ATE245633T1 - Verfahren zur herstellung eines triazolinthion- derivates - Google Patents
Verfahren zur herstellung eines triazolinthion- derivatesInfo
- Publication number
- ATE245633T1 ATE245633T1 AT00991158T AT00991158T ATE245633T1 AT E245633 T1 ATE245633 T1 AT E245633T1 AT 00991158 T AT00991158 T AT 00991158T AT 00991158 T AT00991158 T AT 00991158T AT E245633 T1 ATE245633 T1 AT E245633T1
- Authority
- AT
- Austria
- Prior art keywords
- derivative
- formula
- reacting
- followed
- hydrochloric acid
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- 239000003085 diluting agent Substances 0.000 abstract 2
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 abstract 2
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 abstract 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 abstract 1
- ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- BIVUUOPIAYRCAP-UHFFFAOYSA-N aminoazanium;chloride Chemical class Cl.NN BIVUUOPIAYRCAP-UHFFFAOYSA-N 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N hydrogen thiocyanate Natural products SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 125000005310 triazolidinyl group Chemical class N1(NNCC1)* 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
- C07D249/10—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D249/12—Oxygen or sulfur atoms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Communicable Diseases (AREA)
- Animal Behavior & Ethology (AREA)
- Oncology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Thiazole And Isothizaole Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19961603A DE19961603A1 (de) | 1999-12-21 | 1999-12-21 | Verfahren zur Herstellung eines Triazolinthion-Derivates |
| PCT/EP2000/012494 WO2001046158A1 (de) | 1999-12-21 | 2000-12-08 | Verfahren zur herstellung eines triazolinthion-derivates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE245633T1 true ATE245633T1 (de) | 2003-08-15 |
Family
ID=7933520
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT00991158T ATE245633T1 (de) | 1999-12-21 | 2000-12-08 | Verfahren zur herstellung eines triazolinthion- derivates |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US6559317B2 (de) |
| EP (1) | EP1242388B1 (de) |
| JP (1) | JP3959275B2 (de) |
| KR (1) | KR100591607B1 (de) |
| CN (1) | CN1187343C (de) |
| AT (1) | ATE245633T1 (de) |
| AU (1) | AU3156501A (de) |
| DE (2) | DE19961603A1 (de) |
| DK (1) | DK1242388T3 (de) |
| ES (1) | ES2200988T3 (de) |
| HU (1) | HUP0203851A3 (de) |
| IL (2) | IL149712A0 (de) |
| MX (1) | MX224322B (de) |
| PL (1) | PL199444B1 (de) |
| TW (1) | TW523509B (de) |
| WO (1) | WO2001046158A1 (de) |
| ZA (1) | ZA200203859B (de) |
Families Citing this family (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060238702A1 (en) | 1999-04-30 | 2006-10-26 | Advanced Medical Optics, Inc. | Ophthalmic lens combinations |
| US20120016349A1 (en) | 2001-01-29 | 2012-01-19 | Amo Development, Llc. | Hybrid ophthalmic interface apparatus and method of interfacing a surgical laser with an eye |
| US7763069B2 (en) | 2002-01-14 | 2010-07-27 | Abbott Medical Optics Inc. | Accommodating intraocular lens with outer support structure |
| DE10233171A1 (de) * | 2002-07-22 | 2004-02-12 | Bayer Cropscience Ag | Kristallmodifikation II des 2-[2-(Chlor-cyclopropyl)-3-(2-chlorphenyl)-2-hydroxy-propyl]-2,4dihydro-3H-1,2,4-triazol-3-thions |
| US20040082993A1 (en) * | 2002-10-25 | 2004-04-29 | Randall Woods | Capsular intraocular lens implant having a refractive liquid therein |
| US7662180B2 (en) | 2002-12-05 | 2010-02-16 | Abbott Medical Optics Inc. | Accommodating intraocular lens and method of manufacture thereof |
| US8137399B2 (en) * | 2005-04-11 | 2012-03-20 | Vision Solutions Technologies, Inc. | Implantable prismatic device, and related methods and systems |
| US9636213B2 (en) | 2005-09-30 | 2017-05-02 | Abbott Medical Optics Inc. | Deformable intraocular lenses and lens systems |
| US20080161914A1 (en) | 2006-12-29 | 2008-07-03 | Advanced Medical Optics, Inc. | Pre-stressed haptic for accommodating intraocular lens |
| US8034108B2 (en) | 2008-03-28 | 2011-10-11 | Abbott Medical Optics Inc. | Intraocular lens having a haptic that includes a cap |
| BRPI1009073A2 (pt) | 2009-06-12 | 2016-03-01 | Basf Se | compostos de triazol das fórmulas i e ii, compostos das fórmulas i e ii, composição agrícola, uso de um composto da fórmula i ou ii, método para controlar fungos nocivos, semente, composição farmacêutica, uso de um composto da fórmula i ou ii e método para tratar câncer ou infecções por vírus ou para combater fungos patogênicos para seres humanos e para animais |
| JP2012530109A (ja) | 2009-06-18 | 2012-11-29 | ビーエーエスエフ ソシエタス・ヨーロピア | 抗菌性１，２，４−トリアゾリル誘導体 |
| JP2012530111A (ja) | 2009-06-18 | 2012-11-29 | ビーエーエスエフ ソシエタス・ヨーロピア | ５−硫黄置換基を有する抗菌類性１，２，４−トリアゾリル誘導体 |
| BRPI1009656A2 (pt) | 2009-06-18 | 2016-08-09 | Basf Se | composto triazol das fórmulas i e ii, composição agrícola, uso de um composto de fórmula i, ii e/ou iv, méeodo para o controle de fungos nocivos, semente, composição farmacêutical e método para tratamento contra o câncer ou infecções virais, ou para o combate de fungos zoopatogênicos ou humanopatogênicos |
| WO2010149758A1 (en) | 2009-06-25 | 2010-12-29 | Basf Se | Antifungal 1, 2, 4-triazolyl derivatives |
| CA2766655C (en) | 2009-06-26 | 2017-10-10 | Abbott Medical Optics Inc. | Accommodating intraocular lenses |
| US8343217B2 (en) | 2009-08-03 | 2013-01-01 | Abbott Medical Optics Inc. | Intraocular lens and methods for providing accommodative vision |
| BR112012015040A2 (pt) | 2009-12-18 | 2015-09-22 | Basf Se | processo para a preparação de grupos tio-triazol substituídos da fórmula geral (i) e compostos (lla) |
| US9084674B2 (en) | 2012-05-02 | 2015-07-21 | Abbott Medical Optics Inc. | Intraocular lens with shape changing capability to provide enhanced accomodation and visual acuity |
| EP2984080B1 (de) * | 2013-04-12 | 2017-08-30 | Bayer CropScience Aktiengesellschaft | Neuartige triazolderivate |
| CN104557742A (zh) * | 2013-10-15 | 2015-04-29 | 上海生华化学科技有限公司 | 一种丙硫菌唑类似物的制备方法 |
| CN105949137B (zh) | 2016-07-15 | 2019-01-29 | 泸州东方农化有限公司 | 一种丙硫菌唑及其光学活性体的合成方法和中间体 |
| EP3580217A1 (de) | 2017-02-08 | 2019-12-18 | Bayer Aktiengesellschaft | Triazolthionderivate |
| CN107043359B (zh) * | 2017-05-31 | 2019-08-09 | 江苏七洲绿色化工股份有限公司 | 一种丙硫菌唑中间体的制备方法 |
| CN106986838B (zh) * | 2017-05-31 | 2019-11-15 | 江苏七洲绿色化工股份有限公司 | 一种丙硫菌唑的制备方法 |
| CN107445909B (zh) * | 2017-07-31 | 2020-04-21 | 江苏七洲绿色化工股份有限公司 | 一种丙硫菌唑中间体的制备方法 |
| EP3681438A1 (de) | 2017-09-11 | 2020-07-22 | AMO Groningen B.V. | Verfahren und vorrichtungen zur erhöhung der positionsstabilität von intraokularlinsen |
| CN109912522B (zh) * | 2017-12-12 | 2021-04-13 | 北京颖泰嘉和生物科技股份有限公司 | 制备三唑啉硫酮化合物的方法 |
| US11292775B2 (en) | 2017-12-21 | 2022-04-05 | Gsp Crop Science Pvt. Ltd. | Efficient process for the synthesis of 2-[2-(1-chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-2,4-dihydro-3H-1,2,4-triazole-3-thione(prothioconazole) and its intermediates |
| CN108358860B (zh) * | 2018-02-08 | 2023-11-21 | 辽宁众辉生物科技有限公司 | 一种高收率合成丙硫菌唑的方法 |
| CN108912062B (zh) * | 2018-06-21 | 2020-10-27 | 江西天宇化工有限公司 | 一种三唑硫酮衍生物的制备方法 |
| CN108689952B (zh) * | 2018-06-21 | 2020-10-27 | 江西天宇化工有限公司 | 一种丙硫菌唑的制备方法 |
| CN109232452B (zh) * | 2018-11-01 | 2020-11-24 | 欧阳建峰 | 一种高品质丙硫菌唑的制备方法 |
| CN109369549A (zh) * | 2018-12-29 | 2019-02-22 | 安徽久易农业股份有限公司 | 一种丙硫菌唑的制备方法 |
| CN110218196A (zh) * | 2019-05-20 | 2019-09-10 | 江苏蓝丰生物化工股份有限公司 | 丙硫菌唑中间体三唑烷衍生物的制备方法 |
| CN110183389A (zh) * | 2019-06-25 | 2019-08-30 | 芮城县斯普伦迪生物工程有限公司 | 一种三唑硫酮类衍生化合物及制备方法 |
| CN110498733A (zh) * | 2019-09-17 | 2019-11-26 | 西安近代化学研究所 | 一种1-（2-氯苯基）-2-（1-氯环丙基）-3-肼基-2-丙醇盐酸盐的合成方法 |
| CN113024476A (zh) * | 2019-12-25 | 2021-06-25 | 北京颖泰嘉和生物科技股份有限公司 | 丙硫菌唑化合物的制备方法 |
| CN111892547A (zh) * | 2020-08-28 | 2020-11-06 | 安徽久易农业股份有限公司 | 一种丙硫菌唑中间体的合成方法 |
| EP4247796A1 (de) | 2020-11-19 | 2023-09-27 | Adama Makhteshim Ltd. | Verfahren zur herstellung von prothioconazol und zwischenprodukten davon |
| CN114478411B (zh) * | 2021-09-29 | 2025-03-07 | 辽宁众辉生物科技有限公司 | 丙硫菌唑的合成方法 |
| CN113666840B (zh) * | 2021-10-22 | 2022-01-11 | 江苏七洲绿色科技研究院有限公司 | 一种丙硫菌唑中间体的制备方法 |
| CN116375658A (zh) * | 2021-12-24 | 2023-07-04 | 宁夏苏融达化工有限公司 | 一种丙硫菌唑的制备方法 |
| CN116162067B (zh) * | 2023-04-21 | 2023-08-08 | 江苏七洲绿色科技研究院有限公司 | 一种丙硫菌唑的制备方法 |
| WO2025099715A1 (en) | 2023-11-06 | 2025-05-15 | Adama Makhteshim Ltd. | Process for preparing a salt of prothioconazole and process for preparing prothioconzaole |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3812967A1 (de) * | 1987-06-24 | 1989-01-05 | Bayer Ag | Azolylmethyl-cyclopropyl-derivate |
| DE4030039A1 (de) * | 1990-09-22 | 1992-03-26 | Bayer Ag | Verfahren zur herstellung von 2-(1-chlor-cyclopropyl)-1- (2-chlor-phenyl)-3-(1,2,4-triazol-1-yl- propan-2-ol |
| ES2258824T3 (es) * | 1997-10-08 | 2006-09-01 | Bayer Cropscience Ag | Procedimiento para la obtencion de derivados de triazolintiona. |
| DE19744401A1 (de) * | 1997-10-08 | 1999-04-15 | Bayer Ag | Verfahren zur Herstellung von Triazolinthion-Derivaten |
| DE19744400A1 (de) * | 1997-10-08 | 1999-04-15 | Bayer Ag | Verfahren zur Herstellung von Triazolinthion-Derivaten |
-
1999
- 1999-12-21 DE DE19961603A patent/DE19961603A1/de not_active Withdrawn
-
2000
- 2000-12-08 MX MXPA02006157 patent/MX224322B/es active IP Right Grant
- 2000-12-08 PL PL355711A patent/PL199444B1/pl not_active IP Right Cessation
- 2000-12-08 EP EP00991158A patent/EP1242388B1/de not_active Expired - Lifetime
- 2000-12-08 CN CNB008173753A patent/CN1187343C/zh not_active Expired - Lifetime
- 2000-12-08 AT AT00991158T patent/ATE245633T1/de active
- 2000-12-08 DE DE50003044T patent/DE50003044D1/de not_active Expired - Lifetime
- 2000-12-08 IL IL14971200A patent/IL149712A0/xx active IP Right Grant
- 2000-12-08 ES ES00991158T patent/ES2200988T3/es not_active Expired - Lifetime
- 2000-12-08 JP JP2001547069A patent/JP3959275B2/ja not_active Expired - Lifetime
- 2000-12-08 DK DK00991158T patent/DK1242388T3/da active
- 2000-12-08 KR KR20027006570A patent/KR100591607B1/ko not_active Expired - Lifetime
- 2000-12-08 AU AU31565/01A patent/AU3156501A/en not_active Abandoned
- 2000-12-08 US US10/149,933 patent/US6559317B2/en not_active Expired - Lifetime
- 2000-12-08 HU HU0203851A patent/HUP0203851A3/hu unknown
- 2000-12-08 WO PCT/EP2000/012494 patent/WO2001046158A1/de active IP Right Grant
- 2000-12-20 TW TW089127308A patent/TW523509B/zh not_active IP Right Cessation
-
2002
- 2002-05-15 ZA ZA200203859A patent/ZA200203859B/en unknown
- 2002-05-16 IL IL149712A patent/IL149712A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN1187343C (zh) | 2005-02-02 |
| IL149712A0 (en) | 2002-11-10 |
| HUP0203851A2 (hu) | 2003-04-28 |
| CN1411450A (zh) | 2003-04-16 |
| KR100591607B1 (ko) | 2006-06-20 |
| HUP0203851A3 (en) | 2004-12-28 |
| IL149712A (en) | 2006-10-05 |
| JP2003518104A (ja) | 2003-06-03 |
| DK1242388T3 (da) | 2003-11-17 |
| US6559317B2 (en) | 2003-05-06 |
| ES2200988T3 (es) | 2004-03-16 |
| US20030013890A1 (en) | 2003-01-16 |
| EP1242388B1 (de) | 2003-07-23 |
| JP3959275B2 (ja) | 2007-08-15 |
| ZA200203859B (en) | 2003-05-15 |
| MX224322B (es) | 2004-11-19 |
| TW523509B (en) | 2003-03-11 |
| EP1242388A1 (de) | 2002-09-25 |
| WO2001046158A1 (de) | 2001-06-28 |
| AU3156501A (en) | 2001-07-03 |
| DE50003044D1 (de) | 2003-08-28 |
| PL199444B1 (pl) | 2008-09-30 |
| PL355711A1 (en) | 2004-05-17 |
| DE19961603A1 (de) | 2001-06-28 |
| KR20020052215A (ko) | 2002-07-02 |
| MXPA02006157A (es) | 2003-01-28 |
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