
EP (3) EP3110988B1 (cg-RX-API-DMAC7.html)
JP (3) JP6449317B2 (cg-RX-API-DMAC7.html)
KR (3) KR102341052B1 (cg-RX-API-DMAC7.html)
CN (2) CN106103806B (cg-RX-API-DMAC7.html)
AU (4) AU2015221373C1 (cg-RX-API-DMAC7.html)
CA (6) CA3086843C (cg-RX-API-DMAC7.html)
CL (2) CL2016002121A1 (cg-RX-API-DMAC7.html)
DK (2) DK3110988T3 (cg-RX-API-DMAC7.html)
ES (2) ES2743245T3 (cg-RX-API-DMAC7.html)
HR (2) HRP20191302T1 (cg-RX-API-DMAC7.html)
PL (2) PL3492632T3 (cg-RX-API-DMAC7.html)
PT (2) PT3492632T (cg-RX-API-DMAC7.html)
RS (2) RS61569B1 (cg-RX-API-DMAC7.html)
WO (1) WO2015123762A1 (cg-RX-API-DMAC7.html)

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